FI107929B - Menetelmä level-off-DP-selluloosan valmistamiseksi - Google Patents
Menetelmä level-off-DP-selluloosan valmistamiseksi Download PDFInfo
- Publication number
- FI107929B FI107929B FI945856A FI945856A FI107929B FI 107929 B FI107929 B FI 107929B FI 945856 A FI945856 A FI 945856A FI 945856 A FI945856 A FI 945856A FI 107929 B FI107929 B FI 107929B
- Authority
- FI
- Finland
- Prior art keywords
- cellulose
- level
- process according
- pressure
- oxygen
- Prior art date
Links
- 229920002678 cellulose Polymers 0.000 title claims description 83
- 239000001913 cellulose Substances 0.000 title claims description 78
- 238000000034 method Methods 0.000 title claims description 29
- 238000002360 preparation method Methods 0.000 title claims description 5
- 235000010980 cellulose Nutrition 0.000 claims description 70
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 34
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 25
- 229910052760 oxygen Inorganic materials 0.000 claims description 25
- 239000001301 oxygen Substances 0.000 claims description 25
- 238000006243 chemical reaction Methods 0.000 claims description 22
- 230000007062 hydrolysis Effects 0.000 claims description 21
- 238000006460 hydrolysis reaction Methods 0.000 claims description 21
- 239000001569 carbon dioxide Substances 0.000 claims description 17
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 17
- 239000007789 gas Substances 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 238000006116 polymerization reaction Methods 0.000 claims description 9
- 229920000168 Microcrystalline cellulose Polymers 0.000 claims description 2
- 150000004676 glycans Chemical class 0.000 claims description 2
- 235000019813 microcrystalline cellulose Nutrition 0.000 claims description 2
- 239000008108 microcrystalline cellulose Substances 0.000 claims description 2
- 229940016286 microcrystalline cellulose Drugs 0.000 claims description 2
- 229920001282 polysaccharide Polymers 0.000 claims description 2
- 239000005017 polysaccharide Substances 0.000 claims description 2
- 239000007900 aqueous suspension Substances 0.000 claims 1
- 239000000243 solution Substances 0.000 description 11
- 239000012467 final product Substances 0.000 description 10
- 239000000047 product Substances 0.000 description 8
- 230000035484 reaction time Effects 0.000 description 7
- 239000007795 chemical reaction product Substances 0.000 description 6
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 150000003839 salts Chemical class 0.000 description 3
- 238000012546 transfer Methods 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000011780 sodium chloride Substances 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 description 1
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- 241000218631 Coniferophyta Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 241000238557 Decapoda Species 0.000 description 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 1
- 229920000875 Dissolving pulp Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 229920002488 Hemicellulose Polymers 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 241000208202 Linaceae Species 0.000 description 1
- 235000004431 Linum usitatissimum Nutrition 0.000 description 1
- 241000218657 Picea Species 0.000 description 1
- 229920000297 Rayon Polymers 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Inorganic materials [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 235000009120 camo Nutrition 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 235000005607 chanvre indien Nutrition 0.000 description 1
- 238000005352 clarification Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 239000011487 hemp Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000012452 mother liquor Substances 0.000 description 1
- 238000013386 optimize process Methods 0.000 description 1
- 239000010815 organic waste Substances 0.000 description 1
- 230000004792 oxidative damage Effects 0.000 description 1
- 235000011837 pasties Nutrition 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002964 rayon Substances 0.000 description 1
- 239000004627 regenerated cellulose Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000011122 softwood Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B15/00—Preparation of other cellulose derivatives or modified cellulose, e.g. complexes
- C08B15/02—Oxycellulose; Hydrocellulose; Cellulosehydrate, e.g. microcrystalline cellulose
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE4342442 | 1993-12-13 | ||
| DE4342442A DE4342442C2 (de) | 1993-12-13 | 1993-12-13 | Verfahren zur Herstellung von Level-off DP Cellulose (LODP Cellulose) und ihre Desaggregierung zu mikrokristalliner Cellulose |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| FI945856A0 FI945856A0 (fi) | 1994-12-13 |
| FI945856L FI945856L (fi) | 1995-06-14 |
| FI107929B true FI107929B (fi) | 2001-10-31 |
Family
ID=6504864
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FI945856A FI107929B (fi) | 1993-12-13 | 1994-12-13 | Menetelmä level-off-DP-selluloosan valmistamiseksi |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US5543511A (cs) |
| EP (1) | EP0657472A1 (cs) |
| JP (1) | JPH07206901A (cs) |
| BR (1) | BR9404978A (cs) |
| CA (1) | CA2137890A1 (cs) |
| DE (1) | DE4342442C2 (cs) |
| FI (1) | FI107929B (cs) |
| TW (1) | TW267172B (cs) |
Families Citing this family (36)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6306334B1 (en) | 1996-08-23 | 2001-10-23 | The Weyerhaeuser Company | Process for melt blowing continuous lyocell fibers |
| US6471727B2 (en) | 1996-08-23 | 2002-10-29 | Weyerhaeuser Company | Lyocell fibers, and compositions for making the same |
| US6331354B1 (en) | 1996-08-23 | 2001-12-18 | Weyerhaeuser Company | Alkaline pulp having low average degree of polymerization values and method of producing the same |
| US5769934A (en) * | 1997-01-15 | 1998-06-23 | Fmc Corporation | Method for producing microcrystalline cellulose |
| EP1082348A1 (en) * | 1998-05-14 | 2001-03-14 | Kemestrie Inc. | Process for preparing a high purity chemical-free microcrystalline cellulose from a chemically produced cellulose |
| US6773648B2 (en) | 1998-11-03 | 2004-08-10 | Weyerhaeuser Company | Meltblown process with mechanical attenuation |
| AU766766C (en) * | 1999-07-02 | 2005-09-22 | J. Rettenmaier & Soehne Gmbh + Co. Kg | Treatment of pulp to produce microcrystalline cellulose |
| CA2427397A1 (en) * | 2000-11-03 | 2002-05-10 | Kemestrie Inc. | Process for producing low dp microcrystalline cellulose |
| DE10209812A1 (de) * | 2001-03-22 | 2002-09-26 | Degussa Construction Chem Gmbh | Verwendung von wasserlöslichen Polysaccharid-Derivaten als Dispergiermittel für mineralische Bindemittelsuspensionen |
| KR20050025637A (ko) * | 2002-07-26 | 2005-03-14 | 에프엠씨 코포레이션 | 미세결정 셀룰로스의 제조방법 |
| US7005514B2 (en) * | 2002-10-16 | 2006-02-28 | International Paper Company | Process for preparing microcrystalline cellulose |
| US7037405B2 (en) * | 2003-05-14 | 2006-05-02 | International Paper Company | Surface treatment with texturized microcrystalline cellulose microfibrils for improved paper and paper board |
| US7497924B2 (en) * | 2003-05-14 | 2009-03-03 | International Paper Company | Surface treatment with texturized microcrystalline cellulose microfibrils for improved paper and paper board |
| WO2005049869A1 (ja) * | 2003-11-21 | 2005-06-02 | Tama-Tlo Corporation | 有機化合物の加水分解方法 |
| US20050239744A1 (en) * | 2004-04-22 | 2005-10-27 | Michael Ioelovich | Method of producing microcrystalline cellulose-containing compositions |
| JP4651086B2 (ja) * | 2005-03-22 | 2011-03-16 | トヨタ自動車株式会社 | セルロースの分解方法 |
| US7815741B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| US7815876B2 (en) | 2006-11-03 | 2010-10-19 | Olson David A | Reactor pump for catalyzed hydrolytic splitting of cellulose |
| ES2348843B1 (es) | 2009-05-14 | 2011-10-07 | Blanver Farmoquimica Ltda. | Procedimiento para la preparacion de celulosa microcristalina. |
| RU2395636C1 (ru) * | 2009-07-13 | 2010-07-27 | Учреждение Российской академии наук Институт химии и химической технологии Сибирского отделения РАН (ИХХТ СО РАН) | Способ получения микрокристаллической целлюлозы из автогидролизованной древесины |
| FI123270B2 (fi) * | 2010-06-07 | 2019-04-15 | Kemira Oyj | Mikroselluloosan valmistus |
| FI126573B (fi) | 2010-06-07 | 2017-02-28 | Kemira Oyj | Menetelmä mikroselluloosan valmistamiseksi |
| FI126649B (fi) | 2010-06-07 | 2017-03-31 | Aalto Univ Found | Uusi menetelmä mikroselluloosan valmistamiseksi |
| FI126842B (fi) | 2010-06-07 | 2017-06-15 | Aalto Univ Found | Uusi menetelmä mikroselluloosan valmistamiseksi |
| JP6158191B2 (ja) | 2011-10-05 | 2017-07-05 | エフ エム シー コーポレーションＦｍｃ Ｃｏｒｐｏｒａｔｉｏｎ | 共摩耗型の微結晶セルロースおよびカルボキシメチルセルロースの安定化剤組成物、該組成物の製造方法および用途 |
