JP2001520615A - 単層壁カーボンナノチューブの束 - Google Patents
単層壁カーボンナノチューブの束Info
- Publication number
- JP2001520615A JP2001520615A JP51135997A JP51135997A JP2001520615A JP 2001520615 A JP2001520615 A JP 2001520615A JP 51135997 A JP51135997 A JP 51135997A JP 51135997 A JP51135997 A JP 51135997A JP 2001520615 A JP2001520615 A JP 2001520615A
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- Prior art keywords
- carbon
- carbon nanotubes
- walled carbon
- group viii
- rope
- Prior art date
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
- C01B32/15—Nano-sized carbon materials
- C01B32/158—Carbon nanotubes
- C01B32/16—Preparation
- C01B32/162—Preparation characterised by catalysts
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y15/00—Nanotechnology for interacting, sensing or actuating, e.g. quantum dots as markers in protein assays or molecular motors
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2202/00—Structure or properties of carbon nanotubes
- C01B2202/02—Single-walled nanotubes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
- Y02P20/133—Renewable energy sources, e.g. sunlight
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S977/00—Nanotechnology
- Y10S977/84—Manufacture, treatment, or detection of nanostructure
- Y10S977/842—Manufacture, treatment, or detection of nanostructure for carbon nanotubes or fullerenes
- Y10S977/844—Growth by vaporization or dissociation of carbon source using a high-energy heat source, e.g. electric arc, laser, plasma, e-beam
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2918—Rod, strand, filament or fiber including free carbon or carbide or therewith [not as steel]
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Nanotechnology (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- Composite Materials (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Manufacturing & Machinery (AREA)
- Carbon And Carbon Compounds (AREA)
- Ropes Or Cables (AREA)
- Materials For Medical Uses (AREA)
- Adornments (AREA)
Abstract
Description
Claims (1)
- 【特許請求の範囲】 1. a) 第1のレーザーパルスによって炭素および1種以上のVIII族遷 移金属の混合物を蒸発させることによって炭素および1種以上のVIII族遷移 金属を含む蒸気を作製し、 b) その後にその蒸気を凝縮させて、活性末端を有する単一壁炭素ナノチ ューブを形成し、 c) その後に単一壁炭素ナノチューブの活性末端を焼なまし帯域内に維持 しながら、単一壁炭素ナノチューブの活性末端に炭素蒸気を供給することを含む 単一壁炭素ナノチューブの製造方法。 2. 1種以上のVIII族遷移金属がコバルト、ルテニウム、ニッケルおよび 白金からなるグループから選択される請求項1による方法。 3. 焼なまし帯域が1000℃ないし1400℃の温度および100ないし800Torrの圧力 に維持されている請求項3による方法。 4. 焼なまし帯域の雰囲気が炭素とアルゴン、ネオン、ヘリウム、一酸化炭素 およびこれらの混合物のグループから選択されたガスとを含む請求項3による方 法。 5. 焼なまし帯域の雰囲気が本質的に炭素と鉄、コバルト、ルテニウム、ニッ ケル、白金からなるグループから選択された1種以上の遷移金属およびアルゴン 、ネオン、ヘリウム、一酸化炭素およびこれらの混合物のグループから選択され たガスからなる請求項4による方法。 6. 