FI104824B - Förfarande för att åstadkomma propenterpolymerer - Google Patents

Förfarande för att åstadkomma propenterpolymerer Download PDF

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Publication number
FI104824B
FI104824B FI972714A FI972714A FI104824B FI 104824 B FI104824 B FI 104824B FI 972714 A FI972714 A FI 972714A FI 972714 A FI972714 A FI 972714A FI 104824 B FI104824 B FI 104824B
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FI
Finland
Prior art keywords
weight
gas phase
propylene
reactor
process according
Prior art date
Application number
FI972714A
Other languages
English (en)
Finnish (fi)
Other versions
FI972714A0 (fi
FI972714A (sv
Inventor
Kauno Alastalo
Bo Malm
Paeivi Pitkaenen
Mika Meller
Original Assignee
Borealis As
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=8549114&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=FI104824(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Borealis As filed Critical Borealis As
Priority to FI972714A priority Critical patent/FI104824B/sv
Publication of FI972714A0 publication Critical patent/FI972714A0/fi
Priority to BR9810625-2A priority patent/BR9810625A/pt
Priority to PCT/GB1998/001843 priority patent/WO1998059002A1/en
Priority to JP50385699A priority patent/JP2002504956A/ja
Priority to ZA985489A priority patent/ZA985489B/xx
Priority to KR1019997012298A priority patent/KR100551509B1/ko
Priority to ARP980103030A priority patent/AR013126A1/es
Priority to JP50401399A priority patent/JP4037468B2/ja
Priority to CNB988065789A priority patent/CN1200969C/zh
Priority to BR9810290-7A priority patent/BR9810290A/pt
Priority to KR1019997012176A priority patent/KR100556167B1/ko
Priority to ES98929463T priority patent/ES2209155T3/es
Priority to EP98929463A priority patent/EP0991679B1/en
Priority to AU81211/98A priority patent/AU8121198A/en
Priority to DE69820060T priority patent/DE69820060T2/de
Priority to AT98930935T priority patent/ATE256714T1/de
Priority to US09/446,503 priority patent/US6365682B1/en
Priority to MYPI98002885A priority patent/MY120993A/en
Priority to AT98929463T priority patent/ATE255134T1/de
Priority to PCT/FI1998/000556 priority patent/WO1998058971A1/en
Priority to CN98808290A priority patent/CN1107084C/zh
Priority to EP98930935A priority patent/EP0991719B1/en
Priority to ES98930935T priority patent/ES2209159T3/es
Priority to DE69820626T priority patent/DE69820626T2/de
Priority to US09/446,719 priority patent/US6342564B1/en
Priority to AU79213/98A priority patent/AU726669B2/en
Priority to TW087113335A priority patent/TW562812B/zh
Publication of FI972714A publication Critical patent/FI972714A/sv
Publication of FI104824B publication Critical patent/FI104824B/sv
Application granted granted Critical
Priority to US10/036,728 priority patent/US6552149B2/en

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F297/00—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer
    • C08F297/06—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type
    • C08F297/08—Macromolecular compounds obtained by successively polymerising different monomer systems using a catalyst of the ionic or coordination type without deactivating the intermediate polymer using a catalyst of the coordination type polymerising mono-olefins
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/2435—Loop-type reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • B01J8/26—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique with two or more fluidised beds, e.g. reactor and regeneration installations
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F10/00—Homopolymers and copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F10/04—Monomers containing three or four carbon atoms
    • C08F10/06—Propene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F2/00—Processes of polymerisation
    • C08F2/34—Polymerisation in gaseous state
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F210/04—Monomers containing three or four carbon atoms
    • C08F210/06—Propene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F210/00—Copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond
    • C08F210/16—Copolymers of ethene with alpha-alkenes, e.g. EP rubbers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00121—Controlling the temperature by direct heating or cooling
    • B01J2219/00128—Controlling the temperature by direct heating or cooling by evaporation of reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00184—Controlling or regulating processes controlling the weight of reactants in the reactor vessel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S526/905—Polymerization in presence of transition metal containing catalyst in presence of hydrogen
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S526/00—Synthetic resins or natural rubbers -- part of the class 520 series
    • Y10S526/916—Interpolymer from at least three ethylenically unsaturated monoolefinic hydrocarbon monomers

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Polymerisation Methods In General (AREA)

Claims (11)

1. Förfarande för producering av terpolymerer med en läg smälttemperatur med minst tvä olika α-olefiner minst i en 5 suspensionsreaktor i närvaro av katalysatorer vid en förhöjad temperatur kännetecknat av att det omfattar stegen, väri: a) in i suspensionsreaktoren mätäs en reaktionsblandning, vilken innehäller 50 - 85 vikt-% propen, 1-10 vikt-% eten, 15-40 vikt-% en io annan C4-C8a-olefin, ett katalysatorsystem, vilket underhäller olefinens polymerisering under nämnda temperaturförhällanden, och eventuellt väte, b) nämnda reaktionsblandning polymeriseras vid en temperatur under 70 15 °C tillräckligt länge, varvid terpolymer av propen erhälls, vars mängd stiger upp tili 50 - 99 vikt-% av slutprodukten, c) nämnda reaktionsblandning överförs tili en gasfasreaktor, som . fungerar vid ett tryck over 5 bar, företrädesvis över 10 bar, eventuellt 20 tillsätts 0 - 30 vikt-% eten, 0-10 vikt-% en annan C4 - C8 α-olefin, 0 -_ 40 vikt-% propen och eventuellt väte, och I « * d) polymeriseringen fortsätts i nämnda gasfasreaktor för att erhälla • · · v : terpolymer av propen med en smälttemperatur under 135 °C, 25 företrädesvis under 132 °C, och vars mängd stiger upp tili 1 - 50 vikt-% • · • · I *·*;* av slutprodukten. • · · I · » » • · i
*' 2. Förfarande enligt patentkrav 1, kännetecknat av att nämnda C4 - C8 a- • « ’·;·* olefin är 1-buten, 1-penten, 4-metyl-1-penten, 1-heksen, 1-hepten eller \i.: 30 1-okten eller blandning av dessa. • · 14 104824
3. Förfarande enligt patentkrav 1 eller 2, kännetecknat av att nämnda suspensionsreaktor är en loop-reaktor.
4. Förfarande enligt nägot av patentkraven 1 - 3, kännetecknat av att 5 nämnda steg a) utförs i tvä suspensionsreaktorer, företrädesvis i tvä loop-reaktorer.
5. Förfarande enligt nägot av patentkraven 1 - 4, kännetecknat av att 0-40 vikt-% propen tillsätts tili gasfasreaktoren. 10
6. Förfarande enligt nägot av patentkraven 1 - 5, kännetecknat av att 0-40 vikt-% eten tillsätts tili gasfasreaktoren.
7. Förfarande enligt nägot av patentkraven 1 - 6, kännetecknat av att 0- 15 10 vikt-% 1-buten tillsätts tili gasfasreaktoren.
8. Förfarande enligt nägot av patentkraven 1 - 5, kännetecknat av att en skild α-olefin används i loop-reaktoren och gasfasreaktoren. • « 20
9. Förfarande enligt nägot av patentkraven 1-5, kännetecknat av att t I bara eten och propen används som tilläggsmonomerer i gasfasreaktoren. * · • I I • Il • ·
10. Förfarande enligt nägot av patentkraven 1 - 9, kännetecknat av att • 1 · v : uppehällstiden i gasfasreaktoren är 1 - 180 min. 25 • · v.:
11. Produkter, vilka produceras enligt förfarandet av nägot av ··· • · · patentkraven 1 - 10 för värmeförseglingsfilmer och - skivor, formade ·· • 1·· skivor, lock, flaskor, fibrer osv. • · · • · • « • · · : 30 • · · ·
FI972714A 1997-06-24 1997-06-24 Förfarande för att åstadkomma propenterpolymerer FI104824B (sv)

Priority Applications (28)

