HUP0003325A2 - Eljárás N-alkil-N' -nitro-guanidin-származékok előállítására - Google Patents
Eljárás N-alkil-N' -nitro-guanidin-származékok előállításáraInfo
- Publication number
- HUP0003325A2 HUP0003325A2 HU0003325A HUP0003325A HUP0003325A2 HU P0003325 A2 HUP0003325 A2 HU P0003325A2 HU 0003325 A HU0003325 A HU 0003325A HU P0003325 A HUP0003325 A HU P0003325A HU P0003325 A2 HUP0003325 A2 HU P0003325A2
- Authority
- HU
- Hungary
- Prior art keywords
- alkyl
- nitroguanidines
- producing
- formula
- cyanamide
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 abstract 1
- XZMCDFZZKTWFGF-UHFFFAOYSA-N Cyanamide Chemical compound NC#N XZMCDFZZKTWFGF-UHFFFAOYSA-N 0.000 abstract 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 abstract 1
- 150000003973 alkyl amines Chemical class 0.000 abstract 1
- -1 alkyl guanidine nitrate Chemical compound 0.000 abstract 1
- 229910017604 nitric acid Inorganic materials 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C277/00—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
- C07C277/08—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
A találmány eljárás (I) általános képletű N-alkil-N'-nitro-guanidin-származékok - képletben R jelentése C1-C4-alkilcsoport -előállítására. Az eljárás során alkilamint salétromsavvalsemlegesítenek és a víz adott esetben elvégzett eltávolítása utáncianamiddal reagáltatnak, majd a kapott alkil-guanidin-nitrátotdehidratálják. Ó
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19712885A DE19712885A1 (de) | 1997-03-27 | 1997-03-27 | Verfahren zur Herstellung von N-Alkyl-N'-nitroguanidinen |
PCT/EP1998/001428 WO1998043951A1 (de) | 1997-03-27 | 1998-03-12 | Verfahren zur herstellung von n-alkyl-n'-nitroguanidinen |
Publications (3)
Publication Number | Publication Date |
---|---|
HUP0003325A2 true HUP0003325A2 (hu) | 2001-02-28 |
HUP0003325A3 HUP0003325A3 (en) | 2001-03-28 |
HU224129B1 HU224129B1 (hu) | 2005-05-30 |
Family
ID=7824794
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU0003325A HU224129B1 (hu) | 1997-03-27 | 1998-03-12 | Eljárás N-alkil-N'-nitro-guanidin-származékok előállítására |
Country Status (14)
Country | Link |
---|---|
US (1) | US6114581A (hu) |
EP (1) | EP0971886B1 (hu) |
JP (1) | JP4010570B2 (hu) |
KR (1) | KR100488197B1 (hu) |
CN (1) | CN1119327C (hu) |
AT (1) | ATE231123T1 (hu) |
AU (1) | AU6830998A (hu) |
BR (1) | BR9808051B1 (hu) |
DE (2) | DE19712885A1 (hu) |
DK (1) | DK0971886T3 (hu) |
ES (1) | ES2187014T3 (hu) |
HU (1) | HU224129B1 (hu) |
IL (1) | IL131579A (hu) |
WO (1) | WO1998043951A1 (hu) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE19939609A1 (de) * | 1999-08-20 | 2001-02-22 | Nigu Chemie Gmbh | Verfahren zur Herstellung von 1-Methyl-3-nitroguanidin |
DE19947332A1 (de) * | 1999-10-01 | 2001-04-05 | Nigu Chemie Gmbh | Verfahren zur Herstellung von 3-Alkyl-N-nitro-4H-1,3,5-oxadiazin-3-iminen |
DE10000891A1 (de) * | 2000-01-12 | 2001-07-19 | Bayer Ag | Verfahren zur Herstellung von N-Methyl-N'-nitroguanidin |
DE10003834A1 (de) * | 2000-01-28 | 2001-08-02 | Nigu Chemie Gmbh | Verfahren zur Herstellung von 1-Methyl-3-nitroguanidin |
CN101565392A (zh) * | 2008-04-21 | 2009-10-28 | 南通天泽化工有限公司 | 一种甲基硝基胍及其制备方法 |
CN105503661A (zh) * | 2016-01-12 | 2016-04-20 | 西安近代化学研究所 | 一种1-氨基-3-硝基胍的合成方法 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IE960441L (en) * | 1988-12-27 | 1990-06-27 | Takeda Chemical Industries Ltd | Guanidine derivatives, their production and insecticides |
US6187773B1 (en) * | 1989-11-10 | 2001-02-13 | Agro-Kanesho Co., Ltd. | Hexahydrotriazine compounds and insecticides |
-
1997
- 1997-03-27 DE DE19712885A patent/DE19712885A1/de not_active Withdrawn
-
1998
- 1998-03-12 CN CN98803645A patent/CN1119327C/zh not_active Expired - Lifetime
- 1998-03-12 KR KR10-1999-7007855A patent/KR100488197B1/ko not_active IP Right Cessation
- 1998-03-12 WO PCT/EP1998/001428 patent/WO1998043951A1/de active IP Right Grant
- 1998-03-12 AT AT98913709T patent/ATE231123T1/de not_active IP Right Cessation
- 1998-03-12 IL IL13157998A patent/IL131579A/xx not_active IP Right Cessation
- 1998-03-12 HU HU0003325A patent/HU224129B1/hu not_active IP Right Cessation
- 1998-03-12 ES ES98913709T patent/ES2187014T3/es not_active Expired - Lifetime
- 1998-03-12 DK DK98913709T patent/DK0971886T3/da active
- 1998-03-12 BR BRPI9808051-2A patent/BR9808051B1/pt not_active IP Right Cessation
- 1998-03-12 US US09/381,675 patent/US6114581A/en not_active Expired - Lifetime
- 1998-03-12 DE DE59806938T patent/DE59806938D1/de not_active Expired - Lifetime
- 1998-03-12 JP JP54110098A patent/JP4010570B2/ja not_active Expired - Lifetime
- 1998-03-12 AU AU68309/98A patent/AU6830998A/en not_active Abandoned
- 1998-03-12 EP EP98913709A patent/EP0971886B1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
BR9808051B1 (pt) | 2009-12-01 |
AU6830998A (en) | 1998-10-22 |
BR9808051A (pt) | 2000-03-08 |
KR20000075782A (ko) | 2000-12-26 |
IL131579A0 (en) | 2001-01-28 |
EP0971886A1 (de) | 2000-01-19 |
EP0971886B1 (de) | 2003-01-15 |
DK0971886T3 (da) | 2003-05-05 |
KR100488197B1 (ko) | 2005-05-10 |
US6114581A (en) | 2000-09-05 |
JP2001516362A (ja) | 2001-09-25 |
DE59806938D1 (de) | 2003-02-20 |
IL131579A (en) | 2003-10-31 |
CN1251089A (zh) | 2000-04-19 |
HUP0003325A3 (en) | 2001-03-28 |
ES2187014T3 (es) | 2003-05-16 |
DE19712885A1 (de) | 1998-10-01 |
JP4010570B2 (ja) | 2007-11-21 |
ATE231123T1 (de) | 2003-02-15 |
CN1119327C (zh) | 2003-08-27 |
HU224129B1 (hu) | 2005-05-30 |
WO1998043951A1 (de) | 1998-10-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
HFG4 | Patent granted, date of granting |
Effective date: 20050401 |
|
MM4A | Lapse of definitive patent protection due to non-payment of fees |