炭素および1種以上のVIII族遷移金属を含む蒸気を作製する段階がさ らに第1のパルスの完了の後におよび第1のレーザーパルスによって作製された 蒸気が消え失せ、焦点を合わせる前に到着するように時間設定されている第2の レーザーパルスを含み、その結果第2のレーザーパルスからのエネルギーが蒸気 に吸収される請求項1による方法。 7. 炭素と1種以上のVIII族遷移金属をレーザーで蒸発させ、そのように して生成した蒸気を焼なまし帯域を通じて移動させ、その蒸気を凝縮させ、単一 壁炭素ナノチューブを蒸気から凝縮する素材から回収することを含 む単一壁炭素ナノチューブの製造方法。 8. 1種以上のVIII族遷移金属が鉄、コバルト、ルテニウム、ニッケルお よび白金からなるグループから選択される請求項7による方法。 9. 蒸気を作製するためにレーザービームで叩かれる標的を成すように炭素お よび1種以上のVIII族遷移金属が混合される請求項8による方法。 10. 炭素標的が焼きなまし帯域が焼なまし帯域に維持されている請求項9に よる方法。 11. 焼きなまし帯域が1000℃ないし1400℃の温度に維持されており、焼なま し帯域が100ないし800Torrの圧力に維持されており、その焼なまし帯域の雰囲気 が本質的に炭素、鉄、コバルト、ルテニウム、ニッケルおよび白金から成るグル ープから選択された1種以上のVIII族遷移金属およびアルゴン、ネオン、ヘ リウム、一酸化炭素およびこれらの混合物からなるグループから選択されたガス からなる請求項10による方法。 12. a)炭素をふくむ標的から素材を削摩する第1のレーザーパルスを使用 することおよびその後に第1のパルスの完了の後におよび第1のレーザーパルス によって削摩された素材が消え失せ、焦点を合わせる前に標的に到着するように 時間設定されている第2のレザーパルスを使用することによって、炭素を含む蒸 気を作製し、その結果第2のレーザーパルスからのエネルギーが蒸気を発生する 第1のレーザーパルスによって標的から削摩された素材によって吸収され、 b) 炭素ナノチューブを生成する蒸気を凝縮させることを含む炭素ナノチュー ブの製造方法。 13. 第2のレーザーパルスが第1のレーザービームの終了から約20ナノ秒( ns)から約60nsの遅延時間内で標的に到着する請求項12による方法。 14. 標的がさらに1種以上のVIII族遷移金属を含む請求項13による方法 。 15. 1種以上のVIII族遷移金属が鉄、コバルト、ルテニウム、ニッケル および白金からなるグループから選択される請求項14による方法。 16. 蒸気が凝縮し、活性末端を有する単一壁炭素ナノチューブを形成する請 求項15による方法。 17. 焼なまし帯域中で単一壁炭素ナノチューブの活性末端を維持することお よび単一壁炭素ナノチューブの活性末端に炭素蒸気を供給することをさらに含む 請求項16による方法。 18. 標的が鉄、コバルト、ルテニウム、ニッケルおよび白金からなるグルー プから選択される1種以上のVIII族遷移金属を0.1ないし10原子パーセント 含む請求項17による方法。 19. 焼なまし帯域が約1000℃ないし約1400℃の温度に維持されており、焼な まし帯域の圧力が約100ないし約800Torrの圧力に維持されている請求項18による 方法。 20. 焼なまし帯域が炭素およびアルゴン、ネオン、ヘリウム、一酸化炭素お よびこれらの混合物のグループから選択されるガスを含む雰囲気の中に維持され ている請求項19による方法。 21. 遅延時間が約40nsから約50nsまでである請求項19による方法。 22. 請求項12、13、14、15、19または21のいずれかの方法によって製造され た単一壁炭素ナノチューブ製造物。 23. 10%以上が(10,10)単一壁炭素ナノチューブである50ないし5000本の 単一壁炭素ナノチューブを有する単一壁炭素ナノチューブのロープ。 24. 50%以上が(10,10)単一壁炭素ナノチューブである請求項23による単 一壁炭素ナノチューブのロープ。 25. 90%以上が(10,10)単一壁炭素ナノチューブである請求項24による単 一壁炭素ナノチューブのロープ。 26. ロープが100ないし500本の単一壁炭素ナノチューブを含む請求項25によ る単一壁炭素ナノチューブのロープ。 27. ロープ中のすべての単一壁炭素ナノチューブの平均直径が13.8ű0.3 Åである請求項26による単一壁炭素ナノチューブのロープ。 28. ロープ中のすべての単一壁炭素ナノチューブの平均直径が13.8ű0.2 Åである請求項26による単一壁炭素ナノチューブのロープ。 29. 2−D三角格子定数が17Åである請求項28によるロープ。 30. 約100ないし500本の単一壁炭素ナノチューブの内で50%以上が安楽椅子 型の単一壁炭素ナノチューブを含む請求項23による単一壁炭素ナノチューブのロ ープ。 31. 単一壁炭素ナノチューブの75%以上が安楽椅子型である請求項30による 単一壁炭素ナノチューブのロープ。 32. 単一壁炭素ナノチューブの90%以上が安楽椅子型である請求項31による 単一壁炭素ナノチューブのロープ。 33. 単一壁炭素ナノチューブを形成する炭素を蒸発させるために太陽エネル ギーを使ってロープが製造される請求項30による単一壁炭素ナノチューブのロー プ。 34. 単一壁炭素ナノチューブのロープのフェルト。
Applications Claiming Priority (7)
Application Number | Priority Date | Filing Date | Title |
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US344995P | 1995-09-08 | 1995-09-08 | |
US60/003,449 | 1995-09-08 | ||
US1631396P | 1996-05-08 | 1996-05-08 | |
US60/016,313 | 1996-05-08 | ||
US08/687,665 | 1996-07-26 | ||
