BRPI0514800A - processo para oxidação em fase lìquida, e reator de coluna de bolhas - Google Patents
processo para oxidação em fase lìquida, e reator de coluna de bolhasInfo
- Publication number
- BRPI0514800A BRPI0514800A BRPI0514800-6A BRPI0514800A BRPI0514800A BR PI0514800 A BRPI0514800 A BR PI0514800A BR PI0514800 A BRPI0514800 A BR PI0514800A BR PI0514800 A BRPI0514800 A BR PI0514800A
- Authority
- BR
- Brazil
- Prior art keywords
- liquid phase
- phase oxidation
- bubble column
- column reactor
- cta
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1872—Details of the fluidised bed reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/1836—Heating and cooling the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
- B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
- B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
- C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
- C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
- B01J2208/00008—Controlling the process
- B01J2208/00017—Controlling the temperature
- B01J2208/00106—Controlling the temperature by indirect heat exchange
- B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
- B01J2208/0015—Plates; Cylinders
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Combustion & Propulsion (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
PROCESSO PARA OXIDAçãO EM FASE LìQUIDA, E REATOR DE COLUNA DE BOLHAS. São revelados um processo e aparelho otimizados para realizar de forma mais eficiente e económica a oxidação em fase líquida de um composto oxidável. Tal oxidação em fase líquida é realizada em um reator de coluna de bolhas que permite uma reação altamente eficiente a temperaturas relativamente baixas. Quando o composto oxidado é para-xileno e o produto da reação de oxidação é ácido tereftálico bruto (CTA), tal produto CTA pode ser purificado e seprado por técnicas mais económicas do que as que poderiam ser empregadas se o CTA fosse formado por um processo convencional de oxidação a alta temperatura.
Applications Claiming Priority (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US60685604P | 2004-09-02 | 2004-09-02 | |
US63132004P | 2004-11-29 | 2004-11-29 | |
US63139904P | 2004-11-29 | 2004-11-29 | |
US11/154,202 US7692036B2 (en) | 2004-11-29 | 2005-06-16 | Optimized liquid-phase oxidation |
US11/154,218 US7568361B2 (en) | 2004-09-02 | 2005-06-16 | Optimized liquid-phase oxidation |
PCT/US2005/030546 WO2006028752A2 (en) | 2004-09-02 | 2005-08-29 | Optimized liquid-phase oxidation |
Publications (2)
Publication Number | Publication Date |
---|---|
BRPI0514800A true BRPI0514800A (pt) | 2008-06-24 |
BRPI0514800B1 BRPI0514800B1 (pt) | 2015-11-24 |
Family
ID=35504618
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0514800A BRPI0514800B1 (pt) | 2004-09-02 | 2005-08-29 | processo para oxidação em fase líquida, e reator de coluna de bolhas |
Country Status (12)
Country | Link |
---|---|
EP (1) | EP1791800B1 (pt) |
JP (1) | JP2008511638A (pt) |
KR (2) | KR101281347B1 (pt) |
CN (2) | CN101023046B (pt) |
BR (1) | BRPI0514800B1 (pt) |
CA (1) | CA2576632A1 (pt) |
ES (1) | ES2655728T3 (pt) |
LT (1) | LT1791800T (pt) |
MX (1) | MX2007002565A (pt) |
PL (1) | PL1791800T3 (pt) |
PT (1) | PT1791800T (pt) |
WO (1) | WO2006028752A2 (pt) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8066949B2 (en) | 2008-09-26 | 2011-11-29 | Exxonmobil Research & Engineering Company | Scrubber for fluid coker unit |
US8933266B2 (en) * | 2010-06-30 | 2015-01-13 | Uop Llc | Process for producing terephthalic acid |
US8933265B2 (en) * | 2010-06-30 | 2015-01-13 | Uop Llc | Process for oxidizing alkyl aromatic compounds |
RU2694865C2 (ru) * | 2013-09-25 | 2019-07-17 | Линде Акциенгезелльшафт | Колонна с жидкостными распределителями и массообменными тарелками из уголковых профилей |
CN109772236B (zh) * | 2017-11-14 | 2022-08-12 | 中国石油化工股份有限公司 | 一种流体分布器、反应装置及其应用 |
KR20230088131A (ko) * | 2021-12-10 | 2023-06-19 | 주식회사 엘지화학 | 기포탑 반응기 |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
AT236346B (de) * | 1961-01-25 | 1964-10-12 | Union Carbide Corp | Boden zum Inberührungbringen von Flüssigkeit und Gas |
DE1493192A1 (de) * | 1963-04-30 | 1969-02-20 | Standard Oil Co | Verfahren zur Herstellung von aromatischen Saeuren |
