ES8603495A1 - Un procedimiento para recuperar ceftazidima a partir de una solucion acuosa que la contiene - Google Patents
Un procedimiento para recuperar ceftazidima a partir de una solucion acuosa que la contieneInfo
- Publication number
- ES8603495A1 ES8603495A1 ES541085A ES541085A ES8603495A1 ES 8603495 A1 ES8603495 A1 ES 8603495A1 ES 541085 A ES541085 A ES 541085A ES 541085 A ES541085 A ES 541085A ES 8603495 A1 ES8603495 A1 ES 8603495A1
- Authority
- ES
- Spain
- Prior art keywords
- ceftazidime
- recovering
- solution
- eluting
- adsorbing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D501/00—Heterocyclic compounds containing 5-thia-1-azabicyclo [4.2.0] octane ring systems, i.e. compounds containing a ring system of the formula:, e.g. cephalosporins; Such ring systems being further condensed, e.g. 2,3-condensed with an oxygen-, nitrogen- or sulfur-containing hetero ring
- C07D501/14—Compounds having a nitrogen atom directly attached in position 7
- C07D501/16—Compounds having a nitrogen atom directly attached in position 7 with a double bond between positions 2 and 3
- C07D501/20—7-Acylaminocephalosporanic or substituted 7-acylaminocephalosporanic acids in which the acyl radicals are derived from carboxylic acids
- C07D501/24—7-Acylaminocephalosporanic or substituted 7-acylaminocephalosporanic acids in which the acyl radicals are derived from carboxylic acids with hydrocarbon radicals, substituted by hetero atoms or hetero rings, attached in position 3
- C07D501/38—Methylene radicals, substituted by nitrogen atoms; Lactams thereof with the 2-carboxyl group; Methylene radicals substituted by nitrogen-containing hetero rings attached by the ring nitrogen atom; Quaternary compounds thereof
- C07D501/46—Methylene radicals, substituted by nitrogen atoms; Lactams thereof with the 2-carboxyl group; Methylene radicals substituted by nitrogen-containing hetero rings attached by the ring nitrogen atom; Quaternary compounds thereof with the 7-amino radical acylated by carboxylic acids containing hetero rings
Abstract
PROCEDIMIENTO PARA RECUPERAR CEFTAZIDIMA A PARTIR DE UNA SOLUCION ACUOSA QUE LA CONTIENE. COMPRENDE: A) PONER EN CONTACTO UNA SOLUCION ACUOSA QUE CONTIENE CEFTAZIDIMA Y QUE TIENE UN PH EN EL INTERVALO DE 2,0 A 5,5, CON UNA RESINA MACRORRETICULAR NO FUNCIONAL QUE ES UN COPOLIMERO DE ESTIRENO RETICULADO CON DIVINIL-BENCENO Y CON UNA SUPERFICIE ESPECIFICA DE 200 A 1.200 M/G Y UN DIAMETRO MEDIO DE POROS DE 2 A 18 MM, PARA ADSORBER CEFTAZIDIMA; B) ELUDIR LA CEFTAZIDIMA EMPLEANDO UNO O MAS DISOLVENTES ORGANICOS MISCIBLES CON AGUA MEZCLADOS CON AGUA, SELECCIONADOS ENTRE CETONAS, ETERES, ESTERES, NITRILOS Y ALCOHOLES COMPRENDIENDO DEL 5 AL 50% DEL VOLUMEN TOTAL DEL ELUYENTE; Y C) AISLAR LA CEFTAZIDIMA EN FORMA DE UNA SAL O UN HIDRATO. SIENDO LA CONCENTRACION DE CEFTAZIDIMA EN DICHA SOLUCION ACUOSA PUESTA EN CONTACTO CON LA RESINA, INFERIOR AL 10% EN PESO.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB848406218A GB8406218D0 (en) | 1984-03-09 | 1984-03-09 | Process |
Publications (2)
Publication Number | Publication Date |
---|---|
ES8603495A1 true ES8603495A1 (es) | 1985-12-16 |
ES541085A0 ES541085A0 (es) | 1985-12-16 |
Family
ID=10557840
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES541085A Granted ES541085A0 (es) | 1984-03-09 | 1985-03-08 | Un procedimiento para recuperar ceftazidima a partir de una solucion acuosa que la contiene |
Country Status (22)
Country | Link |
---|---|
US (1) | US4769450A (es) |
JP (1) | JPH0645626B2 (es) |
KR (1) | KR890001010B1 (es) |
AT (1) | AT386206B (es) |
AU (1) | AU581427B2 (es) |
BE (1) | BE901900A (es) |
CA (1) | CA1239391A (es) |
CH (1) | CH664156A5 (es) |
DE (1) | DE3508372C2 (es) |
DK (1) | DK157028C (es) |
ES (1) | ES541085A0 (es) |
FI (1) | FI85488C (es) |
FR (1) | FR2560879B1 (es) |
GB (2) | GB8406218D0 (es) |
IE (1) | IE57953B1 (es) |
IL (1) | IL74456A (es) |
IT (1) | IT1182717B (es) |
NL (1) | NL194238C (es) |
NZ (1) | NZ211363A (es) |
PT (1) | PT80081B (es) |
SE (1) | SE466206B (es) |
ZA (1) | ZA851767B (es) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4954624A (en) * | 1986-10-07 | 1990-09-04 | Sandoz Ltd. | Process for the production of cephalosporin derivatives |
