JP2006511657A - 高固形分装填条件下での制御された構造の材料の連続製造方法 - Google Patents

高固形分装填条件下での制御された構造の材料の連続製造方法 Download PDF

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Publication number
JP2006511657A
JP2006511657A JP2004564999A JP2004564999A JP2006511657A JP 2006511657 A JP2006511657 A JP 2006511657A JP 2004564999 A JP2004564999 A JP 2004564999A JP 2004564999 A JP2004564999 A JP 2004564999A JP 2006511657 A JP2006511657 A JP 2006511657A
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Prior art keywords
monomer
reactor
reaction mixture
temperature
methacrylate
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JP2004564999A
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Japanese (ja)
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JP2006511657A5 (enExample
Inventor
エム. ネルソン,ジェイムズ
イー. マークス,ライアン
ジェイ. アネン,マイケル
ディー. ファンスラー,デュアン
エー. カバナー,モーリーン
エヌ. ガッダム,バブ
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3M Innovative Properties Co
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3M Innovative Properties Co
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Publication of JP2006511657A publication Critical patent/JP2006511657A/ja
Publication of JP2006511657A5 publication Critical patent/JP2006511657A5/ja
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/01Processes of polymerisation characterised by special features of the polymerisation apparatus used
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/02Polymerisation in bulk
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/1812Tubular reactors
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00Processes of polymerisation
    • C08F2/04Polymerisation in solution
    • C08F2/06Organic solvent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081Tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00164Controlling or regulating processes controlling the flow
    • B01J2219/00166Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polymerisation Methods In General (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
JP2004564999A 2002-12-19 2003-11-17 高固形分装填条件下での制御された構造の材料の連続製造方法 Pending JP2006511657A (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US10/324,242 US6716935B1 (en) 2002-12-19 2002-12-19 Continuous process for the production of controlled architecture materials under high solids loading conditions
PCT/US2003/036479 WO2004060927A1 (en) 2002-12-19 2003-11-17 Continuous process for the production of controlled architecture materials under high solids loading conditions

Publications (2)

Publication Number Publication Date
JP2006511657A true JP2006511657A (ja) 2006-04-06
JP2006511657A5 JP2006511657A5 (enExample) 2006-12-14

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JP2004564999A Pending JP2006511657A (ja) 2002-12-19 2003-11-17 高固形分装填条件下での制御された構造の材料の連続製造方法

Country Status (8)

Country Link
US (1) US6716935B1 (enExample)
EP (1) EP1572750B1 (enExample)
JP (1) JP2006511657A (enExample)
KR (1) KR20050085763A (enExample)
AU (1) AU2003291543A1 (enExample)
BR (1) BR0317115B1 (enExample)
MX (1) MXPA05006329A (enExample)
WO (1) WO2004060927A1 (enExample)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012035769A1 (ja) * 2010-09-17 2012-03-22 国立大学法人京都大学 リビングラジカル重合法
JP2013543021A (ja) * 2010-09-22 2013-11-28 コモンウェルス サイエンティフィック アンドインダストリアル リサーチ オーガナイゼーション 連続フロー重合処理
JP2016196442A (ja) * 2015-04-06 2016-11-24 株式会社メニコン 重合性不飽和モノマーの精製方法及び精製装置
JPWO2015008736A1 (ja) * 2013-07-17 2017-03-02 旭化成株式会社 重合体の製造方法
JP2017066276A (ja) * 2015-09-30 2017-04-06 富士フイルム株式会社 重合体の製造方法、及び重合体を製造するフロー式反応システム

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US7157283B2 (en) * 2002-08-02 2007-01-02 3M Innovative Properties Company Continuous process for the production of combinatorial libraries of modified materials
US7632916B2 (en) * 2002-08-02 2009-12-15 3M Innovative Properties Company Process to modify polymeric materials and resulting compositions
US6969491B1 (en) 2004-09-01 2005-11-29 3M Innovative Properties Company Stirred tube reactor and method of using the same
US7691932B2 (en) * 2004-09-27 2010-04-06 3M Innovative Properties Company Method of making a composition and nanocomposites therefrom
US7495051B2 (en) * 2004-09-27 2009-02-24 3M Innovative Properties Company Nanocomposite and method of making the same
US7329702B2 (en) * 2004-09-27 2008-02-12 3M Innovative Properties Company Composition and method of making the same
US8193270B2 (en) * 2004-12-14 2012-06-05 3M Innovative Properties Company Method of making composites and nanocomposites
JP2008531789A (ja) * 2005-02-23 2008-08-14 スリーエム イノベイティブ プロパティズ カンパニー ポリマーブレンド
JP4865279B2 (ja) * 2005-09-06 2012-02-01 日本曹達株式会社 アニオン重合による重合体の製造方法
US20070135577A1 (en) * 2005-12-09 2007-06-14 Shefelbine Terri A Intermediate elastomer compositions
US20080058482A1 (en) * 2006-08-29 2008-03-06 3M Innovative Properties Company Continuous process polymerization of (meth)acrylate copolymers
JP5277314B2 (ja) * 2009-06-19 2013-08-28 東洋エンジニアリング株式会社 ポリ乳酸の製造方法
US8765888B2 (en) 2009-06-30 2014-07-01 Bridgestone Corporation Polymers functionalized with hydroxyl group-containing diphenylethylene
BR112012030344B1 (pt) 2010-05-31 2020-10-27 Bridgestone Corporation metilestireno contendo grupo hidroxila e polímeros incorporando o mesmo
WO2020243234A1 (en) * 2019-05-29 2020-12-03 Saudi Arabian Oil Company Flow synthesis of polymer nanoparticles
ES2983867B2 (es) * 2024-04-15 2025-03-27 Innventik S L Dispositivo compacto de Pre-polimerización tipo flujo tapón Plug Flow para convertir procesos de polimerización por lotes, discontinuos o batch, a continuos

