ES2655728T3 - Oxidación optimizada en fase líquida - Google Patents

Oxidación optimizada en fase líquida Download PDF

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Publication number
ES2655728T3
ES2655728T3 ES05792914.3T ES05792914T ES2655728T3 ES 2655728 T3 ES2655728 T3 ES 2655728T3 ES 05792914 T ES05792914 T ES 05792914T ES 2655728 T3 ES2655728 T3 ES 2655728T3
Authority
ES
Spain
Prior art keywords
reaction medium
reaction
reaction zone
range
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES05792914.3T
Other languages
English (en)
Spanish (es)
Inventor
Alan George Wonders
Robert Lin
Marcel De Vreede
Lee Reynolds Partin
Wayne Scott Strasser
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Grupo Petrotemex SA de CV
Original Assignee
Grupo Petrotemex SA de CV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US11/154,202 external-priority patent/US7692036B2/en
Priority claimed from US11/154,218 external-priority patent/US7568361B2/en
Application filed by Grupo Petrotemex SA de CV filed Critical Grupo Petrotemex SA de CV
Application granted granted Critical
Publication of ES2655728T3 publication Critical patent/ES2655728T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1872—Details of the fluidised bed reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/006—Baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/1836—Heating and cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/20—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium
    • B01J8/22—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles with liquid as a fluidising medium gas being introduced into the liquid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/23—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups
    • C07C51/235—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of oxygen-containing groups to carboxyl groups of —CHO groups or primary alcohol groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00115—Controlling the temperature by indirect heat exchange with heat exchange elements inside the bed of solid particles
    • B01J2208/0015—Plates; Cylinders

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Combustion & Propulsion (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
ES05792914.3T 2004-09-02 2005-08-29 Oxidación optimizada en fase líquida Expired - Lifetime ES2655728T3 (es)

Applications Claiming Priority (11)

Application Number Priority Date Filing Date Title
US154202 1993-11-17
US60685604P 2004-09-02 2004-09-02
US606856P 2004-09-02
US63132004P 2004-11-29 2004-11-29
US63139904P 2004-11-29 2004-11-29
US631320P 2004-11-29
US631399P 2004-11-29
US154218 2005-06-16
US11/154,202 US7692036B2 (en) 2004-11-29 2005-06-16 Optimized liquid-phase oxidation
US11/154,218 US7568361B2 (en) 2004-09-02 2005-06-16 Optimized liquid-phase oxidation
PCT/US2005/030546 WO2006028752A2 (en) 2004-09-02 2005-08-29 Optimized liquid-phase oxidation

Publications (1)

Publication Number Publication Date
ES2655728T3 true ES2655728T3 (es) 2018-02-21

Family

ID=35504618

Family Applications (1)

Application Number Title Priority Date Filing Date
ES05792914.3T Expired - Lifetime ES2655728T3 (es) 2004-09-02 2005-08-29 Oxidación optimizada en fase líquida

Country Status (12)

Country Link
EP (1) EP1791800B1 (enExample)
JP (1) JP2008511638A (enExample)
KR (2) KR101363824B1 (enExample)
CN (2) CN101023046B (enExample)
BR (1) BRPI0514800B1 (enExample)
CA (1) CA2576632A1 (enExample)
ES (1) ES2655728T3 (enExample)
LT (1) LT1791800T (enExample)
MX (1) MX2007002565A (enExample)
PL (1) PL1791800T3 (enExample)
PT (1) PT1791800T (enExample)
WO (1) WO2006028752A2 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8066949B2 (en) 2008-09-26 2011-11-29 Exxonmobil Research & Engineering Company Scrubber for fluid coker unit
US8933265B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for oxidizing alkyl aromatic compounds
US8933266B2 (en) * 2010-06-30 2015-01-13 Uop Llc Process for producing terephthalic acid
WO2015043698A1 (de) * 2013-09-25 2015-04-02 Linde Aktiengesellschaft Kolonne mit flüssigkeitsverteiler und stoffaustauschboden aus winkelprofilen
CN109772236B (zh) * 2017-11-14 2022-08-12 中国石油化工股份有限公司 一种流体分布器、反应装置及其应用
KR102849255B1 (ko) 2021-12-10 2025-08-21 주식회사 엘지화학 기포탑 반응기
CN116351334B (zh) * 2022-12-14 2026-05-08 安徽利科新材料科技有限公司 Mnmp生产装置及生产方法