TW553946B (en) * | 1999-09-08 | 2003-09-21 | Fujisawa Pharmaceutical Co | Method for separating lactone-containing high-molecular weight compounds |
EP1312387B1 (en) * | 2000-08-25 | 2014-05-21 | Kaneka Corporation | Method for removal of bacterial toxins from a bacterial toxin-containing fluid |
US6780442B2 (en) * | 2000-08-31 | 2004-08-24 | Hauser, Inc. | Efficient method for producing compositions enriched in anthocyanins |
CN102924483B (zh) * | 2012-10-31 | 2015-06-17 | 海南合瑞制药股份有限公司 | 一种头孢他啶晶体化合物、其制备方法及其无菌混合粉形式的药物组合物 |
CN102875576A (zh) * | 2012-10-31 | 2013-01-16 | 苏州致君万庆药业有限公司 | 一种抗菌素头孢他啶的合成、注射用头孢他啶及其制备方法 |
CN110857308B (zh) * | 2018-08-24 | 2021-02-26 | 浙江长典医药有限公司 | 一种注射用头孢他啶的制备方法 |
CN111196818A (zh) * | 2018-11-19 | 2020-05-26 | 浙江长典医药有限公司 | 一种注射用头孢他啶的制备方法 |
CN109824698B (zh) * | 2019-01-23 | 2020-09-22 | 华北制药河北华民药业有限责任公司 | 一种头孢他啶的制备方法 |
CN111116611B (zh) * | 2019-11-21 | 2021-05-07 | 华北制药河北华民药业有限责任公司 | 一种注射用头孢他啶粉针制剂的制备方法 |
CN113101274B (zh) * | 2021-03-31 | 2022-09-06 | 海南海灵化学制药有限公司 | 一种注射用头孢他啶粉针剂及其制备工艺 |
CN114047271B (zh) * | 2021-11-12 | 2023-03-17 | 海南葫芦娃药业集团股份有限公司 | 一种注射用头孢他啶制剂中有关物质的检测方法 |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH541579A (de) * | 1969-05-13 | 1973-09-15 | Ciba Geigy Ag | Verfahren zur Abtrennung von Cephalosporin C aus Rohlösungen |
BE824028A (fr) * | 1974-01-23 | 1975-06-30 | Procede pour la purification de cephalosporines comportant un groupe acide carboxylique libre | |
AR229883A1 (es) * | 1978-05-26 | 1983-12-30 | Glaxo Group Ltd | Procedimiento para la preparacion de antibiotico(6r,7r)-7-((z)-2-(2-aminotiazol-4-il)-2-(2-carboxiprop-2-oxiimino)-acetamido)-3-(1-piridinometil)-cef-3-em-4-carboxilato |
GB2058791B (en) * | 1978-05-26 | 1982-11-24 | Glaxo Group Ltd | Cephalosporin antibiotics |
US4329453A (en) * | 1979-10-02 | 1982-05-11 | Glaxo Group Limited | Cephalosporin antibiotic |
US4427677A (en) * | 1980-12-31 | 1984-01-24 | Fujisawa Pharmaceutical Co., Ltd. | Cephem compounds |
DE3313818A1 (de) * | 1983-04-16 | 1984-10-18 | Hoechst Ag, 6230 Frankfurt | Neue kristallmodifikation von ceftazidim |
US4537959A (en) * | 1984-03-26 | 1985-08-27 | Eli Lilly And Company | Crystalline cephalosporin antibiotic salt |
US4616080A (en) * | 1984-07-02 | 1986-10-07 | Eli Lilly And Company | Simplified process of forming crystalline ceftazidime pentahydrate |
US4659813A (en) * | 1984-11-08 | 1987-04-21 | Eli Lilly And Company | Crystallization process for ceftazidime derivative |
-
1984
- 1984-03-09 GB GB848406218A patent/GB8406218D0/en active Pending
-
1985
- 1985-02-27 IL IL74456A patent/IL74456A/xx not_active IP Right Cessation
- 1985-03-07 CH CH1042/85A patent/CH664156A5/de not_active IP Right Cessation
- 1985-03-08 GB GB08506053A patent/GB2157682B/en not_active Expired
- 1985-03-08 ES ES541085A patent/ES541085A0/es active Granted
- 1985-03-08 CA CA000476038A patent/CA1239391A/en not_active Expired
- 1985-03-08 DK DK106585A patent/DK157028C/da not_active IP Right Cessation
- 1985-03-08 BE BE0/214620A patent/BE901900A/fr not_active IP Right Cessation
- 1985-03-08 FR FR8503451A patent/FR2560879B1/fr not_active Expired
- 1985-03-08 AU AU39670/85A patent/AU581427B2/en not_active Ceased
- 1985-03-08 JP JP60044965A patent/JPH0645626B2/ja not_active Expired - Lifetime
- 1985-03-08 AT AT0070185A patent/AT386206B/de not_active IP Right Cessation
- 1985-03-08 SE SE8501170A patent/SE466206B/sv not_active IP Right Cessation
- 1985-03-08 NL NL8500663A patent/NL194238C/nl not_active IP Right Cessation
- 1985-03-08 KR KR1019850001497A patent/KR890001010B1/ko not_active IP Right Cessation
- 1985-03-08 PT PT80081A patent/PT80081B/pt not_active IP Right Cessation
- 1985-03-08 IE IE608/85A patent/IE57953B1/en not_active IP Right Cessation
- 1985-03-08 DE DE3508372A patent/DE3508372C2/de not_active Expired - Fee Related
- 1985-03-08 IT IT47786/85A patent/IT1182717B/it active
- 1985-03-08 FI FI850926A patent/FI85488C/fi not_active IP Right Cessation
- 1985-03-08 ZA ZA851767A patent/ZA851767B/xx unknown
- 1985-03-08 NZ NZ211363A patent/NZ211363A/xx unknown
-
1987
- 1987-06-18 US US07/063,315 patent/US4769450A/en not_active Expired - Lifetime
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