ES2107923T3 - Procedimiento para la obtencion de cianuros de benzoilo o-substituidos. - Google Patents

Procedimiento para la obtencion de cianuros de benzoilo o-substituidos.

Info

Publication number
ES2107923T3
ES2107923T3 ES96101039T ES96101039T ES2107923T3 ES 2107923 T3 ES2107923 T3 ES 2107923T3 ES 96101039 T ES96101039 T ES 96101039T ES 96101039 T ES96101039 T ES 96101039T ES 2107923 T3 ES2107923 T3 ES 2107923T3
Authority
ES
Spain
Prior art keywords
converted
image
general formula
compound
keto
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES96101039T
Other languages
English (en)
Inventor
Horst Dr Wingert
Bernd Dr Wolf
Remy Dr Benoit
Hubert Dr Sauter
Michael Dr Hepp
Wassilios Dr Grammenos
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE4042272A external-priority patent/DE4042272A1/de
Priority claimed from DE4042271A external-priority patent/DE4042271A1/de
Priority claimed from DE4042273A external-priority patent/DE4042273A1/de
Priority claimed from DE4042280A external-priority patent/DE4042280A1/de
Priority claimed from DE4042283A external-priority patent/DE4042283A1/de
Priority claimed from DE4042282A external-priority patent/DE4042282A1/de
Application filed by BASF SE filed Critical BASF SE
Application granted granted Critical
Publication of ES2107923T3 publication Critical patent/ES2107923T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C317/00Sulfones; Sulfoxides
    • C07C317/24Sulfones; Sulfoxides having sulfone or sulfoxide groups and doubly-bound oxygen atoms bound to the same carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C235/00Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms
    • C07C235/02Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C235/32Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton containing six-membered aromatic rings
    • C07C235/34Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by oxygen atoms having carbon atoms of carboxamide groups bound to acyclic carbon atoms and singly-bound oxygen atoms bound to the same carbon skeleton the carbon skeleton containing six-membered aromatic rings having the nitrogen atoms of the carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/48Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C253/00Preparation of carboxylic acid nitriles
    • C07C253/14Preparation of carboxylic acid nitriles by reaction of cyanides with halogen-containing compounds with replacement of halogen atoms by cyano groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C255/00Carboxylic acid nitriles
    • C07C255/01Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms
    • C07C255/17Carboxylic acid nitriles having cyano groups bound to acyclic carbon atoms containing cyano groups and doubly-bound oxygen atoms bound to the same acyclic carbon skeleton
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/09Preparation of carboxylic acids or their salts, halides or anhydrides from carboxylic acid esters or lactones
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/347Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups
    • C07C51/367Preparation of carboxylic acids or their salts, halides or anhydrides by reactions not involving formation of carboxyl groups by introduction of functional groups containing oxygen only in singly bound form
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C65/00Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
    • C07C65/21Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing ether groups, groups, groups, or groups
    • C07C65/24Compounds having carboxyl groups bound to carbon atoms of six—membered aromatic rings and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups containing ether groups, groups, groups, or groups polycyclic
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/66Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety
    • C07C69/73Esters of carboxylic acids having esterified carboxylic groups bound to acyclic carbon atoms and having any of the groups OH, O—metal, —CHO, keto, ether, acyloxy, groups, groups, or in the acid moiety of unsaturated acids
    • C07C69/738Esters of keto-carboxylic acids or aldehydo-carboxylic acids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Toxicology (AREA)
  • Health & Medical Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Saccharide Compounds (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

