ES2160299T3 - Procedimiento para la obtencion de isoforona. - Google Patents

Procedimiento para la obtencion de isoforona.

Info

Publication number
ES2160299T3
ES2160299T3 ES97400120T ES97400120T ES2160299T3 ES 2160299 T3 ES2160299 T3 ES 2160299T3 ES 97400120 T ES97400120 T ES 97400120T ES 97400120 T ES97400120 T ES 97400120T ES 2160299 T3 ES2160299 T3 ES 2160299T3
Authority
ES
Spain
Prior art keywords
sub
sup
isoforona
procedure
obtaining
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES97400120T
Other languages
English (en)
Inventor
Remy Teissier
Jacques Kervennal
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Atofina SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Atofina SA filed Critical Atofina SA
Application granted granted Critical
Publication of ES2160299T3 publication Critical patent/ES2160299T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/20—Unsaturated compounds containing keto groups bound to acyclic carbon atoms
    • C07C49/203—Unsaturated compounds containing keto groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/10—Magnesium; Oxides or hydroxides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/74—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups combined with dehydration
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/587—Unsaturated compounds containing a keto groups being part of a ring
    • C07C49/603—Unsaturated compounds containing a keto groups being part of a ring of a six-membered ring

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)

Abstract

LA PRESENTE INVENCION SE REFIERE A UN PROCEDIMIENTO DE OBTENCION DE ISOFORONA A PARTIR DE ACETONAS CARACTERIZADO PORQUE SE OPERA (I) EN FASE LIQUIDA EN PRESENCIA DE UN DOBLE OXIDO DE MAGNESIO Y DE ALUMINIOO DE FORMULA MG{SUB,1.X}AL{SUB,X}O{SUB,1+X} O (II) BIEN EN FASE GASEOSA O IEN EN FASE LIQUIDA EN PRESENCIA DE UN CATALIZADOR DE FORMULA GEENRAL (I) [(MG{SUP,2+}){SUB,1X}(AL{SUP,3}){SUB,X}(OH{SUP-}){SUB,2}]{SUP,X+ [)OH{SUP,}){SUB,X}]{SUP,X-} (H{SUB,2}O={SUB,N} (I) CON 0,20 INFERIOR O IGUAL A X INFERIOR O IGUAL A 0,33 Y N INFERIOR A 1.
ES97400120T 1996-02-29 1997-01-21 Procedimiento para la obtencion de isoforona. Expired - Lifetime ES2160299T3 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR9602550A FR2745566B1 (fr) 1996-02-29 1996-02-29 Procede d'obtention d'isophorone

Publications (1)

Publication Number Publication Date
ES2160299T3 true ES2160299T3 (es) 2001-11-01

Family

ID=9489719

Family Applications (1)

Application Number Title Priority Date Filing Date
ES97400120T Expired - Lifetime ES2160299T3 (es) 1996-02-29 1997-01-21 Procedimiento para la obtencion de isoforona.

Country Status (13)

Country Link
US (1) US5849957A (es)
EP (1) EP0792863B1 (es)
JP (1) JP2869392B2 (es)
KR (1) KR100228996B1 (es)
CN (1) CN1065232C (es)
BR (1) BR9701136A (es)
CA (1) CA2198770C (es)
DE (1) DE69705333T2 (es)
ES (1) ES2160299T3 (es)
FR (1) FR2745566B1 (es)
MX (1) MX9701632A (es)
TW (1) TW340837B (es)
ZA (1) ZA971576B (es)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1075379C (zh) * 1998-08-15 2001-11-28 林计嶝 野生九叶绞股蓝复合茶
CN100371400C (zh) * 2004-08-25 2008-02-27 上海新大余氟碳喷涂材料有限公司 用于提高氟碳涂料喷涂质量的添加剂
CN101698147B (zh) * 2009-10-23 2012-01-25 广州大学 一种用于丙酮缩合法制备异佛尔酮的催化剂
DE102010029272A1 (de) 2010-05-25 2011-12-01 Evonik Degussa Gmbh Verfahren zur elektrochemischen Herstellung von Isophoron
DE102010062587A1 (de) 2010-12-08 2012-06-14 Evonik Degussa Gmbh Verfahren zur Herstellung von Isophoron
DE102010062603A1 (de) 2010-12-08 2012-06-14 Evonik Degussa Gmbh Verfahren zur Herstellung von 3-Aminomethyl-3,5,5-trimethylcyclohexylamin
DE102011075777A1 (de) 2011-05-13 2012-11-15 Evonik Degussa Gmbh Verfahren zur Herstellung von Isophoron in Gegenwart mindestens eines Entschäumers in der Abwasserkolonne im Aufarbeitungsteil
CN102258994B (zh) * 2011-05-19 2012-06-20 宁波千衍新材料科技有限公司 一种用于丙酮多相法合成异佛尔酮的催化剂的制备方法
CN102976910A (zh) * 2011-09-05 2013-03-20 张锦碧 一种丙酮合成异佛尔酮的环保简易制备方法
CN104549371B (zh) * 2013-10-22 2016-11-23 中国石油化工股份有限公司 丙酮缩合制异佛尔酮的催化剂及其制备方法
CN103694095A (zh) * 2013-12-31 2014-04-02 张锦碧 一种异佛尔酮的制备方法
CN104941626B (zh) * 2015-06-07 2017-07-07 复旦大学 一种高价态金属离子改性的镁铝复合金属氧化物催化剂及其制备方法
CN106423126B (zh) * 2015-08-12 2018-11-20 中国石油化工股份有限公司 异佛尔酮催化剂及其制备方法
CN106423124B (zh) * 2015-08-12 2018-11-20 中国石油化工股份有限公司 异佛尔酮催化剂和其制备方法
CN106423125B (zh) * 2015-08-12 2018-11-20 中国石油化工股份有限公司 异佛尔酮催化剂
CN112441896B (zh) * 2019-09-03 2023-07-14 万华化学集团股份有限公司 一种丙酮液相缩合制备异佛尔酮的反应工艺
KR102477904B1 (ko) * 2020-10-27 2022-12-15 금호석유화학 주식회사 촉매 성형체, 그 제조방법 및 이를 이용한 환형 케톤의 제조방법

