HUP0102539A2 - Továbbfejlesztett epoxid polimerizációs eljárás - Google Patents
Továbbfejlesztett epoxid polimerizációs eljárásInfo
- Publication number
- HUP0102539A2 HUP0102539A2 HU0102539A HUP0102539A HUP0102539A2 HU P0102539 A2 HUP0102539 A2 HU P0102539A2 HU 0102539 A HU0102539 A HU 0102539A HU P0102539 A HUP0102539 A HU P0102539A HU P0102539 A2 HUP0102539 A2 HU P0102539A2
- Authority
- HU
- Hungary
- Prior art keywords
- polyether polyol
- polymerization process
- lewis acid
- epoxide
- epoxide polymerization
- Prior art date
Links
- 150000002118 epoxides Chemical class 0.000 title abstract 3
- 238000006116 polymerization reaction Methods 0.000 title abstract 2
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 3
- 239000002184 metal Substances 0.000 abstract 3
- 229920000570 polyether Polymers 0.000 abstract 3
- 229920005862 polyol Polymers 0.000 abstract 3
- 150000003077 polyols Chemical class 0.000 abstract 3
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 2
- 239000002841 Lewis acid Substances 0.000 abstract 2
- 150000007517 lewis acids Chemical class 0.000 abstract 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000008139 complexing agent Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000003999 initiator Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
- C08G65/2645—Metals or compounds thereof, e.g. salts
- C08G65/2663—Metal cyanide catalysts, i.e. DMC's
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
- B01J27/26—Cyanides
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Polyethers (AREA)
Abstract
A találmány tárgya epoxid polimerizációs eljárás, amelyet úgyvégeznek, hogy egy epoxidot és egy aktív hidrogént tartalmazóiniciátort (a) egy kettős fém-cianidot, egy szerves komplexképző szertés egy fémsót tartalmazó lényegében amorf nagy aktivitású kettős fém-cianid komplex katalizátor és (b) egy hatásos mennyiségű nem protikusLewis-sav jelenlétében a poliéter-poliol képzéséhez megfelelőhőmérsékleten és ideig reagáltatnak, ahol az említett poliéter-poliolcsökkentett mennyiségben tartalmaz nagy molekulatömegű végfrakciót anem protikus Lewis-sav elhagyásával készült analóg poliéter-poliolhozképest. Ó
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US09/092,471 US6028230A (en) | 1998-06-05 | 1998-06-05 | Epoxide polymerization process |
PCT/EP1999/003911 WO1999064493A1 (en) | 1998-06-05 | 1999-06-07 | Improved epoxide polymerization process |
Publications (2)
Publication Number | Publication Date |
---|---|
HUP0102539A2 true HUP0102539A2 (hu) | 2001-11-28 |
HUP0102539A3 HUP0102539A3 (en) | 2002-09-30 |
Family
ID=22233379
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU0102539A HUP0102539A3 (en) | 1998-06-05 | 1999-06-07 | Improved epoxide polymerization process |
Country Status (14)
Country | Link |
---|---|
US (1) | US6028230A (hu) |
EP (1) | EP1091994B1 (hu) |
JP (1) | JP2002517578A (hu) |
KR (1) | KR20010052546A (hu) |
CN (1) | CN1110511C (hu) |
AU (1) | AU4508299A (hu) |
BR (1) | BR9911620A (hu) |
CA (1) | CA2334027A1 (hu) |
DE (1) | DE69907459T2 (hu) |
ES (1) | ES2198919T3 (hu) |
HU (1) | HUP0102539A3 (hu) |
ID (1) | ID27582A (hu) |
PT (1) | PT1091994E (hu) |
WO (1) | WO1999064493A1 (hu) |
Families Citing this family (28)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10001779A1 (de) * | 2000-01-18 | 2001-07-19 | Basf Ag | Verfahren zur Herstellung von Polyetheralkoholen |
