IT1027332B - Procedimento per la sintesi di derivati idrazinici - Google Patents
Procedimento per la sintesi di derivati idraziniciInfo
- Publication number
- IT1027332B IT1027332B IT67128/75A IT6712875A IT1027332B IT 1027332 B IT1027332 B IT 1027332B IT 67128/75 A IT67128/75 A IT 67128/75A IT 6712875 A IT6712875 A IT 6712875A IT 1027332 B IT1027332 B IT 1027332B
- Authority
- IT
- Italy
- Prior art keywords
- hydrogen
- atom
- nitrogen
- azines
- synthesis
- Prior art date
Links
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical class NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 title 1
- 230000015572 biosynthetic process Effects 0.000 title 1
- 238000000034 method Methods 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 abstract 4
- 125000004429 atom Chemical group 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 abstract 2
- 150000001299 aldehydes Chemical class 0.000 abstract 2
- 239000003426 co-catalyst Substances 0.000 abstract 2
- 150000002576 ketones Chemical class 0.000 abstract 2
- 229910052757 nitrogen Inorganic materials 0.000 abstract 2
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 abstract 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-M Bicarbonate Chemical class OC([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-M 0.000 abstract 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical class OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 abstract 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 abstract 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 abstract 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 150000001408 amides Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- 229910052787 antimony Inorganic materials 0.000 abstract 1
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 abstract 1
- 229910052785 arsenic Inorganic materials 0.000 abstract 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 abstract 1
- 150000002429 hydrazines Chemical class 0.000 abstract 1
- 150000007857 hydrazones Chemical class 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 abstract 1
- 230000007062 hydrolysis Effects 0.000 abstract 1
- 238000006460 hydrolysis reaction Methods 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 150000003014 phosphoric acid esters Chemical class 0.000 abstract 1
- 229910052698 phosphorus Inorganic materials 0.000 abstract 1
- 239000011574 phosphorus Substances 0.000 abstract 1
- 238000004064 recycling Methods 0.000 abstract 1
- 229910052711 selenium Inorganic materials 0.000 abstract 1
- 239000011669 selenium Substances 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- 229910052717 sulfur Inorganic materials 0.000 abstract 1
- 239000011593 sulfur Substances 0.000 abstract 1
- 229910052714 tellurium Inorganic materials 0.000 abstract 1
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/72—Hydrazones
- C07C251/88—Hydrazones having also the other nitrogen atom doubly-bound to a carbon atom, e.g. azines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/16—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of hydrazones
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR7404247A FR2260569B1 (cg-RX-API-DMAC7.html) | 1974-02-08 | 1974-02-08 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| IT1027332B true IT1027332B (it) | 1978-11-20 |
Family
ID=9134662
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| IT67128/75A IT1027332B (it) | 1974-02-08 | 1975-01-21 | Procedimento per la sintesi di derivati idrazinici |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US3972878A (cg-RX-API-DMAC7.html) |
| JP (1) | JPS5343922B2 (cg-RX-API-DMAC7.html) |
| AT (1) | AT339873B (cg-RX-API-DMAC7.html) |
| BE (1) | BE825240A (cg-RX-API-DMAC7.html) |
| CA (1) | CA1040203A (cg-RX-API-DMAC7.html) |
| CH (1) | CH626601A5 (cg-RX-API-DMAC7.html) |
