GB887030A - Process for the preparation of trichlorocyanuric acid - Google Patents

Process for the preparation of trichlorocyanuric acid

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Publication number
GB887030A
GB887030A GB1074760A GB1074760A GB887030A GB 887030 A GB887030 A GB 887030A GB 1074760 A GB1074760 A GB 1074760A GB 1074760 A GB1074760 A GB 1074760A GB 887030 A GB887030 A GB 887030A
Authority
GB
United Kingdom
Prior art keywords
alkali metal
cyanurate
chlorine
aqueous solution
trichlorocyanuric acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB1074760A
Inventor
John Donald Christian
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WR Grace and Co
Original Assignee
WR Grace and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WR Grace and Co filed Critical WR Grace and Co
Priority to GB1074760A priority Critical patent/GB887030A/en
Publication of GB887030A publication Critical patent/GB887030A/en
Expired legal-status Critical Current

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Abstract

Trichlorocyanuric acid is made by adding an aqueous solution of "alkali meatal cyanurate" to a cold aqueous solution of chlorine maintaining the resulting mixture at 0 DEG -25 DEG C. and ensuring that the amount of chlorine present is in storchiometric excess over the amount required to convert the added alkali metal cyanurate to trichlorocyanuric acid. Preferably the reaction is carried out at a temperature between 0 DEG and 10 DEG C. "Alkali metal cyanurate" is defined as cyanuric acid, the three hydrogen atoms of which have been replaced by alkali metal atoms. Sufficient alkali metal hydroxide may be present in the reaction mixture to maintain dissolution of the alkali metal cyanurate. Lithium sodium and potassium are specified alkali metals. Chlorine may be passed into the mixture at a rate in excess of the rate required to saturate the mixture with chlorine.ALSO:Trichlorocyanuric acid is made by adding an aqueous solution of "alkali metal cyanurate" to a cold aqueous solution of chlorine, maintaining the resulting mixture at 0 DEG C.-25 DEG C. and ensuring that the amount of chlorine present is in stoichiometric excess over the amount required to convert the added alkali metal cyanurate to trichlorocyanuric acid. Preferably the reaction is carried out at a temperature between 0 DEG C. and 10 DEG C. "Alkali metal cyanurate" is defined as cyanuric acid, the three hydrogen atoms of which have been replaced by alkali metal atoms. Sufficient alkali metal hydroxide may be present in the reaction mixture to maintain p dissolution of the alkali metal cyanurate. Lithium, sodium and potassium are specified alkali metals. Trichlorocyanuric acid may be used as a chlorinating agent for unsaturated organic compounds.
GB1074760A 1960-03-25 1960-03-25 Process for the preparation of trichlorocyanuric acid Expired GB887030A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB1074760A GB887030A (en) 1960-03-25 1960-03-25 Process for the preparation of trichlorocyanuric acid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1074760A GB887030A (en) 1960-03-25 1960-03-25 Process for the preparation of trichlorocyanuric acid

Publications (1)

Publication Number Publication Date
GB887030A true GB887030A (en) 1962-01-10

Family

ID=9973540

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1074760A Expired GB887030A (en) 1960-03-25 1960-03-25 Process for the preparation of trichlorocyanuric acid

Country Status (1)

Country Link
GB (1) GB887030A (en)

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