WO2001083107A2 (en) | 2000-04-28 | 2001-11-08 | Synuthane International, Inc. | Double metal cyanide catalysts containing polyglycol ether complexing agents |
ATE367411T1 (de) * | 2001-11-30 | 2007-08-15 | Asahi Glass Co Ltd | Polyurethanweichschaum und verfahren zur herstellung |
DE10235130A1 (de) * | 2002-08-01 | 2004-02-19 | Bayer Ag | Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen |
DE10317791A1 (de) | 2003-04-16 | 2004-12-02 | Tesa Ag | Haftklebstoff aus Polyurethan für empfindliche Oberflächen |
DE10317788A1 (de) | 2003-04-16 | 2004-12-02 | Tesa Ag | Wiederverwendbare, rückstands- und beschädigungsfrei wiederablösbare, elastische Klebefolie |
DE10317789A1 (de) | 2003-04-16 | 2004-12-02 | Tesa Ag | Haftklebstoff aus Polyurethan |
US20050209438A1 (en) * | 2004-03-19 | 2005-09-22 | Browne Edward P | Starter feed stream acidification in DMC-catalyzed process |
WO2005123805A1 (ja) | 2004-06-16 | 2005-12-29 | Asahi Kasei Chemicals Corporation | 芳香族ポリカーボネートを製造するための重合装置 |
CN100358634C (zh) * | 2005-08-29 | 2008-01-02 | 武汉理工大学 | 一种金属多配体配合物催化剂及其制备方法 |
JP5364966B2 (ja) * | 2006-04-18 | 2013-12-11 | 旭硝子株式会社 | ポリエーテルポリオールまたはポリエーテルモノオールの製造方法 |
DE102006020482A1 (de) | 2006-04-28 | 2007-10-31 | Tesa Ag | Wieder ablösbarer Haftklebstoff aus Polyurethan |
DE102006033796A1 (de) | 2006-07-19 | 2008-01-31 | Tesa Ag | Haftklebestoffe aus einem harzmodifizierten Polyurethan |
US20080021191A1 (en) * | 2006-07-20 | 2008-01-24 | Reese Jack R | High water content tolerant process for the production of polyethers |
US8946486B2 (en) | 2007-12-03 | 2015-02-03 | Tyco Fire & Security Gmbh | Method of forming alkoxylated fluoroalcohols |
DE102008023252A1 (de) | 2008-05-13 | 2009-11-19 | Tesa Se | Hotmelt-Verfahren zur Herstellung eines chemisch vernetzten Polyurethanfilms |
DE102009009757A1 (de) | 2009-02-20 | 2010-08-26 | Tesa Se | Haftklebemasse |
DE102009046657A1 (de) | 2009-11-12 | 2011-05-19 | Tesa Se | Haftklebstoff auf Basis von Polyurethan |
WO2011160296A1 (en) | 2010-06-23 | 2011-12-29 | Basf Se | Modified double metal cyanide catalyst |
JP5731651B2 (ja) * | 2010-08-20 | 2015-06-10 | ビーエーエスエフ ソシエタス・ヨーロピアBasf Se | ポリエーテルエステルポリオールの製造方法 |
ES2881179T3 (es) | 2010-12-27 | 2021-11-29 | Dow Global Technologies Llc | Polimerización de óxido de alquileno usando un complejo catalítico de cianuro de metal doble y un compuesto metálico de magnesio, metal del grupo 3-grupo 15 o metal de la serie de lantánidos |
KR102305944B1 (ko) * | 2013-12-23 | 2021-09-28 | 쉘 인터내셔날 리써취 마트샤피지 비.브이. | 난연성 폴리우레탄 발포체의 제조 방법 |
CN104109234B (zh) * | 2014-08-06 | 2016-06-15 | 山东蓝星东大化工有限责任公司 | 高分子量低不饱和度高伯羟基含量聚醚多元醇的制备方法 |
US9896542B2 (en) * | 2014-10-22 | 2018-02-20 | Dow Global Technologies Llc | Dual catalyst system for high primary hydroxyl polyols |
JP6510098B1 (ja) * | 2018-02-14 | 2019-05-08 | Agc株式会社 | ポリウレタンフォーム製造用組成物、ポリオールシステム液及びポリウレタンフォームの製造方法 |
CN111057228A (zh) * | 2019-12-13 | 2020-04-24 | 张家港美景荣化学工业有限公司 | 一种低分子量聚醚多元醇的制备方法 |
WO2023144294A1 (en) * | 2022-01-28 | 2023-08-03 | Shell Internationale Research Maatschappij B.V. | Processes for polyether polyol purification and preparation |
