FI121541B - Menetelmä muurahaishapon talteenottamiseksi - Google Patents

Menetelmä muurahaishapon talteenottamiseksi Download PDF

Info

Publication number
FI121541B
FI121541B FI20085336A FI20085336A FI121541B FI 121541 B FI121541 B FI 121541B FI 20085336 A FI20085336 A FI 20085336A FI 20085336 A FI20085336 A FI 20085336A FI 121541 B FI121541 B FI 121541B
Authority
FI
Finland
Prior art keywords
furfural
acid
weight
formic acid
extraction
Prior art date
Application number
FI20085336A
Other languages
English (en)
Finnish (fi)
Swedish (sv)
Other versions
FI20085336A0 (fi
FI20085336A (fi
Inventor
Pekka Oinas
Timo Nissinen
Jarmo Reunanen
Original Assignee
Kemira Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kemira Oyj filed Critical Kemira Oyj
Publication of FI20085336A0 publication Critical patent/FI20085336A0/fi
Priority to FI20085336A priority Critical patent/FI121541B/fi
Priority to EP09734366A priority patent/EP2291344A1/en
Priority to CN200980114171.4A priority patent/CN102015611B/zh
Priority to PCT/FI2009/050312 priority patent/WO2009130387A2/en
Priority to US12/988,998 priority patent/US8492586B2/en
Priority to CA2721165A priority patent/CA2721165C/en
Priority to EP09735350A priority patent/EP2285766A2/en
Priority to PCT/FI2009/050311 priority patent/WO2009130386A1/en
Priority to CN200980116973.9A priority patent/CN102026953B/zh
Priority to CA2721168A priority patent/CA2721168A1/en
Priority to US12/989,001 priority patent/US8530695B2/en
Publication of FI20085336A publication Critical patent/FI20085336A/fi
Application granted granted Critical
Publication of FI121541B publication Critical patent/FI121541B/fi

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/43Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/48Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C53/00Saturated compounds having only one carboxyl group bound to an acyclic carbon atom or hydrogen
    • C07C53/02Formic acid
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C59/00Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C59/185Saturated compounds having only one carboxyl group and containing keto groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48Furfural
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D307/00Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
    • C07D307/02Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
    • C07D307/34Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D307/38Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D307/40Radicals substituted by oxygen atoms
    • C07D307/46Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
    • C07D307/48Furfural
    • C07D307/50Preparation from natural products
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00Technologies relating to chemical industry
    • Y02P20/50Improvements relating to the production of bulk chemicals
    • Y02P20/582Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
FI20085336A 2008-04-21 2008-04-21 Menetelmä muurahaishapon talteenottamiseksi FI121541B (fi)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FI20085336A FI121541B (fi) 2008-04-21 2008-04-21 Menetelmä muurahaishapon talteenottamiseksi
EP09735350A EP2285766A2 (en) 2008-04-21 2009-04-21 A process for preparation of formate salt
CN200980114171.4A CN102015611B (zh) 2008-04-21 2009-04-21 用于制备甲酸盐的方法
PCT/FI2009/050312 WO2009130387A2 (en) 2008-04-21 2009-04-21 A process for preparation of formate salt
US12/988,998 US8492586B2 (en) 2008-04-21 2009-04-21 Process for preparation of formate salt
CA2721165A CA2721165C (en) 2008-04-21 2009-04-21 A process for recovery of formic acid
EP09734366A EP2291344A1 (en) 2008-04-21 2009-04-21 A process for recovery of formic acid
PCT/FI2009/050311 WO2009130386A1 (en) 2008-04-21 2009-04-21 A process for recovery of formic acid
CN200980116973.9A CN102026953B (zh) 2008-04-21 2009-04-21 用于回收甲酸的方法
CA2721168A CA2721168A1 (en) 2008-04-21 2009-04-21 A process for preparation of formate salt
US12/989,001 US8530695B2 (en) 2008-04-21 2009-04-21 Process for recovery of formic acid

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20085336 2008-04-21
FI20085336A FI121541B (fi) 2008-04-21 2008-04-21 Menetelmä muurahaishapon talteenottamiseksi

Publications (3)

