JP2008007759A5 - - Google Patents
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- Publication number
- JP2008007759A5 JP2008007759A5 JP2007141543A JP2007141543A JP2008007759A5 JP 2008007759 A5 JP2008007759 A5 JP 2008007759A5 JP 2007141543 A JP2007141543 A JP 2007141543A JP 2007141543 A JP2007141543 A JP 2007141543A JP 2008007759 A5 JP2008007759 A5 JP 2008007759A5
- Authority
- JP
- Japan
- Prior art keywords
- mmol
- added
- toluene
- hours
- block copolymer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 42
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 24
- 238000006243 chemical reaction Methods 0.000 description 15
- 238000000034 method Methods 0.000 description 15
- 229920001400 block copolymer Polymers 0.000 description 12
- 229920001477 hydrophilic polymer Polymers 0.000 description 12
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 12
- 229920001600 hydrophobic polymer Polymers 0.000 description 9
- 239000000203 mixture Substances 0.000 description 9
- 238000001914 filtration Methods 0.000 description 8
- 238000005406 washing Methods 0.000 description 8
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000012300 argon atmosphere Substances 0.000 description 6
- 238000010533 azeotropic distillation Methods 0.000 description 6
- 238000005342 ion exchange Methods 0.000 description 6
- 229910000027 potassium carbonate Inorganic materials 0.000 description 6
- PLVUIVUKKJTSDM-UHFFFAOYSA-N 1-fluoro-4-(4-fluorophenyl)sulfonylbenzene Chemical compound C1=CC(F)=CC=C1S(=O)(=O)C1=CC=C(F)C=C1 PLVUIVUKKJTSDM-UHFFFAOYSA-N 0.000 description 3
- 238000010521 absorption reaction Methods 0.000 description 3
- 238000005266 casting Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 239000005518 polymer electrolyte Substances 0.000 description 3
- VKDSBABHIXQFKH-UHFFFAOYSA-M potassium;4-hydroxy-3-sulfophenolate Chemical compound [K+].OC1=CC=C(O)C(S([O-])(=O)=O)=C1 VKDSBABHIXQFKH-UHFFFAOYSA-M 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- OTSCPDDAOASPMM-UHFFFAOYSA-N 4-(4-hydroxy-3-phenylphenyl)-2-phenylphenol Chemical group OC1=CC=C(C=2C=C(C(O)=CC=2)C=2C=CC=CC=2)C=C1C1=CC=CC=C1 OTSCPDDAOASPMM-UHFFFAOYSA-N 0.000 description 2
- KCIDZIIHRGYJAE-YGFYJFDDSA-L dipotassium;[(2r,3r,4s,5r,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl] phosphate Chemical compound [K+].[K+].OC[C@H]1O[C@H](OP([O-])([O-])=O)[C@H](O)[C@@H](O)[C@H]1O KCIDZIIHRGYJAE-YGFYJFDDSA-L 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 1
- MNZMMCVIXORAQL-UHFFFAOYSA-N naphthalene-2,6-diol Chemical compound C1=C(O)C=CC2=CC(O)=CC=C21 MNZMMCVIXORAQL-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2007141543A JP4930194B2 (ja) | 2006-05-31 | 2007-05-29 | ブロック共重合体及びその用途 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2006151279 | 2006-05-31 | ||
| JP2006151279 | 2006-05-31 | ||
| JP2007141543A JP4930194B2 (ja) | 2006-05-31 | 2007-05-29 | ブロック共重合体及びその用途 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008007759A JP2008007759A (ja) | 2008-01-17 |
