HU182122B - Process for producing elektrode with microchristallic silver surface and process for producing 2,3,5-trichloro-pyridine with the electrode - Google Patents

Process for producing elektrode with microchristallic silver surface and process for producing 2,3,5-trichloro-pyridine with the electrode Download PDF

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Publication number
HU182122B
HU182122B HU80885A HU88580A HU182122B HU 182122 B HU182122 B HU 182122B HU 80885 A HU80885 A HU 80885A HU 88580 A HU88580 A HU 88580A HU 182122 B HU182122 B HU 182122B
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HU
Hungary
Prior art keywords
silver
electrode
conductor
catholyte
aqueous
Prior art date
Application number
HU80885A
Other languages
English (en)
Hungarian (hu)
Inventor
Demetrios Kyriacou
Original Assignee
Dow Chemical Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Chemical Co filed Critical Dow Chemical Co
Publication of HU182122B publication Critical patent/HU182122B/hu

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    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/073Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
    • C25B11/091Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds
    • C25B11/093Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of at least one catalytic element and at least one catalytic compound; consisting of two or more catalytic elements or catalytic compounds at least one noble metal or noble metal oxide and at least one non-noble metal oxide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D213/00Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/61Halogen atoms or nitro radicals
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B11/00Electrodes; Manufacture thereof not otherwise provided for
    • C25B11/04Electrodes; Manufacture thereof not otherwise provided for characterised by the material
    • C25B11/051Electrodes formed of electrocatalysts on a substrate or carrier
    • C25B11/073Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material
    • C25B11/075Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound
    • C25B11/081Electrodes formed of electrocatalysts on a substrate or carrier characterised by the electrocatalyst material consisting of a single catalytic element or catalytic compound the element being a noble metal
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/20Processes
    • C25B3/25Reduction

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Electrodes For Compound Or Non-Metal Manufacture (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Water Treatment By Electricity Or Magnetism (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)
HU80885A 1979-04-13 1980-04-11 Process for producing elektrode with microchristallic silver surface and process for producing 2,3,5-trichloro-pyridine with the electrode HU182122B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US06/029,600 US4242183A (en) 1979-04-13 1979-04-13 Highly active silver cathode, preparation of same and use to make 2,3,5-trichloropyridine

Publications (1)

Publication Number Publication Date
HU182122B true HU182122B (en) 1983-12-28

Family

ID=21849889

Family Applications (1)

Application Number Title Priority Date Filing Date
HU80885A HU182122B (en) 1979-04-13 1980-04-11 Process for producing elektrode with microchristallic silver surface and process for producing 2,3,5-trichloro-pyridine with the electrode

Country Status (21)

