FR2434144A1 - Procede de preparation de mono- et de poly-isocyanates organiques par scission thermique de chlorhydrates d'urees trisubstituees - Google Patents
Procede de preparation de mono- et de poly-isocyanates organiques par scission thermique de chlorhydrates d'urees trisubstitueesInfo
- Publication number
- FR2434144A1 FR2434144A1 FR7916847A FR7916847A FR2434144A1 FR 2434144 A1 FR2434144 A1 FR 2434144A1 FR 7916847 A FR7916847 A FR 7916847A FR 7916847 A FR7916847 A FR 7916847A FR 2434144 A1 FR2434144 A1 FR 2434144A1
- Authority
- FR
- France
- Prior art keywords
- trisubstituted
- isocyanates
- poly
- preparation
- chlorhydrates
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C263/00—Preparation of derivatives of isocyanic acid
- C07C263/06—Preparation of derivatives of isocyanic acid from or via ureas
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procédé de préparation de mono- et de poly-isocyanates organiques ayant la formule générale R(NCO)n dans laquelle R est un radical aliphatique, cycloaliphatique, aromatique ou hétérocyclique éventuellement substitué, n est un nombre entier de 1 à 3, obtenus par décomposition thermite d'une urée trisubstituée ayant la formule genérale R(NHCONR'R'') n dans laquelle R et R'' qui sont identiques ou différents désignent un radical d'hydrocarbure aliphatique éventuellement substitué contenant 1 à 4 atomes de carbone. On utilise comme produit de départ un produit d'addition d'urées trisubstituées et de l'acide chlorhydrique contenant au moins la quantité stoechiométrique et au plus un excès de 10 molécules % d'acide chlorhydrique, et on effectue la décomposition thermique du mélange réactionnel fondu, en présence d'un solvant organique inerte, dans une enceinte fermée, à une température de 0 à 180 degrés C.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2837341A DE2837341C2 (de) | 1978-08-26 | 1978-08-26 | Verfahren zur Herstellung von organischen Mono- und Polyisocyanaten durch thermische Spaltung der Hydrochloride trisubstituierter Harnstoffe |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2434144A1 true FR2434144A1 (fr) | 1980-03-21 |
FR2434144B1 FR2434144B1 (fr) | 1984-10-05 |
Family
ID=6047992
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7916847A Granted FR2434144A1 (fr) | 1978-08-26 | 1979-06-29 | Procede de preparation de mono- et de poly-isocyanates organiques par scission thermique de chlorhydrates d'urees trisubstituees |
Country Status (16)
Country | Link |
---|---|
US (1) | US4223145A (fr) |
JP (1) | JPS5533480A (fr) |
AT (1) | AT362773B (fr) |
AU (1) | AU523314B2 (fr) |
BE (1) | BE878409A (fr) |
BR (1) | BR7905159A (fr) |
CA (1) | CA1116621A (fr) |
DD (1) | DD145632A5 (fr) |
DE (1) | DE2837341C2 (fr) |
ES (1) | ES483389A1 (fr) |
FR (1) | FR2434144A1 (fr) |
GB (1) | GB2029413B (fr) |
IT (1) | IT1119804B (fr) |
NL (1) | NL7906291A (fr) |
SE (1) | SE7907068L (fr) |
ZA (1) | ZA793327B (fr) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS58179292A (ja) * | 1982-04-13 | 1983-10-20 | Nippon Synthetic Chem Ind Co Ltd:The | 炭化水素系液状混合物の安定化法 |
GB8300016D0 (en) * | 1983-01-04 | 1983-02-09 | Exxon Research Engineering Co | Middle distillate compositions |
GB8618397D0 (en) * | 1986-07-29 | 1986-09-03 | Exxon Chemical Patents Inc | Liquid fuel compositions |
US4871871A (en) * | 1988-11-03 | 1989-10-03 | Arco Chemical Technology, Inc. | Process for the preparation of aromatic mono- and polyisocyanates |
US4873364A (en) * | 1988-12-09 | 1989-10-10 | Arco Chemical Technology, Inc. | Process for the preparation of methylene diphenylene diisocyanates and polymethylene polyphenylene poly (diisocyanates) |
US4883908A (en) * | 1989-02-02 | 1989-11-28 | Arco Chemical Technology, Inc. | Process for the preparation of aromatic isocyanates from dialkyl ureas using an organic sulfonic acid promoter |
US4978779A (en) * | 1989-03-09 | 1990-12-18 | Arco Chemical Technology, Inc. | Preparation of methylene diphenylene diisocyanates and polymethylene polyphenylene poly (isocyanates) using an organic sulfonic acid promoter |