GB1250222A (pt) * | 1968-10-25 | 1971-10-20 | ||
US3660476A (en) * | 1968-10-30 | 1972-05-02 | Teijin Ltd | Method for the preparation of terephthalic acid |
BE724040A (pt) * | 1968-11-18 | 1969-05-02 | ||
JPS5912096B2 (ja) * | 1975-10-31 | 1984-03-21 | 三菱化学株式会社 | ホウコウゾクポリカルボンサンノセイゾウホウ |
JPS58177106A (ja) * | 1982-04-13 | 1983-10-17 | Jgc Corp | 多段式高流速気液接触装置 |
JPS59104345A (ja) * | 1982-12-03 | 1984-06-16 | Kuraray Yuka Kk | 直接重合用に適したテレフタル酸の製造方法 |
DE4318893A1 (de) * | 1993-06-07 | 1994-12-08 | Bayer Ag | Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat |
JP3719448B2 (ja) * | 1993-07-29 | 2005-11-24 | 三菱瓦斯化学株式会社 | 芳香族ジカルボン酸製造用酸化反応器 |
SI9500109A (en) * | 1995-04-05 | 1996-10-31 | Levec Janez Dipl Ing Prof Dr | Apparatus and Process for Thermal Oxidative Treatment of Waste Waters |
US5929274A (en) * | 1995-06-07 | 1999-07-27 | Hfm International, Inc. | Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid |
JPH09278709A (ja) * | 1996-02-13 | 1997-10-28 | Mitsubishi Chem Corp | 芳香族カルボン酸の製造方法 |
US6084125A (en) * | 1996-02-27 | 2000-07-04 | Praxair Technology, Inc. | Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid |
ID19133A (id) * | 1996-12-12 | 1998-06-18 | Praxair Technology Inc | Pengisian oksigen langsung kedalam reaktor-reaktor ruang gelembung |
GB9701251D0 (en) * | 1997-01-22 | 1997-03-12 | Bp Chem Int Ltd | Process |
DE19843573A1 (de) * | 1998-09-23 | 2000-03-30 | Degussa | Blasensäule und deren Verwendung |
CN1227208C (zh) * | 2000-01-21 | 2005-11-16 | Bp北美公司 | 在苯甲酸和水溶剂中氧化生产高纯芳香羧酸的方法 |
US7074954B2 (en) * | 2002-12-09 | 2006-07-11 | Eastman Chemical Company | Process for the oxidative purification of terephthalic acid |
MXPA05006120A (es) * | 2002-12-09 | 2005-08-16 | Eastman Chem Co | Proceso para la purificacion oxidativa de acido tereftalico. |
MXPA05006046A (es) * | 2002-12-09 | 2005-08-18 | Eastman Chem Co | Proceso para la purficiacion de una suspension de acido carboxilico crudo. |
-
2005
- 2005-08-29 JP JP2007530196A patent/JP2008511638A/ja active Pending
- 2005-08-29 KR KR1020077006865A patent/KR101281347B1/ko active IP Right Grant
- 2005-08-29 PT PT57929143T patent/PT1791800T/pt unknown
- 2005-08-29 EP EP05792914.3A patent/EP1791800B1/en active Active
- 2005-08-29 CN CN200580029558.1A patent/CN101023046B/zh active Active
- 2005-08-29 BR BRPI0514800A patent/BRPI0514800B1/pt active IP Right Grant
- 2005-08-29 LT LTEP05792914.3T patent/LT1791800T/lt unknown
- 2005-08-29 CA CA002576632A patent/CA2576632A1/en not_active Abandoned
- 2005-08-29 KR KR1020127032262A patent/KR101363824B1/ko active IP Right Grant
- 2005-08-29 WO PCT/US2005/030546 patent/WO2006028752A2/en active Application Filing
- 2005-08-29 MX MX2007002565A patent/MX2007002565A/es active IP Right Grant
- 2005-08-29 ES ES05792914.3T patent/ES2655728T3/es active Active
- 2005-08-29 CN CN2010101169790A patent/CN101766979B/zh active Active
- 2005-08-29 PL PL05792914T patent/PL1791800T3/pl unknown
Also Published As
Publication number | Publication date |
---|---|
WO2006028752A2 (en) | 2006-03-16 |
EP1791800A2 (en) | 2007-06-06 |
KR20070048256A (ko) | 2007-05-08 |
KR20130003039A (ko) | 2013-01-08 |
CN101766979A (zh) | 2010-07-07 |
CN101023046A (zh) | 2007-08-22 |
JP2008511638A (ja) | 2008-04-17 |
CN101023046B (zh) | 2019-01-18 |
ES2655728T3 (es) | 2018-02-21 |
CN101766979B (zh) | 2012-12-26 |
KR101363824B1 (ko) | 2014-02-17 |
KR101281347B1 (ko) | 2013-07-02 |
WO2006028752A3 (en) | 2006-06-01 |
PT1791800T (pt) | 2018-02-02 |
PL1791800T3 (pl) | 2018-04-30 |
CA2576632A1 (en) | 2006-03-16 |
EP1791800B1 (en) | 2017-11-01 |
BRPI0514800B1 (pt) | 2015-11-24 |
LT1791800T (lt) | 2018-01-25 |
MX2007002565A (es) | 2007-04-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B08F | Application dismissed because of non-payment of annual fees [chapter 8.6 patent gazette] |
Free format text: REFERENTE A 9A ANUIDADE. |
|
B08H | Application fees: decision cancelled [chapter 8.8 patent gazette] |
Free format text: REFERENTE AO DESPACHO PUBLICADO 8.6 NA RPI 2269 DE 01/07/2014 |
|
B25G | Requested change of headquarter approved |
Owner name: EASTMAN CHEMICAL COMPANY (US) |
|
B25A | Requested transfer of rights approved |
Owner name: GRUPO PETROTEMEX, S.A. DE C.V. (MX) |
|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 24/11/2015, OBSERVADAS AS CONDICOES LEGAIS. |