Publication Number Publication Date
FI20085336A0 FI20085336A0 (fi) 2008-04-21
FI20085336A FI20085336A (fi) 2009-10-22
FI121541B true FI121541B (fi) 2010-12-31

Family

ID=39385961

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20085336A FI121541B (fi) 2008-04-21 2008-04-21 Menetelmä muurahaishapon talteenottamiseksi

Country Status (6)

Country Link
US (2) US8530695B2 (zh)
EP (2) EP2291344A1 (zh)
CN (2) CN102015611B (zh)
CA (2) CA2721165C (zh)
FI (1) FI121541B (zh)
WO (2) WO2009130387A2 (zh)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FI121541B (fi) 2008-04-21 2010-12-31 Kemira Oyj Menetelmä muurahaishapon talteenottamiseksi
EP2336222A1 (en) * 2009-12-17 2011-06-22 Shell Internationale Research Maatschappij B.V. Process for treating lignocellulosic biomass material
US9174915B2 (en) 2010-06-04 2015-11-03 Exxonmobil Chemical Patents Inc. Extraction towers and processes for using the same
WO2012106040A2 (en) * 2011-02-01 2012-08-09 University Of Maine System Board Of Trustees Process for improving the energy density of feedstocks using formate salts
US8389749B2 (en) 2011-05-25 2013-03-05 Wisconsin Alumni Research Foundation Method to produce, recover and convert furan derivatives from aqueous solutions using alkylphenol extraction
US8962867B2 (en) 2011-05-25 2015-02-24 Wisconsin Alumni Research Foundation Solute-enhanced production of gamma-valerolactone (GVL) from aqueous solutions of levulinic acid
US8389761B2 (en) * 2011-05-25 2013-03-05 Wisconsin Alumni Research Foundation Method to produce and recover levulinic acid and/or gamma-valerolactone from aqueous solutions using alkylphenols
FR2979344B1 (fr) * 2011-08-26 2014-01-24 Centre Nat Rech Scient Procede de preparation de furfural
FI126351B (en) * 2011-11-04 2016-10-14 Taminco Finland Oy Method and apparatus for separating at least one carboxylic acid and furfural from a dilute aqueous solution
US20140316161A1 (en) 2011-11-23 2014-10-23 Segetis, Inc. Process to prepare levulinic acid
WO2013183962A1 (ko) * 2012-06-07 2013-12-12 단국대학교 산학협력단 바이오매스 처리를 위한 전처리 과정과 분리 과정의 동시 진행 방법 및 이를 이용하여 정제되는 바이오 케미컬
EP2872495B1 (en) * 2012-07-13 2016-08-24 DSM IP Assets B.V. Process for the production of furfural and levulinic acid from lignocellulosic biomass
US9073841B2 (en) 2012-11-05 2015-07-07 Segetis, Inc. Process to prepare levulinic acid
TWI476203B (zh) 2013-03-18 2015-03-11 Ind Tech Res Inst 醣類的分離方法
BR112015026960B1 (pt) * 2013-04-27 2021-07-27 The Regents Of The University Of California Métodos para a produção de intermediários reativos a partir de biomassa e para a solubilização e conversão catalítica combinadas de biomassa
US10407373B2 (en) 2013-05-16 2019-09-10 Georgia-Pacific LLC Process for the separation of formic acid from methyltetrahydrofuran
WO2015034964A1 (en) * 2013-09-03 2015-03-12 Virdia, Inc. Methods for extracting and converting hemicellulose sugars
US9403734B2 (en) * 2013-09-18 2016-08-02 Georgia-Pacific LLC Method for producing organic acids and organic acid degradation compounds from biomass
CN104058948B (zh) * 2014-07-03 2016-01-27 河北华旭化工有限公司 从特戊酸合成过程副产的废酸中回收硫酸和特戊酸的方法
US10125344B2 (en) * 2014-10-01 2018-11-13 Korea Institute Of Science And Technology Apparatus and method for bioenergy production using regenerated acid solution
WO2016078698A1 (de) 2014-11-18 2016-05-26 Jbach Gmbh Verfahren zum gewinnen eines formiats aus einem reaktionsgemisch
EP3045447A1 (de) * 2015-01-19 2016-07-20 Jbach GmbH Verfahren zum Absondern von Ameisensäure aus einem Reaktionsgemisch
CN106256809B (zh) * 2015-06-19 2019-04-12 中国石油化工股份有限公司 生物质生产芳烃的方法及该方法得到的组合物
CN106397183B (zh) * 2015-07-28 2021-03-16 易高环保能源研究院有限公司 从生物质酸催化水解产物中分离乙酰丙酸、甲酸和糠醛的方法
CN106748738A (zh) * 2015-11-25 2017-05-31 衡阳屹顺化工有限公司 一种分离甲酸钠的优化萃取工艺
CN109890803A (zh) 2016-11-01 2019-06-14 国际壳牌研究有限公司 用于回收糠醛的方法
CA3039790A1 (en) 2016-11-01 2018-05-11 Shell Internationale Research Maatschappij B.V. Process for the recovery of furfural
BR112019008839B1 (pt) 2016-11-01 2022-12-27 Shell Internationale Research Maatschappij B.V Processo para a extração de furfural
WO2018085182A1 (en) 2016-11-01 2018-05-11 Shell Oil Company Process for the recovery of furfural
CN106748737A (zh) * 2016-11-16 2017-05-31 南京师范大学 一种共沸萃取精馏浓缩甲酸水溶液中甲酸的方法
FI129405B (en) * 2016-12-30 2022-01-31 Upm Kymmene Corp Method and apparatus for separating furfural
CN108299189A (zh) * 2018-02-06 2018-07-20 北京凯瑞英科技有限公司 硝基甲烷水解制备盐酸羟胺副产物回收利用装置和方法
CN113825746B (zh) 2019-05-22 2024-04-05 国际壳牌研究有限公司 用于生产糠醛的方法
CN110241148A (zh) * 2019-07-09 2019-09-17 南京林业大学 一种联产糠醇和乳酸的方法
FI20216275A1 (en) * 2021-12-14 2023-06-15 Chempolis Oy Method and device for processing biomass