US08/687,665 US6183714B1 (en) | 1995-09-08 | 1996-07-26 | Method of making ropes of single-wall carbon nanotubes |
PCT/US1996/014188 WO1997009272A1 (en) | 1995-09-08 | 1996-09-06 | Ropes of single-wall carbon nanotubes |
Publications (3)
Publication Number | Publication Date |
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JP2001520615A true JP2001520615A (ja) | 2001-10-30 |
JP2001520615A5 JP2001520615A5 (ja) | 2004-09-24 |
JP3958792B2 JP3958792B2 (ja) | 2007-08-15 |
Family
ID=27357405
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP51135997A Expired - Fee Related JP3958792B2 (ja) | 1995-09-08 | 1996-09-06 | カーボンナノチューブを含有する組成物の作製方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US6183714B1 (ja) |
EP (1) | EP0854839B1 (ja) |
JP (1) | JP3958792B2 (ja) |
AT (1) | ATE216681T1 (ja) |
DE (1) | DE69620900T2 (ja) |
WO (1) | WO1997009272A1 (ja) |
Cited By (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2004517789A (ja) * | 1998-11-03 | 2004-06-17 | ウィリアム・マーシュ・ライス・ユニバーシティ | 高温一酸化炭素気体からの単層カーボンナノチューブの結晶核形成および成長 |
JP2004331452A (ja) * | 2003-05-07 | 2004-11-25 | Hitachi Chem Co Ltd | カーボンナノファイバ及びその製造方法 |
JP2008093494A (ja) * | 2006-10-05 | 2008-04-24 | Mitsubishi Heavy Ind Ltd | ナノカーボン材料製造用触媒及びナノカーボン材料製造用触媒の製造方法 |
WO2008050794A1 (en) * | 2006-10-25 | 2008-05-02 | Kuraray Co., Ltd. | Transparent conductive film, transparent electrode substrate and method for producing liquid crystal alignment film by using the same, and carbon nanotube and method for producing the same |
JP2008108575A (ja) * | 2006-10-25 | 2008-05-08 | Kuraray Co Ltd | 透明導電膜、透明電極基板およびこれを用いた液晶配向膜の製造方法 |
JP2008214170A (ja) * | 2007-03-07 | 2008-09-18 | Yamaguchi Univ | パルスレーザーによる物質生成方法 |
JP2010001161A (ja) * | 2008-06-18 | 2010-01-07 | National Institute Of Advanced Industrial & Technology | アームチェア型単層カーボンナノチューブによる金属型炭素素材 |
EP2287373A1 (en) | 2003-02-06 | 2011-02-23 | Mitsubishi Heavy Industries, Ltd. | Producing method of carbon nanofibers |
JP2011255382A (ja) * | 2011-09-28 | 2011-12-22 | Mitsubishi Heavy Ind Ltd | ナノカーボン材料製造用触媒の製造方法及びナノカーボン材料の製造方法 |
US8236118B2 (en) | 2009-08-07 | 2012-08-07 | Guardian Industries Corp. | Debonding and transfer techniques for hetero-epitaxially grown graphene, and products including the same |
JP2013502361A (ja) * | 2009-08-21 | 2013-01-24 | バイエル・マテリアルサイエンス・アクチェンゲゼルシャフト | カーボンナノチューブ凝集体 |
US8460747B2 (en) | 2010-03-04 | 2013-06-11 | Guardian Industries Corp. | Large-area transparent conductive coatings including alloyed carbon nanotubes and nanowire composites, and methods of making the same |
US8518472B2 (en) | 2010-03-04 | 2013-08-27 | Guardian Industries Corp. | Large-area transparent conductive coatings including doped carbon nanotubes and nanowire composites, and methods of making the same |