| DE (1) | DE2504924C3 (cg-RX-API-DMAC7.html) |
| ES (1) | ES434559A1 (cg-RX-API-DMAC7.html) |
| FR (1) | FR2260569B1 (cg-RX-API-DMAC7.html) |
| GB (1) | GB1489132A (cg-RX-API-DMAC7.html) |
| IT (1) | IT1027332B (cg-RX-API-DMAC7.html) |
| NL (1) | NL180101C (cg-RX-API-DMAC7.html) |
Families Citing this family (41)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2324618A1 (fr) * | 1975-09-17 | 1977-04-15 | Ugine Kuhlmann | Nouveau procede de preparation d'azines |
| GB2021560B (en) * | 1978-04-13 | 1982-09-08 | Showa Denko Kk | Process for producing ketazines |
| JPS5810547A (ja) * | 1981-07-09 | 1983-01-21 | Mitsubishi Gas Chem Co Inc | ケタジンの製造方法 |
| FR2571711A1 (fr) * | 1984-10-16 | 1986-04-18 | Atochem | Procede de fabrication d'hydrate d'hydrazine |
| DE3905265A1 (de) * | 1989-02-21 | 1990-08-23 | Krumme Hermann Josef | Verfahren zur veredelung von guelle |
| FR2647444B1 (cg-RX-API-DMAC7.html) * | 1989-05-24 | 1991-07-26 | Atochem | |
| ES2062674T5 (es) * | 1990-11-23 | 2002-04-16 | Atofina | Procedimiento de sintesis de azinas. |
| US6642268B2 (en) | 1994-09-13 | 2003-11-04 | G.D. Searle & Co. | Combination therapy employing ileal bile acid transport inhibiting benzothipines and HMG Co-A reductase inhibitors |
| US6268392B1 (en) | 1994-09-13 | 2001-07-31 | G. D. Searle & Co. | Combination therapy employing ileal bile acid transport inhibiting benzothiepines and HMG Co-A reductase inhibitors |
| US6262277B1 (en) * | 1994-09-13 | 2001-07-17 | G.D. Searle And Company | Intermediates and processes for the preparation of benzothiepines having activity as inhibitors of ileal bile acid transport and taurocholate uptake |
| JP3962872B2 (ja) * | 1995-08-14 | 2007-08-22 | 三菱瓦斯化学株式会社 | ケタジンの合成方法 |
| CN1053656C (zh) * | 1995-10-27 | 2000-06-21 | 化学工业部西南化工研究院 | 氨双氧水液相催化氧化法合成水合肼的方法 |
| DK0973791T3 (da) * | 1995-12-11 | 2007-09-17 | Searle Llc | Fremgangsmåde til fremstilling af en epoxyforbindelse |
| AU733559B2 (en) | 1996-12-11 | 2001-05-17 | G.D. Searle & Co. | Processes for preparation of 9,11-epoxy steroids and intermediates useful therein |
| US6887991B1 (en) * | 1996-12-11 | 2005-05-03 | G. D. Searle & Company | Processes for preparation of 9, 11-epoxy steroids and intermediates useful therein |
| CZ20012344A3 (cs) * | 1998-12-23 | 2002-01-16 | G. D. Searle Llc | Kombinace pro kardiovaskulární indikace |
| US6489366B1 (en) * | 1998-12-23 | 2002-12-03 | G. D. Searle, Llc | Combinations of cholesteryl ester transfer protein inhibitors and nicotinic acid derivatives for cardiovascular indications |
| EP1340509A1 (en) * | 1998-12-23 | 2003-09-03 | G.D. Searle LLC. | Combinations of cholesteryl ester transfer protein inhibitors and fibric acid derivatives for cardiovascular indications |
| MXPA01006470A (es) * | 1998-12-23 | 2003-06-06 | Searle Llc | Combinaciones de inhibidores de transporte de acido biliar ileal y agentes de secuentro de acido biliar para indicaciones cardiovasculares. |
| EP1340510A1 (en) | 1998-12-23 | 2003-09-03 | G.D. Searle LLC. | Combinations of cholesteryl ester transfer protein inhibitors and bile acid sequestering agents for cardiovascular indications |
| US6462091B1 (en) | 1998-12-23 | 2002-10-08 | G.D. Searle & Co. | Combinations of cholesteryl ester transfer protein inhibitors and HMG coA reductase inhibitors for cardiovascular indications |
| ES2200587T3 (es) * | 1998-12-23 | 2004-03-01 | G.D. Searle Llc | Combinaciones de inhibidors del transporte de acidos biliares del ileon e inhibidores de la proteina de transferencia de colesteril ester para indicaciones cardiovasculares. |
| DK1140189T3 (da) | 1998-12-23 | 2003-09-15 | Searle Llc | Kombinationer af ileal galdesyre-transportinhibitorer og fibrinsyrederivater til cardiovaskulære indikationer |
| US6586434B2 (en) | 2000-03-10 | 2003-07-01 | G.D. Searle, Llc | Method for the preparation of tetrahydrobenzothiepines |