PROCEDIMIENTO PARA LA OBTENCION DE BENZOILCIANUROS OSUSTITUIDOS DE FORMULA GENERAL VI, EN LA QUE LOS SUSTITUYENTES Y LOS INDICES TIENEN LOS SIGUIENTES SIGNIFICADOS: X,Y HALOGENO, ALQUILO DE C{SUB,1}-C{SUB,4}, ALCOXI DE C{SUB,1}C{SUB,4} O TRIFLUORMETILO, M UN NUMERO ENTERO DE 0 A 4, DONDE LOS RADICALES X PUEDEN SER DIFERENTES CUANDO EL VALOR DE M ES MAYOR QUE 1, N UN NUMERO ENTERO DE 0 A 3, DONDE LOS RADICALES Y PUEDEN SER DIFERENTES, CUANDO EL VALOR DE N ES MAYOR QUE 1. ESTE PROCEDIMIENTO SE CARACTERIZA PORQUE SE COMBINA UN ACIDO 2FENOXIMETILBENZOICO DE FORMULA GENERAL IV CON FOSGENO O TIONILCLORURO OBTENIENDOSE EL CORRESPONDIENTE CLORURO DE BENZOILO O-SUSTITUIDO DE FORMULA GENERAL V, Y FINALMENTE V SE COMBINA CON UN CIANURO DE METAL ALCALINO O ALCALINOTERREO.
ES96101039T 1990-12-31 1991-12-10 Procedimiento para la obtencion de cianuros de benzoilo o-substituidos. Expired - Lifetime ES2107923T3 (es)

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
DE4042272A DE4042272A1 (de) 1990-12-31 1990-12-31 Verfahren zur herstellung von e-oximethern von phenylglyoxylsaeureestern
DE4042271A DE4042271A1 (de) 1990-12-31 1990-12-31 Verfahren zur herstellung von arylglyoxylsaeureestern
DE4042273A DE4042273A1 (de) 1990-12-31 1990-12-31 Verfahren zur herstellung von (alpha)-ketocarbonsaeureestern
DE4042280A DE4042280A1 (de) 1990-12-31 1990-12-31 Verfahren zur herstellung von (alpha)-ketocarbonsaeureestern
DE4042283A DE4042283A1 (de) 1990-12-31 1990-12-31 Verfahren zur herstellung von 2-phenoxymethylbenzoesaeuren
DE4042282A DE4042282A1 (de) 1990-12-31 1990-12-31 O-substituierte benzoylcyanide

Publications (1)

Publication Number Publication Date
ES2107923T3 true ES2107923T3 (es) 1997-12-01

Family

ID=27544603

Family Applications (4)

Application Number Title Priority Date Filing Date
ES91121148T Expired - Lifetime ES2091278T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de eteres de e-oxima de fenilglioxilatos.
ES96101038T Expired - Lifetime ES2105904T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de acidos 2-fenoximetilbenzoicos.
ES96101039T Expired - Lifetime ES2107923T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de cianuros de benzoilo o-substituidos.
ES96101025T Expired - Lifetime ES2105903T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de alfa-cetocarboxilatos.

Family Applications Before (2)

Application Number Title Priority Date Filing Date
ES91121148T Expired - Lifetime ES2091278T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de eteres de e-oxima de fenilglioxilatos.
ES96101038T Expired - Lifetime ES2105904T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de acidos 2-fenoximetilbenzoicos.

Family Applications After (1)

Application Number Title Priority Date Filing Date
ES96101025T Expired - Lifetime ES2105903T3 (es) 1990-12-31 1991-12-10 Procedimiento para la obtencion de alfa-cetocarboxilatos.

Country Status (13)

Country Link
US (1) US5221762A (es)
EP (4) EP0712835B1 (es)
JP (3) JP3343263B2 (es)
KR (1) KR100214191B1 (es)
AT (4) ATE143356T1 (es)
AU (1) AU641579B2 (es)
CA (2) CA2367876C (es)
DE (4) DE59108861D1 (es)
DK (4) DK0493711T3 (es)
ES (4) ES2091278T3 (es)
GR (4) GR3021280T3 (es)
HU (1) HU209283B (es)
IL (5) IL100387A (es)