US8604332B2 (en) | 2010-03-04 | 2013-12-10 | Guardian Industries Corp. | Electronic devices including transparent conductive coatings including carbon nanotubes and nanowire composites, and methods of making the same |
US8771629B2 (en) | 2008-05-30 | 2014-07-08 | Mitsubishi Heavy Industries, Ltd. | Nano-carbon material production apparatus and method |
JP2015509152A (ja) * | 2012-01-20 | 2015-03-26 | フリー フォーム ファイバーズ リミテッド ライアビリティ カンパニー | 高強度セラミック繊維および製造方法 |
US9458018B2 (en) | 2012-02-29 | 2016-10-04 | Mitsubishi Heavy Industries, Ltd. | Apparatus and method for producing nanocarbon material |
US10145005B2 (en) | 2015-08-19 | 2018-12-04 | Guardian Glass, LLC | Techniques for low temperature direct graphene growth on glass |
US10164135B2 (en) | 2009-08-07 | 2018-12-25 | Guardian Glass, LLC | Electronic device including graphene-based layer(s), and/or method or making the same |
US10167572B2 (en) | 2009-08-07 | 2019-01-01 | Guardian Glass, LLC | Large area deposition of graphene via hetero-epitaxial growth, and products including the same |
US10431354B2 (en) | 2013-03-15 | 2019-10-01 | Guardian Glass, LLC | Methods for direct production of graphene on dielectric substrates, and associated articles/devices |
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US6683783B1 (en) * | 1997-03-07 | 2004-01-27 | William Marsh Rice University | Carbon fibers formed from single-wall carbon nanotubes |
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US6280697B1 (en) * | 1999-03-01 | 2001-08-28 | The University Of North Carolina-Chapel Hill | Nanotube-based high energy material and method |
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US7816709B2 (en) | 1999-06-02 | 2010-10-19 | The Board Of Regents Of The University Of Oklahoma | Single-walled carbon nanotube-ceramic composites and methods of use |
US6333016B1 (en) | 1999-06-02 | 2001-12-25 | The Board Of Regents Of The University Of Oklahoma | Method of producing carbon nanotubes |
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JP2001039706A (ja) * | 1999-07-26 | 2001-02-13 | Futaba Corp | 水素吸臓材料の製造方法 |
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Also Published As
Publication number | Publication date |
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ATE216681T1 (de) | 2002-05-15 |
EP0854839B1 (en) | 2002-04-24 |
JP3958792B2 (ja) | 2007-08-15 |
US6183714B1 (en) | 2001-02-06 |
WO1997009272A1 (en) | 1997-03-13 |
DE69620900T2 (de) | 2003-07-24 |
DE69620900D1 (de) | 2002-05-29 |
EP0854839A1 (en) | 1998-07-29 |
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