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2257389A (en) * 1939-10-02 1941-09-30 Du Pont Recovery of levulinic acid
US2684982A (en) * 1951-11-19 1954-07-27 Quaker Oats Co Recovery of levulinic acid
US2813900A (en) * 1953-08-05 1957-11-19 Quaker Oats Co Process for producing levulinic acid
DE1518686A1 (de) 1965-12-07 1969-04-10 Kalk Chemische Fabrik Gmbh Verfahren zur Granulierung von Calciumformiat
US4217460A (en) 1975-10-11 1980-08-12 Basf Aktiengesellschaft Isolation of formic acid from its aqueous solutions
AT367473B (de) 1980-04-10 1982-07-12 Kanzler Walter Verfahren zur gewinnung von furfurol, ameisensaeure, essigsaeure aus sauren hydrolysaten von pflanzen
US4692219A (en) * 1986-12-03 1987-09-08 Celanese Chemical Co. Separation of formic acid from acetic acid by extractive distillation
US4897497A (en) 1988-04-26 1990-01-30 Biofine Incorporated Lignocellulose degradation to furfural and levulinic acid
EP0439503A1 (en) 1988-10-21 1991-08-07 Nicholas Brown Coating compositions and emulsions
US5399751A (en) * 1993-11-05 1995-03-21 Glitsch, Inc. Method for recovering carboxylic acids from aqueous solutions
US5608105A (en) 1995-06-07 1997-03-04 Biofine Incorporated Production of levulinic acid from carbohydrate-containing materials
US5892107A (en) * 1996-11-08 1999-04-06 Arkenol, Inc. Method for the production of levulinic acid
CN1074761C (zh) 1999-11-26 2001-11-14 清华大学 用含磷萃取剂分离提浓甲酸的方法
WO2001046520A1 (de) * 1999-12-22 2001-06-28 Natural Pulping Ag Verfahren zur gewinnung/rückgewinnung von carbonsäuren aus ablaugen der zellstoffherstellung mittels extraktion
DE10002794A1 (de) * 2000-01-24 2001-07-26 Basf Ag Abwasserreinigung beim Verfahren zur Herstellung von wasserfreier Ameisensäure
JP2002193862A (ja) * 2000-12-28 2002-07-10 Idemitsu Petrochem Co Ltd ビスフェノールaの製造方法
DE10065466A1 (de) 2000-12-28 2002-07-18 Consortium Elektrochem Ind Verfahren zur Trennung eines wässrigen Gemisches aus den Hauptkomponenten Essigsäure und Ameisensäure
FI117633B (fi) 2000-12-29 2006-12-29 Chempolis Oy Kemikaalien talteenotto ja valmistus massan valmistuksen yhteydessä
AU2003224812A1 (en) 2002-04-01 2003-10-20 E.I. Du Pont De Nemours And Company Preparation of levulinic acid esters and formic acid esters from biomass and olefins
DE10231891A1 (de) * 2002-07-12 2004-01-22 Basf Ag Zubereitungen, enthaltend Diformiate
BRPI0417599A (pt) 2003-12-15 2007-03-20 Shell Int Research processo para a liquefação de material lignocelulósico ou celulósico
US7378549B2 (en) 2004-01-26 2008-05-27 Shell Oil Company Process for the reactive extractive extraction of levulinic acid
MY158458A (en) 2005-04-13 2016-10-14 Basf Ag Sodium diformate production and use
CN1850770A (zh) * 2006-05-20 2006-10-25 杨淑梅 甲酸钾生产新工艺
CN100522917C (zh) * 2007-03-09 2009-08-05 浙江大学 一种用活性炭分离乙酰丙酸的方法
FI121541B (fi) 2008-04-21 2010-12-31 Kemira Oyj Menetelmä muurahaishapon talteenottamiseksi