Families Citing this family (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5258551A (en) * 1991-12-18 1993-11-02 Shionogi & Co., Ltd. Process for producing α-ketoamide derivative
DE4203170A1 (de) * 1992-02-05 1993-08-12 Basf Ag Verfahren zur herstellung von e-oximethern von phenylglyoxylsaeureestern
DE4311722C1 (de) * 1993-04-08 1994-04-07 Basf Ag Verfahren zur Herstellung von Halogenmethyl-benzoylcyaniden und neue Halogenmethyl-benzoylcyanide
DE4320499A1 (de) * 1993-05-14 1994-11-17 Bayer Ag Verfahren zur Herstellung von 2-Oximinoessigsäurederivaten
BR9405498A (pt) * 1993-07-02 1999-06-15 Shionogi & Co Processo para produzir derivados de acido carboxilico
ES2135741T5 (es) * 1994-06-10 2008-02-16 Bayer Cropscience Ag Metodo y productos intermedios para la preparacion de metilamidas de acido alfa-metoxiiminocarboxilico.
ES2142500T3 (es) * 1994-11-24 2000-04-16 Basf Ag Procedimiento para la obtencion de cianuros de metilbenzoilo halogenados.
DE4442560A1 (de) * 1994-11-30 1996-06-05 Basf Ag Iminooxybenzylcrotonsäureester, Verfahren zu ihrer Herstellung und ihre Verwendung
DE19648009A1 (de) 1996-11-20 1998-05-28 Bayer Ag Glyoxylsäureamide
KR20000057254A (ko) * 1996-11-26 2000-09-15 메리 이. 보울러 메틸 치환된 살진균제 및 살절지동물제
DE19726201A1 (de) 1997-06-20 1998-12-24 Bayer Ag Glyoxylsäureamide
DE19848200A1 (de) * 1998-10-20 2000-04-27 Basf Ag Verfahren zur Trocknung von Phenoxymethylbenzoesäuren
DE19958165A1 (de) 1999-12-02 2001-06-07 Bayer Ag Glyoxylsäureamide
US7238835B2 (en) * 2003-12-22 2007-07-03 Sanofi-Aventis Deutschland Gmbh Process for the preparation of substituted 2-(phenoxymethyl) benzoic acids
CA2575177A1 (en) * 2004-09-02 2006-03-16 Teva Pharmaceutical Industries Ltd. Purification of olmesartan medoxomil
US20070054948A1 (en) * 2004-09-02 2007-03-08 Lilach Hedvati Purification of olmesartan medoxomil
CN100443463C (zh) * 2005-06-28 2008-12-17 沈阳化工研究院 取代的对三氟甲基苯醚类化合物及其制备与应用
JP5417860B2 (ja) * 2008-08-26 2014-02-19 住友化学株式会社 α−ヒドロキシエステル類の製造方法
WO2010089267A2 (en) 2009-02-05 2010-08-12 Basf Se Method for producing 2-halogenomethylphenyl acetic acid derivatives
CN101664031B (zh) * 2009-09-30 2012-09-05 南宁市德丰富化工有限责任公司 一种含醚菌酯和春雷霉素的杀菌组合物
CN102391121B (zh) * 2011-08-04 2014-06-18 京博农化科技股份有限公司 2-(2-甲基苯氧基)-亚甲基苯基乙醛酸甲酯的制备方法
WO2013144924A1 (en) 2012-03-29 2013-10-03 Rallis India Ltd. An improved process for the synthesis of strobilurin fungicides viz trifloxystrobin and kresoxim-methyl
CN103787916B (zh) * 2014-01-15 2016-07-13 京博农化科技股份有限公司 一种肟菌酯的制备方法
CN104529818A (zh) * 2014-12-16 2015-04-22 江苏耕耘化学有限公司 制备(e)-2-(2-取代苯基)-2-甲氧亚胺基乙酸衍生物的方法
CN105884651B (zh) * 2016-04-25 2019-04-12 山东理工大学 一种醚菌酯中间体的制备装置及方法
CN109651190A (zh) * 2018-12-28 2019-04-19 京博农化科技有限公司 一种醚菌酯的合成方法
CN113754527B (zh) * 2021-09-07 2024-01-12 山东京博农化科技股份有限公司 一种醚菌酯中间体的合成方法
CN114478241A (zh) * 2021-12-31 2022-05-13 山东京博生物科技有限公司 一种芳甲酰基甲酸酯的制备方法