| US20020061888A1 (en) * | 2000-03-10 | 2002-05-23 | Keller Bradley T. | Combination therapy for the prophylaxis and treatment of hyperlipidemic conditions and disorders |
| US20040077625A1 (en) * | 2001-07-25 | 2004-04-22 | Tremont Samuel J. | Novel 1,4-benzothiazepine and 1,5-benzothiazepine compounds as inhibitors of apical sodium codependent bile acid transport abd taurocholate uptake |
| JP2005518347A (ja) * | 2001-11-02 | 2005-06-23 | ジー．ディー． サール エルエルシー | 頂端ナトリウム共依存性胆汁酸輸送（ａｓｂｔ）およびタウロコール酸塩取り込みの阻害剤としての新規一および二フッ化ベンゾチエピン化合物 |
| US6852753B2 (en) | 2002-01-17 | 2005-02-08 | Pharmacia Corporation | Alkyl/aryl hydroxy or keto thiepine compounds as inhibitors of apical sodium co-dependent bile acid transport (ASBT) and taurocholate uptake |
| US7235655B2 (en) * | 2002-03-22 | 2007-06-26 | Pharmacia & Upjohn Company | Processes to prepare eplerenone |
| MXPA04009178A (es) * | 2002-03-22 | 2004-11-26 | Upjohn Co | Proceso para preparar eplerenona. |
| US7932316B2 (en) * | 2006-12-30 | 2011-04-26 | Bridgestone Corporation | Processable rubber composition |
| CN102295583A (zh) * | 2011-06-25 | 2011-12-28 | 杭州海虹精细化工有限公司 | 一种利用酮连氮制备联二脲的新方法 |
| US11225413B2 (en) | 2016-10-03 | 2022-01-18 | Council Of Scientific & Industrial Research | Process for production of hydrazine hydrate |
| CN108569681A (zh) * | 2018-05-31 | 2018-09-25 | 邹西红 | 一种过氧化物再生合成水合肼的方法 |
| CN108586285A (zh) * | 2018-05-31 | 2018-09-28 | 邹西红 | 一种酮连氮的制备方法 |
| CN108793105A (zh) * | 2018-05-31 | 2018-11-13 | 邹西红 | 一种中间原料重复再生法合成水合肼工艺 |
| FR3096049B1 (fr) | 2019-05-16 | 2021-12-17 | Arkema France | Procede ameliore de preparation d'hydrate d'hydrazine avec recyclage pyrazoline |
| FR3096048B1 (fr) | 2019-05-16 | 2021-04-30 | Arkema France | Procede ameliore de preparation d'hydrate d'hydrazine avec recyclage oxime |
| FR3130815B1 (fr) | 2021-12-21 | 2025-02-28 | Arkema France | Procede de preparation d'hydrate d'hydrazine en presence d’un agent anti-mousse |
| FR3137087A1 (fr) | 2022-06-24 | 2023-12-29 | Arkema France | Procede de preparation d'hydrate d'hydrazine utilisant une colonne d’absorption |
| FR3137086B1 (fr) | 2022-06-24 | 2025-05-23 | Arkema France | Procede de preparation d'hydrate d'hydrazine utilisant des reacteurs en cascade |
-
1974
- 1974-02-08 FR FR7404247A patent/FR2260569B1/fr not_active Expired
-
1975
- 1975-01-21 IT IT67128/75A patent/IT1027332B/it active
- 1975-01-29 AT AT65675A patent/AT339873B/de not_active IP Right Cessation
- 1975-01-29 CA CA218,888A patent/CA1040203A/fr not_active Expired
- 1975-02-03 GB GB4570/75A patent/GB1489132A/en not_active Expired
- 1975-02-06 DE DE2504924A patent/DE2504924C3/de not_active Expired
- 1975-02-06 BE BE153103A patent/BE825240A/xx not_active IP Right Cessation
- 1975-02-07 CH CH150875A patent/CH626601A5/fr not_active IP Right Cessation
- 1975-02-07 JP JP1551175A patent/JPS5343922B2/ja not_active Expired
- 1975-02-07 ES ES434559A patent/ES434559A1/es not_active Expired
- 1975-02-07 NL NLAANVRAGE7501481,A patent/NL180101C/xx not_active IP Right Cessation
- 1975-02-07 US US05/548,159 patent/US3972878A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| BE825240A (fr) | 1975-05-29 |
| CA1040203A (fr) | 1978-10-10 |
| US3972878A (en) | 1976-08-03 |
| GB1489132A (en) | 1977-10-19 |
| DE2504924B2 (de) | 1979-06-07 |
| ATA65675A (de) | 1977-03-15 |
| DE2504924A1 (de) | 1975-08-14 |
| DE2504924C3 (de) | 1980-01-31 |
| FR2260569A1 (cg-RX-API-DMAC7.html) | 1975-09-05 |
| NL7501481A (nl) | 1975-08-12 |
| JPS50137901A (cg-RX-API-DMAC7.html) | 1975-11-01 |
| ES434559A1 (es) | 1976-09-16 |
| NL180101C (nl) | 1987-01-02 |
| AT339873B (de) | 1977-11-10 |
| FR2260569B1 (cg-RX-API-DMAC7.html) | 1978-06-16 |
| CH626601A5 (cg-RX-API-DMAC7.html) | 1981-11-30 |
| NL180101B (nl) | 1986-08-01 |
| JPS5343922B2 (cg-RX-API-DMAC7.html) | 1978-11-24 |
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