Also Published As

Publication number Publication date
CA2721165A1 (en) 2009-10-29
US20110098490A1 (en) 2011-04-28
WO2009130387A3 (en) 2010-04-01
FI20085336A0 (fi) 2008-04-21
EP2285766A2 (en) 2011-02-23
CN102026953A (zh) 2011-04-20
CN102015611B (zh) 2014-12-24
US8492586B2 (en) 2013-07-23
US20110137051A1 (en) 2011-06-09
CA2721165C (en) 2016-06-07
CA2721168A1 (en) 2009-10-29
FI20085336A (fi) 2009-10-22
WO2009130386A1 (en) 2009-10-29
EP2291344A1 (en) 2011-03-09
CN102026953B (zh) 2014-07-09
CN102015611A (zh) 2011-04-13
US8530695B2 (en) 2013-09-10
WO2009130387A2 (en) 2009-10-29

Similar Documents

Publication Publication Date Title
FI121541B (fi) Menetelmä muurahaishapon talteenottamiseksi
DK2773437T3 (en) A method and arrangement for separating at least one carboxylic acid, and furfural from dilute aqueous mixture thereof
Bokhary et al. Liquid–liquid extraction technology for resource recovery: Applications, potential, and perspectives
EP2904144B1 (en) Processes for producing cellulose pulp, sugars, and co-products from lignocellulosic biomass
Baktash et al. Production of furfural from an industrial pre-hydrolysis liquor
CN101481307B (zh) 一种从反应产物中分离出乙酸和乙酸仲丁酯的方法
KR20080063349A (ko) 아세트산 탈수 시스템 및 방법
US9656940B2 (en) Process for the recovery of acetic acid
US20130047979A1 (en) Methods for the recovery of hcl and for the production of carbohydrates
EP3114103A1 (en) Energy efficient batch recycle method for the production of biomolecules
CN104926690A (zh) 一种用于头孢曲松钠合成中乙腈的回收精制方法及装置
CN102089292A (zh) 糠基衍生物的氢解方法
US20130331601A1 (en) Method for recovery of organic acid from dilute aqueous solution
CN112694409B (zh) 一种回收废水中三乙胺的方法和装置
CA2942217C (en) A method of hydrolyzing cellulosic materials
CN115181080B (zh) 一种甲基叔丁基醚-四氢呋喃-乙醇-水共沸体系的分离工艺
WO2011141904A1 (en) Viscous carbohydrate compositions and methods for the production thereof

Legal Events

Date Code Title Description
PC Transfer of assignment of patent

Owner name: TAMINCO FINLAND OY

MM Patent lapsed