FR3117380B1 - Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage - Google Patents

Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage Download PDF

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Publication number
FR3117380B1
FR3117380B1 FR2013244A FR2013244A FR3117380B1 FR 3117380 B1 FR3117380 B1 FR 3117380B1 FR 2013244 A FR2013244 A FR 2013244A FR 2013244 A FR2013244 A FR 2013244A FR 3117380 B1 FR3117380 B1 FR 3117380B1
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catalyst
regenerated
rejuvenating
metal
group
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FR2013244A
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FR3117380A1 (fr
Inventor
Elodie Devers
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IFP Energies Nouvelles IFPEN
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IFP Energies Nouvelles IFPEN
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Priority to FR2013244A priority Critical patent/FR3117380B1/fr
Priority to PCT/EP2021/083868 priority patent/WO2022128486A1/fr
Priority to US18/266,661 priority patent/US20240042423A1/en
Priority to CA3198520A priority patent/CA3198520A1/fr
Priority to EP21819481.9A priority patent/EP4263054A1/fr
Priority to CN202180084641.8A priority patent/CN116583351A/zh
Publication of FR3117380A1 publication Critical patent/FR3117380A1/fr
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/485—Impregnating or reimpregnating with, or deposition of metal compounds or catalytically active elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/02—Boron or aluminium; Oxides or hydroxides thereof
    • B01J21/04—Alumina
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/88—Molybdenum
    • B01J23/882—Molybdenum and cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/92—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/90—Regeneration or reactivation
    • B01J23/94—Regeneration or reactivation of catalysts comprising metals, oxides or hydroxides of the iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/14—Phosphorus; Compounds thereof
    • B01J27/186—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J27/188—Phosphorus; Compounds thereof with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium with chromium, molybdenum, tungsten or polonium
    • B01J27/19—Molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/28—Regeneration or reactivation
    • B01J27/285—Regeneration or reactivation of catalysts comprising compounds of phosphorus
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0213—Preparation of the impregnating solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/20—Sulfiding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/28—Phosphorising
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/02—Heat treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/04—Gas or vapour treating; Treating by using liquids vaporisable upon contacting spent catalyst
    • B01J38/12—Treating with free oxygen-containing gas
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J38/00—Regeneration or reactivation of catalysts, in general
    • B01J38/48—Liquid treating or treating in liquid phase, e.g. dissolved or suspended
    • B01J38/60—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using acids
    • B01J38/62—Liquid treating or treating in liquid phase, e.g. dissolved or suspended using acids organic
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/02—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing
    • C10G45/04—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used
    • C10G45/06—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof
    • C10G45/08—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to eliminate hetero atoms without changing the skeleton of the hydrocarbon involved and without cracking into lower boiling hydrocarbons; Hydrofinishing characterised by the catalyst used containing nickel or cobalt metal, or compounds thereof in combination with chromium, molybdenum, or tungsten metals, or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G47/00—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions
    • C10G47/02—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used
    • C10G47/10—Cracking of hydrocarbon oils, in the presence of hydrogen or hydrogen- generating compounds, to obtain lower boiling fractions characterised by the catalyst used with catalysts deposited on a carrier
    • C10G47/12—Inorganic carriers
    • C10G47/16—Crystalline alumino-silicate carriers
    • C10G47/20—Crystalline alumino-silicate carriers the catalyst containing other metals or compounds thereof

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)

Abstract

L'invention concerne un procédé de réjuvénation d’un catalyseur d’hydrotraitement et/ou d’hydrocraquage au moins partiellement usé, ledit catalyseur comprenant un métal du groupe VIIl, un métal du groupe VIB et un support d’oxyde, ledit procédé comprenant les étapes suivantes : a) on régénère le catalyseur,b) puis on met en contact ledit catalyseur régénéré avec une solution d’imprégnation consistant en un mélange d’eau, d’au moins un précurseur d’un métal du groupe VIB, d’au moins un précurseur d’un métal du groupe VIII et d’au moins un composé organique, la quantité de composé organique introduite dans le catalyseur régénéré étant optimisée par rapport aux métaux déjà présents dans le catalyseur régénéré et par rapport à la quantité de métaux introduite via la solution d’imprégnation,c) puis on effectue une étape de séchage sans le calciner ultérieurement.
FR2013244A 2020-12-15 2020-12-15 Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage Active FR3117380B1 (fr)

Priority Applications (6)