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2399976A (en) * 1943-01-28 1946-05-07 Shell Dev Production of isophorone and related products
US4476324A (en) * 1982-06-02 1984-10-09 Union Carbide Corporation Catalyzed aldol condensations
US4458026A (en) * 1982-06-02 1984-07-03 Union Carbide Corporation Catalysts for aldol condensations
US5153156A (en) * 1989-04-18 1992-10-06 Aristech Chemical Corporation Process for making efficient anionic clay catalyst, catalysts made thereby, and method of making isophorone
US4970191A (en) * 1989-04-18 1990-11-13 Aristech Chemical Corporation Basic mixed oxide
US5055620A (en) * 1989-04-18 1991-10-08 Aristech Chemical Corporation Process for aldol condensation
US5202496A (en) * 1989-04-18 1993-04-13 Aristech Chemical Corporation Method of making isophorne
DE4020838A1 (de) * 1990-06-29 1992-01-02 Henkel Kgaa Verfahren zur aldolisierung von verbindungen mit aktiven wasserstoffatomen
US5254743A (en) * 1992-12-09 1993-10-19 Uop Solid bases as catalysts in aldol condensations
EP0640387A1 (en) * 1993-08-25 1995-03-01 Union Carbide Chemicals & Plastics Technology Corporation Preparation of isophorone using a magnesium/aluminum mixed oxide catalyst

Also Published As

Publication number Publication date
JP2869392B2 (ja) 1999-03-10
ZA971576B (en) 1997-09-09
CN1065232C (zh) 2001-05-02
KR100228996B1 (ko) 1999-11-01
BR9701136A (pt) 1998-09-01
EP0792863B1 (fr) 2001-06-27
JPH09241204A (ja) 1997-09-16
FR2745566B1 (fr) 1998-04-24
DE69705333D1 (de) 2001-08-02
CA2198770A1 (fr) 1997-08-29
FR2745566A1 (fr) 1997-09-05
KR970061839A (ko) 1997-09-12
CN1166481A (zh) 1997-12-03
EP0792863A1 (fr) 1997-09-03
CA2198770C (fr) 2000-07-18
DE69705333T2 (de) 2001-11-08
MX9701632A (es) 1998-04-30
US5849957A (en) 1998-12-15
TW340837B (en) 1998-09-21

Similar Documents

Publication Publication Date Title
ES2160299T3 (es) Procedimiento para la obtencion de isoforona.
AU4934996A (en) Thrombin inhibitors based on the amino acid sequence of hirudin
NZ525575A (en) Silica abrasive dentifrice composition comprising a proteolytic enzyme and a low oil silica abrasive with an oil absorption value of less than 100 cc per 100g silica
AU5779400A (en) Process for the preparation of 3,3-dimethylbutanal
GB0309765D0 (en) A cosmetic or dermopharmaceutical composition comprising an enzyme which is insoluble in an aqueous medium, as well as its uses.
DE69629210D1 (de) Insulinabkömmlinge
MX9605613A (es) Procedimiento para preparar formas anhidras e hidratadas de derivados de piperidina antihistaminica, polimorfos y pseudomorfos de los mismos.
HK1068782A1 (en) Pharmaceutical composition of 2-(4-isobutylphenyl)propionic acid
EP0985690A3 (en) Acrylic acid-maleic acid copolymer (or its salt), its production process and use, and production process for aqueous maleic salt solution with low impurity content
MXPA02012944A (es) Analogos de acido graso para el tratamiento de cancer.
BR0011030A (pt) Composições de cicloporina substancialmente livre de óleo
PL340580A1 (en) Dibenzylidene sorbitol containing antiperspirant
HUP9904302A2 (hu) Aciltranszferáz enzim és az aciltranszferázt kódoló gén
WO2002000615A3 (en) Process for the isolation of lovastatin
WO2002026218A3 (en) Fatty acid analogues for the treatment of proliferative skin disorders
AU6135898A (en) Enzymatic conversion of alpha-hydroxynitriles to the corresponding alpha-hydroxyamides, acids or acid salts
WO1991019734A3 (en) Thrombin inhibitors based on the amino acid sequence of hirudin
KR950702507A (ko) 염화 제이철의 제조방법(process for the preparation of ferric chloride)
BR9805626A (pt) Combinação , composição cosmética, uso de pelo menos um poliol e processo para estabilizar a procisteìna em uma composição doméstica.
WO2002061147A3 (en) Self-complementary molecular probe and methods using it
WO2001035087A3 (en) A gas sensor seal and method of producing same
KR910014122A (ko) 에토포시드-2-디메틸아미노 화합물의 동결건조 제제
TW332199B (en) Process for the preparation of 3-chloropropionic acid
WO2002030387A3 (en) Composition containing oat extract for increased cell renewal rate
AU7028798A (en) Use of 2-methylthiazolidine-2,4-dicarboxylic acid as mucolytic agent

Legal Events

Date Code Title Description
FG2A Definitive protection

Ref document number: 792863

Country of ref document: ES