JPH03173859A (ja) * | 1989-04-06 | 1991-07-29 | Arco Chem Technol Inc | 芳香族アミンからの芳香族モノーおよびポリイソシアネートの製造方法 |
EP0402020A1 (fr) * | 1989-06-05 | 1990-12-12 | Arco Chemical Technology, Inc. | Procédé intégré pour la préparation de diisocyanates méthylène diphénylène et de polyisocyanates polyméthylène polyphénylène à partir d'amines et de polyamines |
DE10021742A1 (de) * | 2000-05-04 | 2001-11-08 | Bayer Ag | Verfahren zur Herstellung organischer Monoisocyanate |
EP2042485A1 (fr) * | 2007-09-28 | 2009-04-01 | Huntsman International Llc | Procédé pour le fractionnement d'un mélange de polyisocyanates |
JP5165815B2 (ja) * | 2011-06-24 | 2013-03-21 | 昭和電工株式会社 | エチレン性不飽和基含有イソシアネート化合物の製造方法 |
CN103351312A (zh) * | 2013-07-01 | 2013-10-16 | 太仓市恒益医药化工原料厂 | 一种用于苯二异氰酸酯的制备工艺 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2773086A (en) * | 1953-01-19 | 1956-12-04 | Monsanto Chemicals | Production of isocyanates from substituted ureas |
FR1473821A (fr) * | 1963-07-05 | 1967-03-24 | Carbochimique Et Inst Francais | Nouveaux procédé de fabrication d'esters isocyaniques |
FR2139577A5 (fr) * | 1971-06-01 | 1973-01-05 | Quimco Gmbh | |
US3936848A (en) * | 1972-10-20 | 1976-02-03 | Fuji Photo Optical Co., Ltd. | Independent mirror swing-up means in a single lens reflex camera with memory exposure device |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3936484A (en) * | 1974-09-25 | 1976-02-03 | Atlantic Richfield Company | Production of isocyanates from substituted ureas |
-
1978
- 1978-08-26 DE DE2837341A patent/DE2837341C2/de not_active Expired
-
1979
- 1979-06-29 FR FR7916847A patent/FR2434144A1/fr active Granted
- 1979-07-04 ZA ZA793327A patent/ZA793327B/xx unknown
- 1979-07-05 AU AU48677/79A patent/AU523314B2/en not_active Expired - Fee Related
- 1979-07-10 AT AT0481279A patent/AT362773B/de active
- 1979-07-26 IT IT49869/79A patent/IT1119804B/it active
- 1979-08-01 US US06/062,900 patent/US4223145A/en not_active Expired - Lifetime
- 1979-08-10 BR BR7905159A patent/BR7905159A/pt unknown
- 1979-08-14 ES ES483389A patent/ES483389A1/es not_active Expired
- 1979-08-20 NL NL7906291A patent/NL7906291A/nl not_active Application Discontinuation
- 1979-08-22 CA CA000334276A patent/CA1116621A/fr not_active Expired
- 1979-08-23 DD DD79215154A patent/DD145632A5/de unknown
- 1979-08-24 JP JP10731679A patent/JPS5533480A/ja active Granted
- 1979-08-24 GB GB7929568A patent/GB2029413B/en not_active Expired
- 1979-08-24 BE BE0/196864A patent/BE878409A/fr unknown
- 1979-08-24 SE SE7907068A patent/SE7907068L/xx not_active Application Discontinuation
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2773086A (en) * | 1953-01-19 | 1956-12-04 | Monsanto Chemicals | Production of isocyanates from substituted ureas |
FR1473821A (fr) * | 1963-07-05 | 1967-03-24 | Carbochimique Et Inst Francais | Nouveaux procédé de fabrication d'esters isocyaniques |
FR2139577A5 (fr) * | 1971-06-01 | 1973-01-05 | Quimco Gmbh | |
DE2225365A1 (de) * | 1971-06-01 | 1973-01-25 | Quimco Gmbh | Verfahren zur herstellung von organischen mono- und polyisocyanaten |
US3936848A (en) * | 1972-10-20 | 1976-02-03 | Fuji Photo Optical Co., Ltd. | Independent mirror swing-up means in a single lens reflex camera with memory exposure device |
Also Published As
Publication number | Publication date |
---|---|
IT7949869A0 (it) | 1979-07-26 |
BE878409A (fr) | 1979-12-17 |
AU4867779A (en) | 1980-03-06 |
NL7906291A (nl) | 1980-02-28 |
SE7907068L (sv) | 1980-02-27 |
JPS5533480A (en) | 1980-03-08 |
BR7905159A (pt) | 1980-05-06 |
DE2837341C2 (de) | 1983-02-17 |
GB2029413B (en) | 1982-11-03 |
ES483389A1 (es) | 1980-04-16 |
AT362773B (de) | 1981-06-10 |
AU523314B2 (en) | 1982-07-22 |
GB2029413A (en) | 1980-03-19 |
US4223145A (en) | 1980-09-16 |
IT1119804B (it) | 1986-03-10 |
ZA793327B (en) | 1980-07-30 |
FR2434144B1 (fr) | 1984-10-05 |
ATA481279A (de) | 1980-11-15 |
DE2837341A1 (de) | 1980-03-20 |
CA1116621A (fr) | 1982-01-19 |
DD145632A5 (de) | 1980-12-24 |
JPS6320218B2 (fr) | 1988-04-26 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |