FR2514744A1 - Procede pour fabriquer du silicium a partir de materiau pulverulent contenant de la silice - Google Patents
Procede pour fabriquer du silicium a partir de materiau pulverulent contenant de la silice Download PDFInfo
- Publication number
- FR2514744A1 FR2514744A1 FR8213478A FR8213478A FR2514744A1 FR 2514744 A1 FR2514744 A1 FR 2514744A1 FR 8213478 A FR8213478 A FR 8213478A FR 8213478 A FR8213478 A FR 8213478A FR 2514744 A1 FR2514744 A1 FR 2514744A1
- Authority
- FR
- France
- Prior art keywords
- reducing agent
- process according
- plasma
- pieces
- gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 29
- 229910052710 silicon Inorganic materials 0.000 title claims abstract description 21
- 239000010703 silicon Substances 0.000 title claims abstract description 20
- 239000000463 material Substances 0.000 title claims abstract description 15
- 239000000377 silicon dioxide Substances 0.000 title claims abstract description 13
- 239000003638 chemical reducing agent Substances 0.000 claims abstract description 28
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 239000007787 solid Substances 0.000 claims abstract description 9
- 239000007789 gas Substances 0.000 claims description 15
- 238000004519 manufacturing process Methods 0.000 claims description 7
- 239000006229 carbon black Substances 0.000 claims description 6
- 239000003610 charcoal Substances 0.000 claims description 6
- 239000012159 carrier gas Substances 0.000 claims description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 4
- 239000002006 petroleum coke Substances 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000000571 coke Substances 0.000 claims description 3
- 238000010891 electric arc Methods 0.000 claims description 3
- 239000004065 semiconductor Substances 0.000 claims description 3
- 239000000428 dust Substances 0.000 claims description 2
- 239000003345 natural gas Substances 0.000 claims description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- 239000003502 gasoline Substances 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 13
- 239000002994 raw material Substances 0.000 description 10
- 230000005611 electricity Effects 0.000 description 6
- 239000012535 impurity Substances 0.000 description 6
- 210000004027 cell Anatomy 0.000 description 5
- 238000002474 experimental method Methods 0.000 description 5
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 229910002091 carbon monoxide Inorganic materials 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 229910018540 Si C Inorganic materials 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 239000001294 propane Substances 0.000 description 2
- 238000006722 reduction reaction Methods 0.000 description 2
- 150000003376 silicon Chemical class 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 1
- 229930006000 Sucrose Natural products 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002817 coal dust Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000001939 inductive effect Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910003465 moissanite Inorganic materials 0.000 description 1
- 210000002569 neuron Anatomy 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000010405 reoxidation reaction Methods 0.000 description 1
- 239000011034 rock crystal Substances 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- LIVNPJMFVYWSIS-UHFFFAOYSA-N silicon monoxide Inorganic materials [Si-]#[O+] LIVNPJMFVYWSIS-UHFFFAOYSA-N 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/023—Preparation by reduction of silica or free silica-containing material
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/02—Silicon
- C01B33/021—Preparation
- C01B33/023—Preparation by reduction of silica or free silica-containing material
- C01B33/025—Preparation by reduction of silica or free silica-containing material with carbon or a solid carbonaceous material, i.e. carbo-thermal process
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Silicon Compounds (AREA)
- Medicinal Preparation (AREA)
- Chemical Vapour Deposition (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| SE8106179A SE435370B (sv) | 1981-10-20 | 1981-10-20 | Sett att framstella kisel |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR2514744A1 true FR2514744A1 (fr) | 1983-04-22 |
| FR2514744B1 FR2514744B1 (https=) | 1984-01-06 |
Family
ID=20344826
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR8213478A Granted FR2514744A1 (fr) | 1981-10-20 | 1982-08-02 | Procede pour fabriquer du silicium a partir de materiau pulverulent contenant de la silice |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US4439410A (https=) |
| JP (1) | JPS5869713A (https=) |
| AU (1) | AU546050B2 (https=) |
| BR (1) | BR8204263A (https=) |
| CA (1) | CA1193071A (https=) |
| DE (1) | DE3236705C2 (https=) |
| ES (1) | ES513983A0 (https=) |
| FI (1) | FI68389C (https=) |
| FR (1) | FR2514744A1 (https=) |
| GB (1) | GB2108096B (https=) |
| NO (1) | NO155802B (https=) |
| NZ (1) | NZ201450A (https=) |
| OA (1) | OA07235A (https=) |
| PH (1) | PH17730A (https=) |
| SE (1) | SE435370B (https=) |
| ZA (1) | ZA825405B (https=) |
Families Citing this family (33)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SE432584B (sv) * | 1982-09-07 | 1984-04-09 | Skf Steel Eng Ab | Sett for framstellning av kalciumkarbid sett for framstellning av kalciumkarbid |
| US4680096A (en) * | 1985-12-26 | 1987-07-14 | Dow Corning Corporation | Plasma smelting process for silicon |
| US4981668A (en) * | 1986-04-29 | 1991-01-01 | Dow Corning Corporation | Silicon carbide as a raw material for silicon production |
| US4798659A (en) * | 1986-12-22 | 1989-01-17 | Dow Corning Corporation | Addition of calcium compounds to the carbothermic reduction of silica |
| SE461037B (sv) * | 1987-10-09 | 1989-12-18 | Skf Plasma Tech | Saett att av kol och kiseldioxid kontinuerligt framstaella flytande kisel i en reaktor |
| US5986206A (en) * | 1997-12-10 | 1999-11-16 | Nanogram Corporation | Solar cell |
| NO20061105L (no) * | 2006-03-07 | 2007-09-10 | Kopperaa Miljoinvest As | Fremstilling av rent silisium metall og amorf silika ved reduksjon av kvarts (Sio2) |
| US20080314445A1 (en) * | 2007-06-25 | 2008-12-25 | General Electric Company | Method for the preparation of high purity silicon |
| US20080314446A1 (en) * | 2007-06-25 | 2008-12-25 | General Electric Company | Processes for the preparation of solar-grade silicon and photovoltaic cells |
| US7572425B2 (en) * | 2007-09-14 | 2009-08-11 | General Electric Company | System and method for producing solar grade silicon |
| DE102008010744B4 (de) * | 2008-02-20 | 2010-09-30 | CBD Labs Pty Ltd., Double Bay | Reduktion von Siliziumdioxid |
| RU2367600C1 (ru) * | 2008-04-16 | 2009-09-20 | Борис Георгиевич Грибов | Способ получения кремния высокой чистоты |
| RU2385291C1 (ru) * | 2008-06-24 | 2010-03-27 | Государственное научное учреждение Всероссийский научно-исследовательский институт электрификации сельского хозяйства Российской Академии Сельскохозяйственных наук (ГНУ ВИЭСХ) | Способ получения кристаллического кремния высокой чистоты (варианты) |
| DE102008041334A1 (de) * | 2008-08-19 | 2010-02-25 | Evonik Degussa Gmbh | Herstellung von Silizium durch Umsetzung von Siliziumoxid und Siliziumcarbid gegebenenfalls in Gegenwart einer zweiten Kohlenstoffquelle |
| WO2011099883A1 (ru) * | 2010-02-10 | 2011-08-18 | Shishov Sergey Vladimirovich | Способ получения кремния |
| CA3009630C (en) | 2015-12-16 | 2023-08-01 | Amastan Technologies Llc | Spheroidal dehydrogenated metals and metal alloy particles |
| US10987735B2 (en) | 2015-12-16 | 2021-04-27 | 6K Inc. | Spheroidal titanium metallic powders with custom microstructures |
| KR20190134597A (ko) | 2017-04-04 | 2019-12-04 | 가부시키가이샤 브이 테크놀로지 | 고압 방전 램프 및 그 제어 방법 |
| CN112654444A (zh) | 2018-06-19 | 2021-04-13 | 6K有限公司 | 由原材料制造球化粉末的方法 |
| CA3134579A1 (en) | 2019-04-30 | 2020-11-05 | Gregory Wrobel | Lithium lanthanum zirconium oxide (llzo) powder |
| SG11202111576QA (en) | 2019-04-30 | 2021-11-29 | 6K Inc | Mechanically alloyed powder feedstock |
| CN114641462A (zh) | 2019-11-18 | 2022-06-17 | 6K有限公司 | 用于球形粉末的独特原料及制造方法 |
| US11590568B2 (en) | 2019-12-19 | 2023-02-28 | 6K Inc. | Process for producing spheroidized powder from feedstock materials |
| CA3180426A1 (en) | 2020-06-25 | 2021-12-30 | Richard K. Holman | Microcomposite alloy structure |
| US20220041457A1 (en) * | 2020-08-07 | 2022-02-10 | 6K Inc. | Synthesis of silicon products |
| AU2021349358A1 (en) | 2020-09-24 | 2023-02-09 | 6K Inc. | Systems, devices, and methods for starting plasma |
| CA3196653A1 (en) | 2020-10-30 | 2022-05-05 | Sunil Bhalchandra BADWE | Systems and methods for synthesis of spheroidized metal powders |
| AU2022206483A1 (en) | 2021-01-11 | 2023-08-31 | 6K Inc. | Methods and systems for reclamation of li-ion cathode materials using microwave plasma processing |
| WO2022212291A1 (en) | 2021-03-31 | 2022-10-06 | 6K Inc. | Systems and methods for additive manufacturing of metal nitride ceramics |
| WO2023229928A1 (en) | 2022-05-23 | 2023-11-30 | 6K Inc. | Microwave plasma apparatus and methods for processing materials using an interior liner |
| US12040162B2 (en) | 2022-06-09 | 2024-07-16 | 6K Inc. | Plasma apparatus and methods for processing feed material utilizing an upstream swirl module and composite gas flows |
| WO2024044498A1 (en) | 2022-08-25 | 2024-02-29 | 6K Inc. | Plasma apparatus and methods for processing feed material utilizing a powder ingress preventor (pip) |
| US12195338B2 (en) | 2022-12-15 | 2025-01-14 | 6K Inc. | Systems, methods, and device for pyrolysis of methane in a microwave plasma for hydrogen and structured carbon powder production |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2924584A1 (de) * | 1979-06-19 | 1981-01-15 | Straemke Siegfried | Verfahren zur herstellung von silicium fuer solarzellen |
| DE3000802A1 (de) * | 1980-01-11 | 1981-07-30 | Licentia Patent-Verwaltungs-Gmbh, 6000 Frankfurt | Verfahren zur herstellung vn silizium |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2555507A (en) * | 1949-12-02 | 1951-06-05 | Pratt Emil Bruce | Method of reducing metallic oxide ores |
| FR1328326A (fr) * | 1961-12-01 | 1963-05-31 | Dispositif pour la fusion des produits réfractaires pulvérulents au chalumeau à plasma |
-
1981
- 1981-10-20 SE SE8106179A patent/SE435370B/sv unknown
-
1982
- 1982-06-21 NO NO822065A patent/NO155802B/no unknown
- 1982-07-07 FI FI822417A patent/FI68389C/fi not_active IP Right Cessation
- 1982-07-09 GB GB08219954A patent/GB2108096B/en not_active Expired
- 1982-07-15 ES ES513983A patent/ES513983A0/es active Granted
- 1982-07-22 BR BR8204263A patent/BR8204263A/pt not_active IP Right Cessation
- 1982-07-28 ZA ZA825405A patent/ZA825405B/xx unknown
- 1982-07-29 CA CA000408385A patent/CA1193071A/en not_active Expired
- 1982-07-30 AU AU86635/82A patent/AU546050B2/en not_active Ceased
- 1982-08-02 FR FR8213478A patent/FR2514744A1/fr active Granted
- 1982-08-02 NZ NZ201450A patent/NZ201450A/en unknown
- 1982-08-02 US US06/404,403 patent/US4439410A/en not_active Expired - Fee Related
- 1982-08-04 JP JP57135278A patent/JPS5869713A/ja active Pending
- 1982-08-13 PH PH27726A patent/PH17730A/en unknown
- 1982-10-04 DE DE3236705A patent/DE3236705C2/de not_active Expired
- 1982-10-20 OA OA57827A patent/OA07235A/xx unknown
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2924584A1 (de) * | 1979-06-19 | 1981-01-15 | Straemke Siegfried | Verfahren zur herstellung von silicium fuer solarzellen |
| DE3000802A1 (de) * | 1980-01-11 | 1981-07-30 | Licentia Patent-Verwaltungs-Gmbh, 6000 Frankfurt | Verfahren zur herstellung vn silizium |
Non-Patent Citations (2)
| Title |
|---|
| EXBK/77 * |
| EXBK/79 * |
Also Published As
| Publication number | Publication date |
|---|---|
| GB2108096B (en) | 1985-07-03 |
| FI68389B (fi) | 1985-05-31 |
| FI68389C (fi) | 1987-01-20 |
| AU546050B2 (en) | 1985-08-15 |
| NO155802B (no) | 1987-02-23 |
| PH17730A (en) | 1984-11-21 |
| CA1193071A (en) | 1985-09-10 |
| OA07235A (fr) | 1984-04-30 |
| ES8304886A1 (es) | 1983-04-16 |
| FI822417L (fi) | 1983-04-21 |
| NO822065L (no) | 1983-04-21 |
| SE8106179L (sv) | 1983-04-21 |
| ZA825405B (en) | 1983-06-29 |
| JPS5869713A (ja) | 1983-04-26 |
| FR2514744B1 (https=) | 1984-01-06 |
| GB2108096A (en) | 1983-05-11 |
| BR8204263A (pt) | 1983-07-19 |
| ES513983A0 (es) | 1983-04-16 |
| DE3236705A1 (de) | 1983-04-28 |
| US4439410A (en) | 1984-03-27 |
| SE435370B (sv) | 1984-09-24 |
| AU8663582A (en) | 1983-04-28 |
| DE3236705C2 (de) | 1984-11-29 |
| FI822417A0 (fi) | 1982-07-07 |
| NZ201450A (en) | 1984-09-28 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| ST | Notification of lapse |