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04218512A (ja) * 1990-12-19 1992-08-10 Nippon Steel Chem Co Ltd スチレン系樹脂の製造方法
JPH07206906A (ja) * 1994-01-07 1995-08-08 Mitsubishi Gas Chem Co Inc 耐熱分解性を有するメタクリル樹脂及びその製造方法
JPH08253507A (ja) * 1995-03-16 1996-10-01 Mitsubishi Gas Chem Co Inc メタクリル樹脂の製造方法
JPH093102A (ja) * 1995-06-15 1997-01-07 Elf Atochem Sa (メタ)アクリルモノマーの連続アニオン重合方法
JPH10147620A (ja) * 1996-11-20 1998-06-02 Kao Corp 共重合体の連続製造方法
JP2002128806A (ja) * 2000-05-08 2002-05-09 Asahi Kasei Corp 低分子成分の少ないスチレン系樹脂の製造方法
WO2002081079A2 (en) * 2001-04-02 2002-10-17 3M Innovative Properties Company A continuous process for the production of combinatorial libraries of materials

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5952882B2 (ja) 1979-11-02 1984-12-21 株式会社日立製作所 スチレン系樹脂の連続塊状重合方法
IT1230085B (it) 1989-05-24 1991-10-05 Montedipe Spa Processo per la produzione in massa e in continuo di (co) polimeri vinil aromatici antiurto.
IT1274361B (it) * 1995-02-16 1997-07-17 Enichem Spa Procedimento per la preparazione di copolimeri vinilaromatici rinforzati con gomma
US5644007A (en) 1996-04-26 1997-07-01 Minnesota Mining And Manufacturing Company Continuous process for the production of poly(1-alkenes)
US5814278A (en) 1996-04-26 1998-09-29 Minnesota Mining And Manufacturing Company Shrouded reaction vessel
US6013735A (en) 1998-02-13 2000-01-11 Ethyl Corporation Process for the preparation of acrylate and methacrylate polymers
US6448353B1 (en) 2000-02-08 2002-09-10 3M Innovative Properties Company Continuous process for the production of controlled architecture materials

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04218512A (ja) * 1990-12-19 1992-08-10 Nippon Steel Chem Co Ltd スチレン系樹脂の製造方法
JPH07206906A (ja) * 1994-01-07 1995-08-08 Mitsubishi Gas Chem Co Inc 耐熱分解性を有するメタクリル樹脂及びその製造方法
JPH08253507A (ja) * 1995-03-16 1996-10-01 Mitsubishi Gas Chem Co Inc メタクリル樹脂の製造方法
JPH093102A (ja) * 1995-06-15 1997-01-07 Elf Atochem Sa (メタ)アクリルモノマーの連続アニオン重合方法
JPH10147620A (ja) * 1996-11-20 1998-06-02 Kao Corp 共重合体の連続製造方法
JP2002128806A (ja) * 2000-05-08 2002-05-09 Asahi Kasei Corp 低分子成分の少ないスチレン系樹脂の製造方法
WO2002081079A2 (en) * 2001-04-02 2002-10-17 3M Innovative Properties Company A continuous process for the production of combinatorial libraries of materials

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012035769A1 (ja) * 2010-09-17 2012-03-22 国立大学法人京都大学 リビングラジカル重合法
JP2012062449A (ja) * 2010-09-17 2012-03-29 Kyoto Univ リビングラジカル重合法
US8642711B2 (en) 2010-09-17 2014-02-04 Kyoto University Living radical polymerization method
JP2013543021A (ja) * 2010-09-22 2013-11-28 コモンウェルス サイエンティフィック アンドインダストリアル リサーチ オーガナイゼーション 連続フロー重合処理
JPWO2015008736A1 (ja) * 2013-07-17 2017-03-02 旭化成株式会社 重合体の製造方法
JP2016196442A (ja) * 2015-04-06 2016-11-24 株式会社メニコン 重合性不飽和モノマーの精製方法及び精製装置
JP2017066276A (ja) * 2015-09-30 2017-04-06 富士フイルム株式会社 重合体の製造方法、及び重合体を製造するフロー式反応システム

Also Published As

Publication number Publication date
BR0317115A (pt) 2005-10-25
EP1572750B1 (en) 2013-06-19
EP1572750A1 (en) 2005-09-14
BR0317115B1 (pt) 2014-01-28
US6716935B1 (en) 2004-04-06
AU2003291543A1 (en) 2004-07-29
WO2004060927A1 (en) 2004-07-22
MXPA05006329A (es) 2005-08-26
KR20050085763A (ko) 2005-08-29

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