FR2371405A1 - Procede pour la fabrication d'ethyleneglycols tres purs - Google Patents
Procede pour la fabrication d'ethyleneglycols tres pursInfo
- Publication number
- FR2371405A1 FR2371405A1 FR7734511A FR7734511A FR2371405A1 FR 2371405 A1 FR2371405 A1 FR 2371405A1 FR 7734511 A FR7734511 A FR 7734511A FR 7734511 A FR7734511 A FR 7734511A FR 2371405 A1 FR2371405 A1 FR 2371405A1
- Authority
- FR
- France
- Prior art keywords
- manufacture
- pure
- ethyleneglycols
- pure ethylene
- fibers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title abstract 4
- 238000000034 method Methods 0.000 title abstract 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical class OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 1
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000000835 fiber Substances 0.000 abstract 1
- 239000012535 impurity Substances 0.000 abstract 1
- 229910000033 sodium borohydride Inorganic materials 0.000 abstract 1
- 239000012279 sodium borohydride Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/09—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis
- C07C29/10—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes
- C07C29/103—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers
- C07C29/106—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by hydrolysis of ethers, including cyclic ethers, e.g. oxiranes of cyclic ethers of oxiranes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/20—Dihydroxylic alcohols
- C07C31/202—Ethylene glycol
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procédé pour la fabrication d'éthylèneglycols très purs. Dans ce procédé, le perfectionnement consiste à réduire les impuretés organiques oxygénées, en traitant leurs solutions aqueuses obtenues pendant la fabrication de l'oxyde d'éthylène, avec une solution d'un borohydrure de métal alcalin, en l'occurence de borohydrure de sodium, dans un milieu de préférence nettement alcalin. L'éthylèneglycol très pur ainsi obtenu a des valeurs d'absorption en UV extrêmement faibles et convient très bien pour la fabrication des fibres.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
IT29386/76A IT1063805B (it) | 1976-11-17 | 1976-11-17 | Procedimento per la produzione di glicoli etilenici ad alta purezza |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2371405A1 true FR2371405A1 (fr) | 1978-06-16 |
FR2371405B1 FR2371405B1 (fr) | 1980-08-22 |
Family
ID=11226884
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7734511A Granted FR2371405A1 (fr) | 1976-11-17 | 1977-11-16 | Procede pour la fabrication d'ethyleneglycols tres purs |
Country Status (26)
Country | Link |
---|---|
US (1) | US4358625A (fr) |
JP (1) | JPS5363304A (fr) |
AR (1) | AR217090A1 (fr) |
AT (1) | AT359054B (fr) |
AU (1) | AU514202B2 (fr) |
BE (1) | BE860929A (fr) |
BR (1) | BR7707598A (fr) |
CS (1) | CS196408B2 (fr) |
DD (1) | DD133791A5 (fr) |
DE (1) | DE2751383B2 (fr) |
DK (1) | DK500077A (fr) |
ES (1) | ES464378A1 (fr) |
FR (1) | FR2371405A1 (fr) |
GB (1) | GB1560135A (fr) |
HU (1) | HU175533B (fr) |
IN (1) | IN146447B (fr) |
IT (1) | IT1063805B (fr) |
LU (1) | LU78518A1 (fr) |
NL (1) | NL7712471A (fr) |
NO (1) | NO773911L (fr) |
PL (1) | PL109691B1 (fr) |
RO (1) | RO71280A (fr) |
SE (1) | SE7712960L (fr) |
TR (1) | TR19507A (fr) |
YU (1) | YU270477A (fr) |
ZA (1) | ZA776810B (fr) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2430925A1 (fr) * | 1978-07-15 | 1980-02-08 | Huels Chemische Werke Ag | Procede de purification du 2-(2-ethoxyethoxy)-ethanol (ethermonoethylique du diethyleneglycol) et du dipropyleneglycol |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3001727A1 (de) * | 1980-01-18 | 1981-07-23 | Hoechst Ag, 6000 Frankfurt | Verfahren zur herstellung von hochreinem monoethylenglykol |
DE3683264D1 (de) * | 1985-11-18 | 1992-02-13 | Mitsui Toatsu Chemicals | Verfahren zur herstellung von ethylenglykol und/oder propylenglykol. |
US4830712A (en) * | 1987-09-29 | 1989-05-16 | Union Carbide Corporation | Process for refining ethylene glycol |
US5196601A (en) * | 1989-12-26 | 1993-03-23 | Kao Corporation | Process for producing alcohol or amine |
DE4304465C2 (de) * | 1993-02-15 | 1995-01-05 | Schilling Chemie Gmbh U Produk | Verfahren zur Entfernung in Wasser gelösten Sauerstoffs, insbesondere in wasserführenden, geschlossenen Systemen |
JP4740432B2 (ja) * | 1999-07-14 | 2011-08-03 | 株式会社日本触媒 | エチレングリコールの精製方法 |
US6187973B1 (en) | 2000-04-06 | 2001-02-13 | Scientific Design Company, Inc. | Glycol purification |
