GB1277668A - Improved method of making glycidyl ethers - Google Patents
Improved method of making glycidyl ethersInfo
- Publication number
- GB1277668A GB1277668A GB6219969A GB6219969A GB1277668A GB 1277668 A GB1277668 A GB 1277668A GB 6219969 A GB6219969 A GB 6219969A GB 6219969 A GB6219969 A GB 6219969A GB 1277668 A GB1277668 A GB 1277668A
- Authority
- GB
- United Kingdom
- Prior art keywords
- water
- epichlorohydrin
- alkaline earth
- alkali metal
- earth metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical class C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 title abstract 8
- 238000004519 manufacturing process Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 6
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract 5
- 150000001340 alkali metals Chemical class 0.000 abstract 4
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 229910000272 alkali metal oxide Inorganic materials 0.000 abstract 3
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 abstract 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 2
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 abstract 1
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 abstract 1
- 239000003849 aromatic solvent Substances 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- MIHINWMALJZIBX-UHFFFAOYSA-N cyclohexa-2,4-dien-1-ol Chemical class OC1CC=CC=C1 MIHINWMALJZIBX-UHFFFAOYSA-N 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229920003986 novolac Polymers 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
- C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
- C07D303/22—Ethers with hydroxy compounds containing no oxirane rings with monohydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
- C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
- C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/02—Polycondensates containing more than one epoxy group per molecule
- C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
- C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
- C08G59/063—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Epoxy Compounds (AREA)
- Epoxy Resins (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH18969A CH508680A (de) | 1969-01-08 | 1969-01-08 | Verfahren zum Herstellung von Glycidyläthern |
| CH1602569A CH536334A (de) | 1969-01-08 | 1969-10-28 | Verfahren zum Herstellen von Glycidyläthern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1277668A true GB1277668A (en) | 1972-06-14 |
Family
ID=25683815
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB6219969A Expired GB1277668A (en) | 1969-01-08 | 1969-12-22 | Improved method of making glycidyl ethers |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5218180B1 (https=) |
| AT (1) | AT298805B (https=) |
| CH (1) | CH536334A (https=) |
| DE (1) | DE1961888C3 (https=) |
| FR (1) | FR2027896A1 (https=) |
| GB (1) | GB1277668A (https=) |
| NL (1) | NL7000133A (https=) |
| SE (1) | SE370228B (https=) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109553755A (zh) * | 2017-09-27 | 2019-04-02 | 中国石油化工股份有限公司 | 一种降低环氧氯丙烷消耗的双酚a型环氧树脂生产方法 |
| CN110144038A (zh) * | 2019-05-31 | 2019-08-20 | 江苏鑫露化工新材料有限公司 | 一种双酚a二缩水甘油醚型环氧树脂的合成工艺 |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH551406A (de) * | 1971-04-23 | 1974-07-15 | Reichhold Albert Chemie Ag | Verfahren zum herstellen von glycidylaethern. |
| US3983056A (en) * | 1973-09-27 | 1976-09-28 | Dai Nippon Toryo Co., Ltd. | Aqueous epoxy resin paint composition |
| JPS5558873U (https=) * | 1978-10-16 | 1980-04-21 | ||
| JPS55155468U (https=) * | 1979-04-24 | 1980-11-08 | ||
| JPS56147874U (https=) * | 1980-04-07 | 1981-11-07 | ||
| CA1293837C (en) * | 1986-10-14 | 1991-12-31 | Ha Q. Pham | Preparation of epoxy resins |
| JP6166568B2 (ja) * | 2013-03-28 | 2017-07-19 | 四日市合成株式会社 | エポキシ樹脂組成物、その製造方法、及びエポキシ樹脂硬化物 |
-
1969
- 1969-10-28 CH CH1602569A patent/CH536334A/de unknown
- 1969-12-10 DE DE19691961888 patent/DE1961888C3/de not_active Expired
- 1969-12-15 FR FR6943270A patent/FR2027896A1/fr not_active Withdrawn
- 1969-12-22 GB GB6219969A patent/GB1277668A/en not_active Expired
-
1970
- 1970-01-05 SE SE7270A patent/SE370228B/xx unknown
- 1970-01-05 JP JP1370A patent/JPS5218180B1/ja active Pending
- 1970-01-07 AT AT12570A patent/AT298805B/de not_active IP Right Cessation
- 1970-01-07 NL NL7000133A patent/NL7000133A/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109553755A (zh) * | 2017-09-27 | 2019-04-02 | 中国石油化工股份有限公司 | 一种降低环氧氯丙烷消耗的双酚a型环氧树脂生产方法 |
| CN110144038A (zh) * | 2019-05-31 | 2019-08-20 | 江苏鑫露化工新材料有限公司 | 一种双酚a二缩水甘油醚型环氧树脂的合成工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| SE370228B (https=) | 1974-10-07 |
| AT298805B (de) | 1972-05-25 |
| FR2027896A1 (https=) | 1970-10-02 |
| JPS5218180B1 (https=) | 1977-05-20 |
| DE1961888C3 (de) | 1979-03-29 |
| CH536334A (de) | 1973-04-30 |
| DE1961888B2 (de) | 1978-08-03 |
| NL7000133A (https=) | 1970-07-10 |
| DE1961888A1 (de) | 1970-07-09 |
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| DE1643497C3 (de) | Verfahren zur Herstellung von Glycidyläthern ein- und mehrwertiger Phenole | |
| DE3780349T2 (de) | Deaktivierung eines phosphoniumsalzkatalysators. | |
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| US3023225A (en) | Xchxch | |
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| US3117138A (en) | ||
| GB1453882A (en) | Process for the manufacture of glycidyl ethers of monohydric or polyhydric phenols having improved properties | |
| US3102874A (en) | Diglycidyl ethers of 2,2,2-trichloroethylidene bisphenols | |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |