FR2456786A1 - Procede de nickelage chimique de pieces metalliques - Google Patents

Procede de nickelage chimique de pieces metalliques

Info

Publication number
FR2456786A1
FR2456786A1 FR8010945A FR8010945A FR2456786A1 FR 2456786 A1 FR2456786 A1 FR 2456786A1 FR 8010945 A FR8010945 A FR 8010945A FR 8010945 A FR8010945 A FR 8010945A FR 2456786 A1 FR2456786 A1 FR 2456786A1
Authority
FR
France
Prior art keywords
treatment solution
agent
solutions
metal parts
treatment
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR8010945A
Other languages
English (en)
Other versions
FR2456786B1 (fr
Inventor
Dimiter Todorov Buchkov
Georgi Gavrilov Georgiev
Svetoslav Alexandrov Savov
Boris Petrov Kozov
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Vmei Lenin
Original Assignee
Vmei Lenin
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Vmei Lenin filed Critical Vmei Lenin
Publication of FR2456786A1 publication Critical patent/FR2456786A1/fr
Application granted granted Critical
Publication of FR2456786B1 publication Critical patent/FR2456786B1/fr
Granted legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601—Process or apparatus
    • C23C18/1633—Process of electroless plating
    • C23C18/1675—Process conditions
    • C23C18/168—Control of temperature, e.g. temperature of bath, substrate
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601—Process or apparatus
    • C23C18/1633—Process of electroless plating
    • C23C18/1655—Process features
    • C23C18/1658—Process features with two steps starting with metal deposition followed by addition of reducing agent
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601—Process or apparatus
    • C23C18/1633—Process of electroless plating
    • C23C18/1675—Process conditions
    • C23C18/1676—Heating of the solution
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/1601—Process or apparatus
    • C23C18/1633—Process of electroless plating
    • C23C18/1675—Process conditions
    • C23C18/1683—Control of electrolyte composition, e.g. measurement, adjustment
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
    • C23C18/31—Coating with metals
    • C23C18/32—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron
    • C23C18/34—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron using reducing agents
    • C23C18/36—Coating with nickel, cobalt or mixtures thereof with phosphorus or boron using reducing agents using hypophosphites

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Electrochemistry (AREA)
  • Chemically Coating (AREA)
  • Electroplating And Plating Baths Therefor (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

PROCEDE DE NICKELAGE CHIMIQUE DE PIECES METALLIQUES. IL CONSISTE A UTILISER TROIS SOLUTIONS CONCENTREES, LA PREMIERE CONTENANT UN SEL DE NICKEL ET UN ACCELERATEUR, LA SECONDE CONTENANT UN AGENT REDUCTEUR, UN AGENT COMPLEXANT, UN AGENT STABILISATEUR ET UN AGENT MOUILLANT ET LA TROISIEME CONTENANT UN AGENT REDUCTEUR QUI EST LE MEME QUE DANS LA SECONDE SOLUTION, UN AGENT COMPLEXANT ET UN AGENT STABILISATEUR, LA SOLUTION DE TRAITEMENT ETANT PREPAREE PAR MELANGE DESDITES PREMIERE ET SECONDE SOLUTIONS CONCENTREES AVEC DE L'EAU DEMINERALISEE DANS DES RAPPORTS EN VOLUME DE 10-20 : 10-20: 60-80, ET REGLAGE PAR ADMISSION DIRECTE, A LA TEMPERATURE DE TRAITEMENT DE CERTAINES QUANTITES DE LA PREMIERE ET DE LA TROISIEME SOLUTIONS DANS LA SOLUTION TRAITANTE, ET EN CE QU'ON AJOUTE DES QUANTITES EGALES RESPECTIVES DE LA PREMIERE ET DE LA TROISIEME SOLUTIONS CONCENTREES, A LA SOLUTION DE TRAITEMENT SELON LA CHARGE DE SURFACE DE CETTE DERNIERE, A DES PERIODES EGALES DE TEMPS CALCULEES PAR UN NOMBRE ENTIER DE MINUTES, LEDIT NOMBRE ENTIER DE MINUTES ETANT EGAL AU NOMBRE DE GRAMMES DU METAL CONTENU DANS LA SOLUTION DE TRAITEMENT SUR UN MODE LINEAIRE EN PARTANT DE LA TEMPERATURE OPTIMALE DE TRAITEMENT POUR ATTEINDRE UNE TEMPERATURE INFERIEURE DE 2C AU POINT D'EBULLITION DE LA SOLUTION DE TRAITEMENT. NICKELAGE DE PIECES METALLIQUES DESTINEES NOTAMMENT AUX ORDINATEURS, AUX REGULATEURS, AUX SYSTEMES DE COMMANDE.
FR8010945A 1979-05-18 1980-05-14 Procede de nickelage chimique de pieces metalliques Granted FR2456786A1 (fr)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
BG7943647A BG32650A1 (en) 1979-05-18 1979-05-18 Method for chemical nickelplating of metal parts

Publications (2)

Publication Number Publication Date
FR2456786A1 true FR2456786A1 (fr) 1980-12-12
FR2456786B1 FR2456786B1 (fr) 1984-12-07

Family

ID=3906083

Family Applications (1)

Application Number Title Priority Date Filing Date
FR8010945A Granted FR2456786A1 (fr) 1979-05-18 1980-05-14 Procede de nickelage chimique de pieces metalliques

Country Status (9)

Country Link
BG (1) BG32650A1 (fr)
CS (1) CS241955B1 (fr)
DD (1) DD160945A3 (fr)
DE (1) DE3018511C2 (fr)
FR (1) FR2456786A1 (fr)
GB (1) GB2050435B (fr)
HU (1) HU182797B (fr)
IT (1) IT8048703A0 (fr)
RO (1) RO79638A (fr)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150307994A1 (en) * 2014-04-29 2015-10-29 Lam Research Corporation ELECTROLESS DEPOSITION OF CONTINUOUS NICKEL LAYER USING COMPLEXED Ti3+ METAL IONS AS REDUCING AGENTS
US20150307995A1 (en) * 2014-04-29 2015-10-29 Lam Research Corporation ELECTROLESS DEPOSITION OF CONTINUOUS PALLADIUM LAYER USING COMPLEXED Co2+ METAL IONS OR Ti3+ METAL IONS AS REDUCING AGENTS

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1179734A (fr) * 1957-07-23 1959-05-27 Procédé et appareillage perfectionnés de nickelage chimique
US3709715A (en) * 1966-05-31 1973-01-09 Dow Chemical Co Electroless nickel plating of hollow containers
US3934054A (en) * 1969-08-25 1976-01-20 Electro Chemical Engineering Gmbh Electroless metal plating

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1621344A1 (de) * 1967-08-04 1971-05-13 Siemens Ag Bad und Verfahren zum chemischen Vernickeln eines festen Koerpers aus Metall,Kunststoff oder Keramik

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1179734A (fr) * 1957-07-23 1959-05-27 Procédé et appareillage perfectionnés de nickelage chimique
US3709715A (en) * 1966-05-31 1973-01-09 Dow Chemical Co Electroless nickel plating of hollow containers
US3934054A (en) * 1969-08-25 1976-01-20 Electro Chemical Engineering Gmbh Electroless metal plating

Also Published As

Publication number Publication date
RO79638A (fr) 1982-08-17
GB2050435A (en) 1981-01-07
IT8048703A0 (it) 1980-05-16
BG32650A1 (en) 1982-09-15
GB2050435B (en) 1983-02-16
CS241955B1 (en) 1986-04-17
FR2456786B1 (fr) 1984-12-07
HU182797B (en) 1984-03-28
DE3018511C2 (de) 1983-12-15
DD160945A3 (de) 1984-07-04
DE3018511A1 (de) 1980-11-27

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Legal Events

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