| BR112014007366B1 (pt) | 2011-10-05 | 2020-09-15 | Dupont Nutrition Usa, Inc | Processo para fabricar uma composição estabilizadora compreendendo extrusão em duas etapas, composição estabilizadora de celulose microcristalina e produto alimentício comestível e suspensão industrial compreendendo a mesma |
| BR112014013792B8 (pt) | 2011-12-09 | 2020-11-10 | Dupont Nutrition Usa Inc | composição estabilizadora co-atritada compreendendo carboximetilcelulose de alto grau de substituição e baixa viscosidade, alimento, composição industrial, e, método para fazer a composição estabilizadora |
| CN102617750A (zh) * | 2012-03-07 | 2012-08-01 | 中国科技开发院广西分院 | 一种二氧化碳催化制备微分子右旋糖酐的方法 |
| CN102702361B (zh) * | 2012-05-19 | 2014-03-19 | 吉林大学 | 一种微晶纤维素的酯化改性方法 |
| BR112017009224B8 (pt) | 2014-11-03 | 2022-04-12 | Dupont Nutrition Usa Inc | Estabilizadores eficazes de bebida de proteína vegetal compreendendo celulose microcristalina coloidal fabricada a partir de polpa de celulose não dissolvível |
| BR112017022867B1 (pt) | 2015-05-14 | 2022-07-19 | Dupont Nutrition Usa, Inc | Método para fabricaçao de celulose microcristalina |
| CN108264569B (zh) * | 2017-01-03 | 2020-01-03 | 中国科学院金属研究所 | 一种纤维素ii型纳米晶粒子及其制备方法和应用 |
| WO2022125895A1 (en) | 2020-12-11 | 2022-06-16 | Dupont Nutrition Biosciences Aps | Microcrystalline cellulose, compositions, methods of making the same and food products comprising them |
| CN116829133A (zh) | 2021-01-13 | 2023-09-29 | 营养与生物科学美国1有限责任公司 | 用于制备微晶纤维素的改善方法 |
| EP4277948A1 (en) | 2021-01-13 | 2023-11-22 | Nutrition & Biosciences USA 1, LLC | Improved method for the preparation of colloidal microcrystalline cellulose |
| WO2023094048A1 (en) | 2021-11-24 | 2023-06-01 | Nutrition & Biosciences Usa 1, Llc | Process for producing microcrystalline cellulose with reduced nitrite salt content |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL224413A (cs) * | 1957-01-28 | |||
| US3278519A (en) * | 1960-05-06 | 1966-10-11 | Fmc Corp | Formed products of cellulose crystallite aggregates |
| US3012914A (en) * | 1960-11-14 | 1961-12-12 | American Viscose Corp | Reconstituted tobacco products and method of manufacture |
| US3141875A (en) * | 1961-03-15 | 1964-07-21 | Fmc Corp | Crystallite aggregates disintegrated in acid medium |
| US3146168A (en) * | 1962-04-10 | 1964-08-25 | Fmc Corp | Manufacture of pharmaceutical preparations containing cellulose crystallite aggregates |
| SU767124A1 (ru) * | 1978-07-31 | 1980-09-30 | Сибирский технологический институт | Способ определени фракционного состава целлюлозы |
| CA1198703A (en) * | 1984-08-02 | 1985-12-31 | Edward A. De Long | Method of producing level off d p microcrystalline cellulose and glucose from lignocellulosic material |
| DD245823A1 (de) * | 1986-01-22 | 1987-05-20 | Zellstoff Und Papier Stammbetr | Verfahren zur kontinuierlichen durchfuehrung von technologischen prozessen unter erhoehtem druck |
| DE3618377A1 (de) * | 1986-05-31 | 1987-12-03 | Wolff Walsrode Ag | Verfahren zur herstellung von mikrokristalliner cellulose |
| RU1796632C (ru) * | 1990-05-29 | 1993-02-23 | Советско-Шведское Совместное Предприятие "Техноферм - Инжиниринг" | Способ получени порошковой целлюлозы |
-
1993
- 1993-12-13 DE DE4342442A patent/DE4342442C2/de not_active Expired - Fee Related
-
1994
- 1994-12-06 EP EP94119200A patent/EP0657472A1/de not_active Withdrawn
- 1994-12-08 TW TW083111415A patent/TW267172B/zh active
- 1994-12-12 JP JP6308014A patent/JPH07206901A/ja active Pending
- 1994-12-12 CA CA002137890A patent/CA2137890A1/en not_active Abandoned
- 1994-12-12 US US08/354,788 patent/US5543511A/en not_active Expired - Fee Related
- 1994-12-13 BR BR9404978A patent/BR9404978A/pt not_active Application Discontinuation
- 1994-12-13 FI FI945856A patent/FI107929B/fi active
Also Published As
| Publication number | Publication date |
|---|---|
| DE4342442A1 (de) | 1995-06-14 |
| FI945856A0 (fi) | 1994-12-13 |
| DE4342442C2 (de) | 1996-11-21 |
| BR9404978A (pt) | 1995-08-08 |
| EP0657472A1 (de) | 1995-06-14 |
| US5543511A (en) | 1996-08-06 |
| FI945856L (fi) | 1995-06-14 |
| JPH07206901A (ja) | 1995-08-08 |
| TW267172B (cs) | 1996-01-01 |
| CA2137890A1 (en) | 1995-06-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GB | Transfer or assigment of application |
Owner name: MANFRED BERGFELD |