US6242655B1 (en) * | 2000-07-11 | 2001-06-05 | Scientific Design Company, Inc. | Glycol purification |
TW200838838A (en) * | 2006-12-22 | 2008-10-01 | Dow Technology Investments Llc | Process for reducing side-reactions during alkylene glycol and poly-alkylene glycol manufacturing |
DE102009038398A1 (de) * | 2009-08-24 | 2011-03-03 | Uhde Gmbh | Verfahren und Vorrichtung zur Herstellung von Alkylenoxiden und von Alkylenglykolen |
ES2781984T3 (es) * | 2013-10-23 | 2020-09-09 | Basf Se | Procedimiento para la preparación de 1,4-butanodiol con un número de color APHA menor que 30 |
CN107285997B (zh) * | 2016-03-30 | 2022-04-22 | 长春美禾科技发展有限公司 | 一种改善乙二醇紫外透过率的方法 |
CN111662162B (zh) * | 2020-05-23 | 2022-08-12 | 安阳化学工业集团有限责任公司 | 一种提高煤制乙二醇紫外透光率所用的添加剂及其利用添加剂制备聚酯级乙二醇的方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1025852B (de) | 1954-11-19 | 1958-03-13 | Basf Ag | Verfahren zur Gewinnung reiner Glykole |
US2867651A (en) * | 1955-10-24 | 1959-01-06 | Standard Oil Co | Purification of alcohols and production of esters in the presence of borohydrides |
GB912797A (en) | 1960-04-22 | 1962-12-12 | Union Carbide Corp | Improvements in and relating to a process for refining alcohols |
US3860520A (en) * | 1967-08-22 | 1975-01-14 | Continental Oil Co | Odor reduction in alcohols |
US3597452A (en) * | 1968-02-19 | 1971-08-03 | Jefferson Chem Co Inc | Treatment of ethylene oxide process cycle water with an amine residue |
US3970711A (en) * | 1971-07-19 | 1976-07-20 | Ppg Industries, Inc. | Method of producing glycols |
US3904656A (en) * | 1973-02-13 | 1975-09-09 | Ppg Industries Inc | Process for preparing monoethylene glycol and ethylene oxide |
-
1976
- 1976-11-17 IT IT29386/76A patent/IT1063805B/it active
-
1977
- 1977-11-10 DK DK500077A patent/DK500077A/da unknown
- 1977-11-11 BR BR7707598A patent/BR7707598A/pt unknown
- 1977-11-11 YU YU02704/77A patent/YU270477A/xx unknown
- 1977-11-11 NL NL7712471A patent/NL7712471A/xx not_active Application Discontinuation
- 1977-11-15 IN IN1605/CAL/77A patent/IN146447B/en unknown
- 1977-11-15 PL PL1977202145A patent/PL109691B1/pl unknown
- 1977-11-15 DD DD7700202095A patent/DD133791A5/xx unknown
- 1977-11-15 ZA ZA00776810A patent/ZA776810B/xx unknown
- 1977-11-15 NO NO773911A patent/NO773911L/no unknown
- 1977-11-15 LU LU78518A patent/LU78518A1/xx unknown
- 1977-11-16 GB GB47766/77A patent/GB1560135A/en not_active Expired
- 1977-11-16 CS CS777549A patent/CS196408B2/cs unknown
- 1977-11-16 AT AT818177A patent/AT359054B/de not_active IP Right Cessation
- 1977-11-16 SE SE7712960A patent/SE7712960L/xx not_active Application Discontinuation
- 1977-11-16 FR FR7734511A patent/FR2371405A1/fr active Granted
- 1977-11-16 AU AU30693/77A patent/AU514202B2/en not_active Expired
- 1977-11-16 RO RO7792137A patent/RO71280A/fr unknown
- 1977-11-16 HU HU77SA3073A patent/HU175533B/hu unknown
- 1977-11-17 AR AR270011A patent/AR217090A1/es active
- 1977-11-17 JP JP13731677A patent/JPS5363304A/ja active Pending
- 1977-11-17 BE BE182703A patent/BE860929A/fr unknown
- 1977-11-17 DE DE2751383A patent/DE2751383B2/de not_active Withdrawn
- 1977-11-17 ES ES464378A patent/ES464378A1/es not_active Expired
- 1977-11-17 TR TR19507A patent/TR19507A/xx unknown
-
1979
- 1979-03-09 US US06/019,109 patent/US4358625A/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2430925A1 (fr) * | 1978-07-15 | 1980-02-08 | Huels Chemische Werke Ag | Procede de purification du 2-(2-ethoxyethoxy)-ethanol (ethermonoethylique du diethyleneglycol) et du dipropyleneglycol |
Also Published As
Publication number | Publication date |
---|---|
DE2751383A1 (de) | 1978-05-18 |
PL109691B1 (en) | 1980-06-30 |
PL202145A1 (pl) | 1978-12-04 |
BE860929A (fr) | 1978-05-17 |
DD133791A5 (de) | 1979-01-24 |
AU514202B2 (en) | 1981-01-29 |
GB1560135A (en) | 1980-01-30 |
IN146447B (fr) | 1979-06-02 |
YU270477A (en) | 1982-05-31 |
AU3069377A (en) | 1979-05-24 |
NL7712471A (nl) | 1978-05-19 |
DE2751383B2 (de) | 1980-03-06 |
RO71280A (fr) | 1982-02-26 |
TR19507A (tr) | 1979-03-29 |
SE7712960L (sv) | 1978-05-18 |
HU175533B (hu) | 1980-08-28 |
IT1063805B (it) | 1985-02-18 |
LU78518A1 (fr) | 1978-03-20 |
ATA818177A (de) | 1980-03-15 |
ZA776810B (en) | 1978-09-27 |
AT359054B (de) | 1980-10-27 |
DK500077A (da) | 1978-05-18 |
US4358625A (en) | 1982-11-09 |
JPS5363304A (en) | 1978-06-06 |
BR7707598A (pt) | 1978-06-20 |
NO773911L (no) | 1978-05-19 |
AR217090A1 (es) | 1980-02-29 |
CS196408B2 (en) | 1980-03-31 |
FR2371405B1 (fr) | 1980-08-22 |
ES464378A1 (es) | 1978-09-01 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |