GB425728A - Improvements in a method of preserving glycol ethers - Google Patents
Improvements in a method of preserving glycol ethersInfo
- Publication number
- GB425728A GB425728A GB1393334A GB1393334A GB425728A GB 425728 A GB425728 A GB 425728A GB 1393334 A GB1393334 A GB 1393334A GB 1393334 A GB1393334 A GB 1393334A GB 425728 A GB425728 A GB 425728A
- Authority
- GB
- United Kingdom
- Prior art keywords
- ether
- glycol ethers
- preserving
- triethanolamine
- alkali
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/34—Separation; Purification; Stabilisation; Use of additives
- C07C41/46—Use of additives, e.g. for stabilisation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Glycol ethers, especially the mono and dialkyl ethers of alkylene and polyalkylene 1,2 glycols, are stabilized by adding a small quantity of a hydroxyalkylamine such as triethanolamine. If aldehydes are present, the ether is preferably first treated by refluxing with acid, neutralizing with alkali, and distilling under reduced pressure. In an example, the monoethyl ether of ethylene glycol is refluxed for 5 hours with a small quantity of sulphuric acid, then a slight excess of alkali is added, and the mixture is fractionated, after which 0,1 per cent of triethanolamine is added to the purified ether.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1393334A GB425728A (en) | 1934-05-08 | 1934-05-08 | Improvements in a method of preserving glycol ethers |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB1393334A GB425728A (en) | 1934-05-08 | 1934-05-08 | Improvements in a method of preserving glycol ethers |
Publications (1)
Publication Number | Publication Date |
---|---|
GB425728A true GB425728A (en) | 1935-03-20 |
Family
ID=10032008
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB1393334A Expired GB425728A (en) | 1934-05-08 | 1934-05-08 | Improvements in a method of preserving glycol ethers |
Country Status (1)
Country | Link |
---|---|
GB (1) | GB425728A (en) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2481278A (en) * | 1946-08-31 | 1949-09-06 | Shell Dev | Polyoxyalkylene compounds |
US2492955A (en) * | 1946-08-31 | 1950-01-03 | Shell Dev | Polyoxyalkylene compounds |
US2514982A (en) * | 1946-10-18 | 1950-07-11 | Shell Dev | Stabilized lubricant |
US2624708A (en) * | 1950-06-23 | 1953-01-06 | Union Carbide & Carbon Corp | Inhibited polyoxyalkylene glycol fluids |
US2665312A (en) * | 1951-08-03 | 1954-01-05 | Dow Chemical Co | Stabilized polyglycol compositions |
US2687377A (en) * | 1951-12-11 | 1954-08-24 | California Research Corp | Lubricant |
US2687378A (en) * | 1951-12-11 | 1954-08-24 | California Research Corp | Lubricating oil composition |
US3294734A (en) * | 1961-04-13 | 1966-12-27 | Hoechst Ag | Amine stabilized trioxane copolymers |
-
1934
- 1934-05-08 GB GB1393334A patent/GB425728A/en not_active Expired
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2481278A (en) * | 1946-08-31 | 1949-09-06 | Shell Dev | Polyoxyalkylene compounds |
US2492955A (en) * | 1946-08-31 | 1950-01-03 | Shell Dev | Polyoxyalkylene compounds |
US2514982A (en) * | 1946-10-18 | 1950-07-11 | Shell Dev | Stabilized lubricant |
US2624708A (en) * | 1950-06-23 | 1953-01-06 | Union Carbide & Carbon Corp | Inhibited polyoxyalkylene glycol fluids |
US2665312A (en) * | 1951-08-03 | 1954-01-05 | Dow Chemical Co | Stabilized polyglycol compositions |
US2687377A (en) * | 1951-12-11 | 1954-08-24 | California Research Corp | Lubricant |
US2687378A (en) * | 1951-12-11 | 1954-08-24 | California Research Corp | Lubricating oil composition |
US3294734A (en) * | 1961-04-13 | 1966-12-27 | Hoechst Ag | Amine stabilized trioxane copolymers |
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