FR3076554B1 - Procede de production de 5-hydroxymethylfurfural - Google Patents

Procede de production de 5-hydroxymethylfurfural Download PDF

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Publication number
FR3076554B1
FR3076554B1 FR1850210A FR1850210A FR3076554B1 FR 3076554 B1 FR3076554 B1 FR 3076554B1 FR 1850210 A FR1850210 A FR 1850210A FR 1850210 A FR1850210 A FR 1850210A FR 3076554 B1 FR3076554 B1 FR 3076554B1
Authority
FR
France
Prior art keywords
production process
hydroxymethylfurfural
fructose
hydroxymethylfurfural production
producing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
FR1850210A
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English (en)
Other versions
FR3076554A1 (fr
Inventor
Marc Jacquin
Damien Delcroix
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
IFP Energies Nouvelles IFPEN
Original Assignee
IFP Energies Nouvelles IFPEN
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to FR1850210A priority Critical patent/FR3076554B1/fr
Application filed by IFP Energies Nouvelles IFPEN filed Critical IFP Energies Nouvelles IFPEN
Priority to BR112020012936-4A priority patent/BR112020012936B1/pt
Priority to JP2020537741A priority patent/JP2021510371A/ja
Priority to US16/961,184 priority patent/US11261168B2/en
Priority to EP18836825.2A priority patent/EP3737674A1/fr
Priority to PCT/EP2018/086707 priority patent/WO2019137810A1/fr
Priority to CN201880086143.5A priority patent/CN111770916A/zh
Publication of FR3076554A1 publication Critical patent/FR3076554A1/fr
Application granted granted Critical
Publication of FR3076554B1 publication Critical patent/FR3076554B1/fr
Active legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48—Furfural
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40—Radicals substituted by oxygen atoms
    • C07D307/42—Singly bound oxygen atoms
    • C07D307/44—Furfuryl alcohol

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Furan Compounds (AREA)
  • Saccharide Compounds (AREA)

Abstract

L'invention concerne un procédé de production de 5-hydroxyméthylfurfural à partir d'une charge contenant du fructose en présence d'au moins un solvant polaire aprotique et d'au moins un catalyseur de déshydratation, procédé dans lequel la concentration instantanée en fructose est inférieure ou égale à 5,0%pds.
FR1850210A 2018-01-10 2018-01-10 Procede de production de 5-hydroxymethylfurfural Active FR3076554B1 (fr)

Priority Applications (7)

Application Number Priority Date Filing Date Title
FR1850210A FR3076554B1 (fr) 2018-01-10 2018-01-10 Procede de production de 5-hydroxymethylfurfural
JP2020537741A JP2021510371A (ja) 2018-01-10 2018-12-21 ５−ヒドロキシメチルフルフラールの合成プロセス
US16/961,184 US11261168B2 (en) 2018-01-10 2018-12-21 Process for synthesizing 5-hydroxymethylfurfural
EP18836825.2A EP3737674A1 (fr) 2018-01-10 2018-12-21 Procede de production de 5-hydroxymethylfurfural
BR112020012936-4A BR112020012936B1 (pt) 2018-01-10 2018-12-21 Processo de produção de 5-hidroximetilfurfural
PCT/EP2018/086707 WO2019137810A1 (fr) 2018-01-10 2018-12-21 Procede de production de 5-hydroxymethylfurfural
CN201880086143.5A CN111770916A (zh) 2018-01-10 2018-12-21 用于合成5-羟甲基糠醛的方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1850210 2018-01-10
FR1850210A FR3076554B1 (fr) 2018-01-10 2018-01-10 Procede de production de 5-hydroxymethylfurfural

Publications (2)

Publication Number Publication Date
FR3076554A1 FR3076554A1 (fr) 2019-07-12
FR3076554B1 true FR3076554B1 (fr) 2020-09-18

Family

ID=61913371

Family Applications (1)

Application Number Title Priority Date Filing Date
FR1850210A Active FR3076554B1 (fr) 2018-01-10 2018-01-10 Procede de production de 5-hydroxymethylfurfural

Country Status (7)

Country Link
US (1) US11261168B2 (fr)
EP (1) EP3737674A1 (fr)
JP (1) JP2021510371A (fr)
CN (1) CN111770916A (fr)
BR (1) BR112020012936B1 (fr)
FR (1) FR3076554B1 (fr)
WO (1) WO2019137810A1 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3097547B1 (fr) * 2019-06-24 2023-04-28 Ifp Energies Now Procede de production de 5-hydroxymethylfurfural
FR3109778A1 (fr) 2020-04-29 2021-11-05 IFP Energies Nouvelles Procede d’oxydation du 5-hydroxymethylfurfural
FR3115535A1 (fr) 2020-10-23 2022-04-29 IFP Energies Nouvelles Procede d’oxydation du 5-hydroxymethylfurfural
CN113861139B (zh) * 2021-11-04 2023-12-12 浙江糖能科技有限公司 一种制备5-羟甲基糠醛的方法
CN114904510B (zh) * 2022-05-11 2023-04-11 南京林业大学 一种废糖蜜化学活化提高5-hmf浓度的工艺方法及其应用
FR3143384A1 (fr) 2022-12-15 2024-06-21 IFP Energies Nouvelles Monolithe de réplique carbonée de zéolithe et son procédé de préparation

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2551754B1 (fr) * 1983-09-14 1988-04-08 Roquette Freres Procede de fabrication du 5-hydroxymethylfurfural
FR2669635B1 (fr) 1990-11-22 1994-06-10 Furchim Procede de fabrication d'hydroxymethylfurfural (hmf) du purete elevee.
JP6447061B2 (ja) * 2014-11-28 2019-01-09 三菱ケミカル株式会社 フルフラール製造触媒の回収方法、フルフラール製造触媒、および該フルフラール製造触媒を用いたフルフラールの製造方法
FR3039150B1 (fr) 2015-07-24 2017-07-28 Ifp Energies Now Procede de production de 5-hydroxymethylfurfural en presence de catalyseurs organiques de la famille des thiourees
FR3043082B1 (fr) * 2015-11-02 2019-07-26 IFP Energies Nouvelles Procede de production de 5-hydroxymethylfurfural en presence de catalyseurs de la famille des acides sulfoniques homogenes en presence d'au moins un solvant polaire aprotique
FR3043081B1 (fr) * 2015-11-02 2017-12-08 Ifp Energies Now Procede de production de 5-hydroxymethylfurfural en presence d'un catalyseur acide de lewis et/ou d'un catalyseur base heterogene et d'un catalyseur organique homogene acide de brønsted en presence d'au moins un solvant polaire aprotique
JP6648545B2 (ja) * 2016-02-08 2020-02-14 三菱ケミカル株式会社 フルフラール製造原料用糖液の製造方法及びフルフラールの製造方法
DE102016224073A1 (de) * 2016-12-02 2018-06-07 Südzucker AG Verbessertes HMF-Herstellungsverfahren

Also Published As

Publication number Publication date
WO2019137810A1 (fr) 2019-07-18
BR112020012936A2 (pt) 2020-12-01
JP2021510371A (ja) 2021-04-22
EP3737674A1 (fr) 2020-11-18
FR3076554A1 (fr) 2019-07-12
US11261168B2 (en) 2022-03-01
US20210053930A1 (en) 2021-02-25
CN111770916A (zh) 2020-10-13
BR112020012936B1 (pt) 2024-04-30

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