CN114437335B (zh) * | 2022-02-24 | 2023-09-29 | 浙江皇马科技股份有限公司 | 一种宽分子量分布的脂肪醇聚醚消泡剂的合成方法 |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB1063525A (en) * | 1963-02-14 | 1967-03-30 | Gen Tire & Rubber Co | Organic cyclic oxide polymers, their preparation and tires prepared therefrom |
US3829505A (en) * | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
AU551979B2 (en) * | 1982-03-31 | 1986-05-15 | Shell Internationale Research Maatschappij B.V. | Epoxy polymerisation catalysts |
AU552988B2 (en) * | 1982-03-31 | 1986-06-26 | Shell Internationale Research Maatschappij B.V. | Polymerizing epoxides and catalyst suspensions for this |
JP2743454B2 (ja) * | 1989-04-07 | 1998-04-22 | 旭硝子株式会社 | ポリエーテル類の製造方法 |
JP3068890B2 (ja) * | 1991-05-29 | 2000-07-24 | 旭硝子株式会社 | ポリエーテル類の製造方法 |
JPH06248068A (ja) * | 1993-02-26 | 1994-09-06 | Asahi Glass Co Ltd | ポリエーテル化合物および複合金属シアン化物錯体触媒の製造方法 |
US5712216A (en) * | 1995-05-15 | 1998-01-27 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
US5470813A (en) * | 1993-11-23 | 1995-11-28 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts |
US5482908A (en) * | 1994-09-08 | 1996-01-09 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
US5627122A (en) * | 1995-07-24 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
US5545601A (en) * | 1995-08-22 | 1996-08-13 | Arco Chemical Technology, L.P. | Polyether-containing double metal cyanide catalysts |
US5777177A (en) * | 1996-02-07 | 1998-07-07 | Arco Chemical Technology, L.P. | Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter |
US5689012A (en) * | 1996-07-18 | 1997-11-18 | Arco Chemical Technology, L.P. | Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter |
-
1998
- 1998-06-05 US US09/092,471 patent/US6028230A/en not_active Expired - Fee Related
-
1999
- 1999-06-07 PT PT99927896T patent/PT1091994E/pt unknown
- 1999-06-07 KR KR1020007013695A patent/KR20010052546A/ko not_active Application Discontinuation
- 1999-06-07 BR BR9911620-0A patent/BR9911620A/pt not_active IP Right Cessation
- 1999-06-07 JP JP2000553494A patent/JP2002517578A/ja active Pending
- 1999-06-07 ID IDW20002543A patent/ID27582A/id unknown
- 1999-06-07 CA CA002334027A patent/CA2334027A1/en not_active Abandoned
- 1999-06-07 AU AU45082/99A patent/AU4508299A/en not_active Abandoned
- 1999-06-07 HU HU0102539A patent/HUP0102539A3/hu unknown
- 1999-06-07 DE DE69907459T patent/DE69907459T2/de not_active Expired - Fee Related
- 1999-06-07 WO PCT/EP1999/003911 patent/WO1999064493A1/en not_active Application Discontinuation
- 1999-06-07 EP EP99927896A patent/EP1091994B1/en not_active Expired - Lifetime
- 1999-06-07 CN CN99807060A patent/CN1110511C/zh not_active Expired - Fee Related
- 1999-06-07 ES ES99927896T patent/ES2198919T3/es not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
ID27582A (id) | 2001-04-12 |
ES2198919T3 (es) | 2004-02-01 |
DE69907459T2 (de) | 2004-03-18 |
HUP0102539A3 (en) | 2002-09-30 |
US6028230A (en) | 2000-02-22 |
DE69907459D1 (de) | 2003-06-05 |
PT1091994E (pt) | 2003-08-29 |
CN1110511C (zh) | 2003-06-04 |
CN1304424A (zh) | 2001-07-18 |
EP1091994B1 (en) | 2003-05-02 |
JP2002517578A (ja) | 2002-06-18 |
CA2334027A1 (en) | 1999-12-16 |
BR9911620A (pt) | 2001-10-02 |
EP1091994A1 (en) | 2001-04-18 |
AU4508299A (en) | 1999-12-30 |
KR20010052546A (ko) | 2001-06-25 |
WO1999064493A1 (en) | 1999-12-16 |
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