| JP2008007759A5 true JP2008007759A5 (enExample) | 2010-05-20 |
| JP4930194B2 JP4930194B2 (ja) | 2012-05-16 |
Family
ID=39066240
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2007141543A Expired - Fee Related JP4930194B2 (ja) | 2006-05-31 | 2007-05-29 | ブロック共重合体及びその用途 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP4930194B2 (enExample) |
Families Citing this family (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US8138231B2 (en) * | 2007-10-29 | 2012-03-20 | Sumitomo Chemical Company, Limited | Polymer having oxycarbon group, and use thereof |
| JP2009235124A (ja) * | 2008-03-25 | 2009-10-15 | Sumitomo Chemical Co Ltd | イオン交換基含有ポリアリーレン樹脂の取得方法 |
| JP5018588B2 (ja) * | 2008-03-26 | 2012-09-05 | 東洋紡績株式会社 | プロトン酸基含有ブロックコポリマー、及びその製造方法、並びに高分子電解質膜 |
| EP2381522B1 (en) * | 2009-01-19 | 2017-09-13 | Toray Industries, Inc. | Process for producing polymeric electrolyte membrane |
| JP5407355B2 (ja) * | 2009-01-21 | 2014-02-05 | 東レ株式会社 | 電解質膜の製造方法 |
| JP5407063B2 (ja) * | 2009-01-19 | 2014-02-05 | 東レ株式会社 | 高分子電解質膜の製造方法 |
| JP4864107B2 (ja) * | 2009-02-17 | 2012-02-01 | 株式会社日立製作所 | ブロック共重合体並びにこれを用いた燃料電池用固体高分子電解質、燃料電池用固体高分子電解質膜、膜電極接合体及び燃料電池 |
| JP5672795B2 (ja) * | 2009-07-17 | 2015-02-18 | 東レ株式会社 | 高分子重合方法 |
| JP5338656B2 (ja) * | 2009-12-25 | 2013-11-13 | 東レ株式会社 | 高分子電解質膜の製造方法 |
| EP2752928B1 (en) * | 2011-08-29 | 2017-11-22 | Toray Industries, Inc. | Polymer electrolyte membrane, membrane electrode assembly using same, and solid polymer fuel cell |
| JP6048007B2 (ja) * | 2011-08-31 | 2016-12-21 | 東レ株式会社 | ブロック共重合体およびその製造方法、ならびにブロック共重合体を用いた高分子電解質材料、高分子電解質成型体および固体高分子型燃料電池 |
| KR101532886B1 (ko) * | 2014-12-02 | 2015-07-02 | 성균관대학교산학협력단 | 연료전지의 멤브레인 제조용 공중합체, 이의 제조 방법 및 연료전지용 멤브레인 |
| KR102440712B1 (ko) * | 2015-03-13 | 2022-09-07 | 도레이 카부시키가이샤 | 복합 고분자 전해질막, 그리고 그것을 사용한 촉매층 부착 전해질막, 막 전극 복합체 및 고체 고분자형 연료 전지 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004359925A (ja) * | 2003-04-07 | 2004-12-24 | Mitsui Chemicals Inc | プロトン伝導性ブロック共重合体およびプロトン伝導膜 |
| JP4375170B2 (ja) * | 2003-09-30 | 2009-12-02 | 住友化学株式会社 | ブロック共重合体及びその用途 |
| JP4424129B2 (ja) * | 2003-10-17 | 2010-03-03 | 住友化学株式会社 | ブロック共重合体及びその用途 |
| US20050136314A1 (en) * | 2003-12-17 | 2005-06-23 | Ballard Power Systems Inc. | Ion-exchange membrane for an electrochemical fuel cell |
| EP1788649B1 (en) * | 2004-07-23 | 2012-09-26 | Mitsui Chemicals, Inc. | Binder for fuel cell, composition for electrode formation, electrode, and fuel cell using the electrode |
| EP1883671A2 (en) * | 2005-05-27 | 2008-02-06 | Polyfuel, Inc. | End-capped ion-conductive polymers |
| CA2607966A1 (en) * | 2005-06-01 | 2006-12-07 | Polyfuel Inc. | Ion-conducting polymers containing pendant ion conducting groups |
| JP2008542505A (ja) * | 2005-06-01 | 2008-11-27 | ポリフューエル・インコーポレイテッド | イオン伝導性架橋コポリマー |
-
2007
- 2007-05-29 JP JP2007141543A patent/JP4930194B2/ja not_active Expired - Fee Related
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