Application Number Priority Date Filing Date Title
FI972714A FI104824B (sv) 1997-06-24 1997-06-24 Förfarande för att åstadkomma propenterpolymerer
AU79213/98A AU726669B2 (en) 1997-06-24 1998-06-24 Propylene terpolymers and a process for the production thereof
AU81211/98A AU8121198A (en) 1997-06-24 1998-06-24 Heterophasic propylene copolymer and process for its preparation
US09/446,503 US6365682B1 (en) 1997-06-24 1998-06-24 Process for the production of propylene terpolymers
JP50385699A JP2002504956A (ja) 1997-06-24 1998-06-24 プロピレンターポリマーおよびその製造方法
ZA985489A ZA985489B (en) 1997-06-24 1998-06-24 Propylene terpolymers and a process for the production thereof
KR1019997012298A KR100551509B1 (ko) 1997-06-24 1998-06-24 프로필렌 삼원공중합체 및 이들의 제조 방법
ARP980103030A AR013126A1 (es) 1997-06-24 1998-06-24 Terpolimeros de propileno y un proceso para la produccion de los mismos
JP50401399A JP4037468B2 (ja) 1997-06-24 1998-06-24 プロピレンを含む異相ポリマーの製造方法
CNB988065789A CN1200969C (zh) 1997-06-24 1998-06-24 多相丙烯共聚物的制备工艺
BR9810290-7A BR9810290A (pt) 1997-06-24 1998-06-24 Copolìmero polipropileno heterofásico, processo para a preparação do mesmo, e, uso de um polìmero.
KR1019997012176A KR100556167B1 (ko) 1997-06-24 1998-06-24 불균일상 프로필렌 공중합체 및 그의 제조 방법
ES98929463T ES2209155T3 (es) 1997-06-24 1998-06-24 Termopolimeros de propileno y procedimiento para su fabricacion.
EP98929463A EP0991679B1 (en) 1997-06-24 1998-06-24 Propylene terpolymers and a process for the production thereof
BR9810625-2A BR9810625A (pt) 1997-06-24 1998-06-24 Terpolìmeros de propileno e processo para sua produção
DE69820060T DE69820060T2 (de) 1997-06-24 1998-06-24 Filmbildendes Terpolymer aus Propylen sowie Verfahren zur Herstellung solcher Terpolymere
AT98930935T ATE256714T1 (de) 1997-06-24 1998-06-24 Verfahren zur herstellung von heterophasigem propylencopolymer
PCT/GB1998/001843 WO1998059002A1 (en) 1997-06-24 1998-06-24 Heterophasic propylene copolymer and process for its preparation
MYPI98002885A MY120993A (en) 1997-06-24 1998-06-24 Process for the production of propylene terpolymers
AT98929463T ATE255134T1 (de) 1997-06-24 1998-06-24 Propylenterpolymere und ein verfahren zur herstellung
PCT/FI1998/000556 WO1998058971A1 (en) 1997-06-24 1998-06-24 Propylene terpolymers and a process for the production thereof
CN98808290A CN1107084C (zh) 1997-06-24 1998-06-24 丙烯三元共聚物及其制备方法
EP98930935A EP0991719B1 (en) 1997-06-24 1998-06-24 Process for the preparation of heterophasic propylene copolymer
ES98930935T ES2209159T3 (es) 1997-06-24 1998-06-24 Procedimiento para la preparacion de copolimero de propileno heterofasico.
DE69820626T DE69820626T2 (de) 1997-06-24 1998-06-24 Verfahren zur herstellung von heterophasigem propylencopolymer
US09/446,719 US6342564B1 (en) 1997-06-24 1998-06-24 Heterophasic propylene copolymer and process for its preparation
TW087113335A TW562812B (en) 1997-06-24 1998-08-13 Propylene terpolymers and a process for the production thereof
US10/036,728 US6552149B2 (en) 1997-06-24 2001-12-21 Propylene terpolymers

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI972714A FI104824B (sv) 1997-06-24 1997-06-24 Förfarande för att åstadkomma propenterpolymerer
FI972714 1997-06-24

Publications (3)

Publication Number Publication Date
FI972714A0 FI972714A0 (fi) 1997-06-24
FI972714A FI972714A (sv) 1998-12-25
FI104824B true FI104824B (sv) 2000-04-14

Family

ID=8549114

Family Applications (1)

Application Number Title Priority Date Filing Date
FI972714A FI104824B (sv) 1997-06-24 1997-06-24 Förfarande för att åstadkomma propenterpolymerer

Country Status (16)

Country Link
US (2) US6365682B1 (sv)
EP (1) EP0991679B1 (sv)
JP (1) JP2002504956A (sv)
KR (1) KR100551509B1 (sv)
CN (1) CN1107084C (sv)
AR (1) AR013126A1 (sv)
AT (1) ATE255134T1 (sv)
AU (1) AU726669B2 (sv)
BR (1) BR9810625A (sv)
DE (1) DE69820060T2 (sv)
ES (1) ES2209155T3 (sv)
FI (1) FI104824B (sv)
MY (1) MY120993A (sv)
TW (1) TW562812B (sv)
WO (1) WO1998058971A1 (sv)
ZA (1) ZA985489B (sv)

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BR112016002682A8 (pt) 2013-08-21 2020-01-28 Borealis Ag composição de poliolefina de alto fluxo com alta rigidez e tenacidade
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US20020082376A1 (en) 2002-06-27
KR20010020516A (ko) 2001-03-15
FI972714A0 (fi) 1997-06-24
KR100551509B1 (ko) 2006-02-13
WO1998058971A1 (en) 1998-12-30
DE69820060D1 (de) 2004-01-08
CN1107084C (zh) 2003-04-30
US6552149B2 (en) 2003-04-22
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JP2002504956A (ja) 2002-02-12
CN1267310A (zh) 2000-09-20
FI972714A (sv) 1998-12-25
ATE255134T1 (de) 2003-12-15
MY120993A (en) 2005-12-30
DE69820060T2 (de) 2004-07-22
TW562812B (en) 2003-11-21
AU726669B2 (en) 2000-11-16
ES2209155T3 (es) 2004-06-16
AU7921398A (en) 1999-01-04
EP0991679B1 (en) 2003-11-26
US6365682B1 (en) 2002-04-02
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AR013126A1 (es) 2000-12-13

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