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AT236346B (de) * 1961-01-25 1964-10-12 Union Carbide Corp Boden zum Inberührungbringen von Flüssigkeit und Gas
DE1493192A1 (de) * 1963-04-30 1969-02-20 Standard Oil Co Verfahren zur Herstellung von aromatischen Saeuren
GB1250222A (enExample) * 1968-10-25 1971-10-20
US3660476A (en) * 1968-10-30 1972-05-02 Teijin Ltd Method for the preparation of terephthalic acid
BE724040A (enExample) * 1968-11-18 1969-05-02
JPS5912096B2 (ja) * 1975-10-31 1984-03-21 三菱化学株式会社 ホウコウゾクポリカルボンサンノセイゾウホウ
JPS58177106A (ja) * 1982-04-13 1983-10-17 Jgc Corp 多段式高流速気液接触装置
JPS59104345A (ja) * 1982-12-03 1984-06-16 Kuraray Yuka Kk 直接重合用に適したテレフタル酸の製造方法
DE4318893A1 (de) * 1993-06-07 1994-12-08 Bayer Ag Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat
JP3719448B2 (ja) * 1993-07-29 2005-11-24 三菱瓦斯化学株式会社 芳香族ジカルボン酸製造用酸化反応器
SI9500109A (en) * 1995-04-05 1996-10-31 Levec Janez Dipl Ing Prof Dr Apparatus and Process for Thermal Oxidative Treatment of Waste Waters
US5929274A (en) * 1995-06-07 1999-07-27 Hfm International, Inc. Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid
JPH09278709A (ja) * 1996-02-13 1997-10-28 Mitsubishi Chem Corp 芳香族カルボン酸の製造方法
US6084125A (en) * 1996-02-27 2000-07-04 Praxair Technology, Inc. Process for producing aliphatic acids using a reactor system having a shell and a tube reactor configuration to force circulation of reaction liquid
ID19133A (id) * 1996-12-12 1998-06-18 Praxair Technology Inc Pengisian oksigen langsung kedalam reaktor-reaktor ruang gelembung
GB9701251D0 (en) * 1997-01-22 1997-03-12 Bp Chem Int Ltd Process
DE19843573A1 (de) * 1998-09-23 2000-03-30 Degussa Blasensäule und deren Verwendung
AU2001232878A1 (en) * 2000-01-21 2001-07-31 Bp Corporation North America Inc. Production of high purity aromatic carboxylic acid by oxidation in benzoic acid and water solvent
AU2003293251A1 (en) * 2002-12-09 2004-06-30 Eastman Chemical Company Process for the oxidative purification of terephthalic acid
JP2006509044A (ja) * 2002-12-09 2006-03-16 イーストマン ケミカル カンパニー 粗製カルボン酸スラリーの精製方法
US7074954B2 (en) * 2002-12-09 2006-07-11 Eastman Chemical Company Process for the oxidative purification of terephthalic acid

Also Published As

Publication number Publication date
BRPI0514800B1 (pt) 2015-11-24
MX2007002565A (es) 2007-04-24
CN101023046B (zh) 2019-01-18
EP1791800B1 (en) 2017-11-01
WO2006028752A3 (en) 2006-06-01
KR101281347B1 (ko) 2013-07-02
KR20130003039A (ko) 2013-01-08
CN101023046A (zh) 2007-08-22
CN101766979A (zh) 2010-07-07
CN101766979B (zh) 2012-12-26
LT1791800T (lt) 2018-01-25
WO2006028752A2 (en) 2006-03-16
BRPI0514800A (pt) 2008-06-24
CA2576632A1 (en) 2006-03-16
JP2008511638A (ja) 2008-04-17
EP1791800A2 (en) 2007-06-06
KR20070048256A (ko) 2007-05-08
KR101363824B1 (ko) 2014-02-17
PL1791800T3 (pl) 2018-04-30
PT1791800T (pt) 2018-02-02

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