Country Link
US (1) US4242183A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
EP (1) EP0018069B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
JP (1) JPS55141585A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
KR (1) KR840001661B1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
AR (1) AR223704A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
AU (1) AU527014B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
BR (1) BR8002257A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CA (1) CA1149767A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
CS (1) CS221544B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DD (1) DD150082A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DE (1) DE3064869D1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
DK (1) DK156480A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ES (1) ES8103783A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
GB (1) GB2051863B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
HU (1) HU182122B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IL (1) IL59482A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
IN (1) IN153664B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
MY (1) MY8500087A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
NZ (1) NZ192994A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
SU (1) SU925254A3 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)
ZA (1) ZA801261B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4367133A (en) * 1980-07-02 1983-01-04 Comsip, Inc. Electrochemical gas analyzer
EP0209611A1 (en) * 1985-07-18 1987-01-28 The Dow Chemical Company Electrolytic cell comprising stainless steel anode and a process for preparing polychloropicolinate anions
US4592811A (en) * 1981-09-28 1986-06-03 The Dow Chemical Company Electrolytic cell comprising stainless steel anode, basic aqueous electrolyte and a cathode at which tetrachloro-2-picolinate ions can be selectively reduced in high yield to 3,6-dichloropicolinate ions _
US4460441A (en) * 1982-08-31 1984-07-17 The Dow Chemical Company Expanded metal as more efficient form of silver cathode for electrolytic reduction of polychloropicolinate anions
US4482436A (en) * 1983-08-10 1984-11-13 The Dow Chemical Company Use of H2 SO4 H3 PO4 to remove electrolytic deposits from silver cathode surfaces
US4755266A (en) * 1986-07-11 1988-07-05 The Dow Chemical Company Process for silver cathode activation
US4778576A (en) * 1986-07-31 1988-10-18 The Dow Chemical Company Nickel alloy anodes for electrochemical dechlorination
DE60100620T2 (de) 2000-01-14 2004-03-11 Dow Agrosciences Llc, Indianapolis Gezielte elektrochemische reduktion von halogenierten 4-amino-picolinsäuren
US7666293B2 (en) * 2007-10-04 2010-02-23 Dow Agrosciences Llc Electrochemical reduction of halogenated 4-aminopicolinic acids
CN101603179B (zh) * 2009-06-29 2013-11-06 浙江工业大学 3,5,6-三氯吡啶甲酸的电解合成方法
JP5818803B2 (ja) * 2009-10-27 2015-11-18 ダウ アグロサイエンシィズ エルエルシー 銀陰極活性化の改良
HRP20170693T1 (hr) * 2009-11-04 2017-07-28 Ffgf Limited Proizvodnja ugljikovodika
CN105887128B (zh) * 2016-05-16 2018-01-12 浙江工业大学 一种五氯吡啶电催化选择性氢化脱氯的方法
CN108611656B (zh) * 2016-12-12 2019-07-30 利尔化学股份有限公司 一种4-氨基-3,6-二氯吡啶-2-甲酸的合成方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1069586B (de) * 1953-09-14 1959-11-26 Union Carbide Corporation New York N Y (V St A) Verfahren zur Elektrolyse wäßriger Salzlosungen unter Verwendung einer kohlenstoffhaltigen Anode
US3130136A (en) * 1961-05-10 1964-04-21 Hercules Powder Co Ltd Electrolytic method for the preparation of gem-dinitrocompounds
US3449162A (en) * 1965-09-17 1969-06-10 Analytic Systems Co Method of making oxygen measuring cells
DE1546728C3 (de) * 1965-09-18 1975-07-17 Varta Batterie Ag, 3000 Hannover Verfahren zur Herstellung eines silberhaltigen pulverförmiger! Katalysators für Sauerstoffelektroden
DE1567689A1 (de) * 1965-10-09 1970-06-11 Barthel Dipl Chem Guenter Elektrode fuer die elektrolytische Zerlegung von Salzsaeure und Verfahren zu ihrer Herstellung
US3657003A (en) * 1970-02-02 1972-04-18 Western Electric Co Method of rendering a non-wettable surface wettable
US3687826A (en) * 1971-01-25 1972-08-29 Dow Chemical Co Electrolytic reduction of polyhaloquinoline and polyhaloisoquinoline
US3694332A (en) * 1971-03-05 1972-09-26 Dow Chemical Co Electrolytic reduction of halogenated pyridines
CH576529A5 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * 1974-10-09 1976-06-15 Bbc Brown Boveri & Cie
DE2508853C3 (de) * 1975-02-28 1980-06-26 Siemens Ag, 1000 Berlin Und 8000 Muenchen Verfahren zur Herstellung dunner Silberkathoden für elektrochemische Zellen
GB1532038A (en) * 1976-10-26 1978-11-15 Ici Ltd Process for the preparation of 2,3,5-trichloropyridine
US4111938A (en) * 1977-09-14 1978-09-05 The Dow Chemical Company Preparation of 2,3,5-trichloropyridine

Also Published As

Publication number Publication date
IL59482A0 (en) 1980-05-30
CA1149767A (en) 1983-07-12
ES489966A0 (es) 1981-03-16
CS221544B2 (en) 1983-04-29
JPH0149793B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1989-10-26
GB2051863B (en) 1983-06-29
DD150082A5 (de) 1981-08-12
IL59482A (en) 1984-02-29
US4242183A (en) 1980-12-30
JPS55141585A (en) 1980-11-05
KR840001661B1 (ko) 1984-10-12
SU925254A3 (ru) 1982-04-30
BR8002257A (pt) 1980-12-02
AR223704A1 (es) 1981-09-15
DK156480A (da) 1980-10-14
ZA801261B (en) 1981-07-29
MY8500087A (en) 1985-12-31
EP0018069B1 (en) 1983-09-21
DE3064869D1 (en) 1983-10-27
KR830002911A (ko) 1983-05-31
GB2051863A (en) 1981-01-21
AU527014B2 (en) 1983-02-10
AU5590280A (en) 1980-10-16
NZ192994A (en) 1983-05-10
ES8103783A1 (es) 1981-03-16
EP0018069A1 (en) 1980-10-29
IN153664B (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) 1984-08-04

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Legal Events

Date Code Title Description
HU90 Patent valid on 900628
HMM4 Cancellation of final prot. due to non-payment of fee