Application Number Priority Date Filing Date Title
FR2013244A FR3117380B1 (fr) 2020-12-15 2020-12-15 Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage
PCT/EP2021/083868 WO2022128486A1 (fr) 2020-12-15 2021-12-02 Procede de rejuvenation d'un catalyseur d'un procede d'hydrotraitement et/ou d'hydrocraquage
US18/266,661 US20240042423A1 (en) 2020-12-15 2021-12-02 Method for rejuvenating a catalyst from a hydroprocessing and/or hydrocracking process
CA3198520A CA3198520A1 (fr) 2020-12-15 2021-12-02 Procede de rejuvenation d'un catalyseur d'un procede d'hydrotraitement et/ou d'hydrocraquage
EP21819481.9A EP4263054A1 (fr) 2020-12-15 2021-12-02 Procede de rejuvenation d'un catalyseur d'un procede d'hydrotraitement et/ou d'hydrocraquage
CN202180084641.8A CN116583351A (zh) 2020-12-15 2021-12-02 将来自加氢处理和/或加氢裂化方法的催化剂复原的方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR2013244A FR3117380B1 (fr) 2020-12-15 2020-12-15 Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage
FR2013244 2020-12-15

Publications (2)

Publication Number Publication Date
FR3117380A1 FR3117380A1 (fr) 2022-06-17
FR3117380B1 true FR3117380B1 (fr) 2023-03-03

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FR2013244A Active FR3117380B1 (fr) 2020-12-15 2020-12-15 Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage

Country Status (6)

Country Link
US (1) US20240042423A1 (fr)
EP (1) EP4263054A1 (fr)
CN (1) CN116583351A (fr)
CA (1) CA3198520A1 (fr)
FR (1) FR3117380B1 (fr)
WO (1) WO2022128486A1 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3138053A1 (fr) * 2022-07-22 2024-01-26 IFP Energies Nouvelles Procédé de régénération comprenant une étape de régénération, une étape de réjuvénation et une étape de calcination d’un catalyseur d’hydrocraquage à base de zéolithe et son utilisation dans un procédé d’hydrocraquage.
FR3138054A1 (fr) * 2022-07-22 2024-01-26 IFP Energies Nouvelles Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage
FR3138051A1 (fr) * 2022-07-22 2024-01-26 IFP Energies Nouvelles Procédé de régénération d’un catalyseur d’hydrocraquage à base de zéolithe et son utilisation dans un procédé d’hydrocraquage.
FR3138055A1 (fr) * 2022-07-22 2024-01-26 IFP Energies Nouvelles Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage.
FR3138052A1 (fr) * 2022-07-22 2024-01-26 IFP Energies Nouvelles Procédé de régénération comprenant au moins deux étapes d’un catalyseur d’hydrocraquage à base de zéolithe et son utilisation dans un procédé d’hydrocraquage.
CN117903854A (zh) * 2024-03-19 2024-04-19 成都南玉电力设备有限公司 一种醇氢发动机甲醇燃料催化剂

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BRPI0414865B1 (pt) 2003-10-03 2014-07-08 Albemarle Netherlands Bv Processo para ativação de um catalisador de hidrotratamento
US7820579B2 (en) * 2004-01-20 2010-10-26 Shell Oil Company Method of restoring catalytic activity to a spent hydrotreating catalyst, the resulting restored catalyst, and a method of hydroprocessing
US7906447B2 (en) 2008-04-11 2011-03-15 Exxonmobil Research And Engineering Company Regeneration and rejuvenation of supported hydroprocessing catalysts
CN102463127B (zh) 2010-11-04 2014-05-21 中国石油化工股份有限公司 一种催化剂再生活化方法
FR2972648B1 (fr) 2011-03-18 2013-04-26 Ifp Energies Now Catalyseur utilisable en hydrotraitement comprenant des metaux des groupes viii et vib et preparation avec de l'acide citrique et du succinate de dialkyle c1-c4
JP5892989B2 (ja) 2013-10-07 2016-03-23 日揮触媒化成株式会社 水素化脱硫触媒の再生方法
LU92430B1 (en) 2014-04-16 2015-10-19 Catalyst Recovery Europ Sa Process for rejuvenating hydrotreating catalyst
FR3089824B1 (fr) * 2018-12-18 2021-05-07 Ifp Energies Now Procédé de réjuvénation d’un catalyseur usé et régénéré d’un procédé d'hydrodésulfuration d'essences.
FR3089826B1 (fr) 2018-12-18 2021-05-07 Ifp Energies Now Procédé de réjuvénation d’un catalyseur d’un procédé d'hydrotraitement et/ou d’hydrocraquage.

Also Published As

Publication number Publication date
CN116583351A (zh) 2023-08-11
US20240042423A1 (en) 2024-02-08
EP4263054A1 (fr) 2023-10-25
WO2022128486A1 (fr) 2022-06-23
CA3198520A1 (fr) 2022-06-23
FR3117380A1 (fr) 2022-06-17

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