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DE1279682B (de) * 1961-08-12 1968-10-10 Boehringer & Soehne Gmbh Verfahren zur Herstellung von 6, 11-Dihydro-dibenzo-[b, e]-oxepin- bzw. -thiepin-11-on
CA1004689A (en) * 1972-09-12 1977-02-01 Genichi Tsuchihashi Enaminosulfoxides and a process for their preparation
DE2528211C3 (de) * 1975-06-25 1980-03-06 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von Acylcyaniden
DE2708189C2 (de) 1977-02-25 1985-07-04 Bayer Ag, 5090 Leverkusen Verfahren zur Herstellung von Phenylglyoxylsäureestern
US4234739A (en) 1978-12-05 1980-11-18 Stauffer Chemical Company Method for preparing glyoxylic acids and derivatives thereof
DE3002203A1 (de) 1980-01-22 1981-07-23 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von (alpha)-ketocarbonsaeure-n-tert.-butylamiden
DE3009044A1 (de) 1980-03-08 1981-09-24 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von (alpha)-ketocarbon-n-acylamiden
DE3623921A1 (de) * 1986-07-16 1988-01-21 Basf Ag Oximether und diese enthaltende fungizide
GB8617648D0 (en) 1986-07-18 1986-08-28 Ici Plc Fungicides
DE3705389A1 (de) 1987-02-20 1988-09-01 Basf Ag Substituierte crotonsaeureester und diese enthaltende fungizide
ATE145891T1 (de) * 1989-05-17 1996-12-15 Shionogi & Co Verfahren zur herstellung von alkoxyiminoacetamid-derivaten und ein zwischenproduckt dafür
FR2647110B1 (fr) * 1989-05-19 1991-07-26 Atochem Procede de synthese de cyanures d'acyle
JPH02306934A (ja) * 1989-05-19 1990-12-20 Mitsubishi Petrochem Co Ltd 4―(アルキルフェノキシ)酪酸の製造方法
FR2647109B1 (fr) * 1989-05-19 1991-07-26 Atochem Procede de preparation de cyanures d'acyle en milieu anhydre
DE3917352A1 (de) * 1989-05-27 1990-11-29 Basf Ag Neue oximether und diese enthaltende fungizide

Also Published As

Publication number Publication date
JP2002356468A (ja) 2002-12-13
EP0712835A2 (de) 1996-05-22
CA2367876A1 (en) 1992-07-01
IL116443A0 (en) 1996-03-31
EP0712833B1 (de) 1997-09-03
DK0493711T3 (da) 1996-11-11
EP0718279A1 (de) 1996-06-26
GR3025370T3 (en) 1998-02-27
JP3378555B2 (ja) 2003-02-17
EP0712833A2 (de) 1996-05-22
IL100387A (en) 1997-06-10
DK0718279T3 (da) 1997-10-27
EP0493711B1 (de) 1996-09-25
EP0493711A1 (de) 1992-07-08
JP3343263B2 (ja) 2002-11-11
CA2058553A1 (en) 1992-07-01
KR100214191B1 (ko) 1999-08-02
CA2058553C (en) 2005-09-13
ATE157643T1 (de) 1997-09-15
EP0712835B1 (de) 1997-08-20
ATE143356T1 (de) 1996-10-15
IL116442A0 (en) 1996-03-31
DE59108848D1 (de) 1997-10-09
ES2091278T3 (es) 1996-11-01
GR3021280T3 (en) 1997-01-31
DE59108861D1 (de) 1997-10-30
GR3025219T3 (en) 1998-02-27
IL116442A (en) 1997-06-10
ES2105903T3 (es) 1997-10-16
AU641579B2 (en) 1993-09-23
JP3378576B2 (ja) 2003-02-17
US5221762A (en) 1993-06-22
CA2367876C (en) 2006-10-24
DE59108832D1 (de) 1997-09-25
EP0712835A3 (es) 1996-06-05
JPH04295454A (ja) 1992-10-20
DE59108229D1 (de) 1996-10-31
HU209283B (en) 1994-04-28
DK0712835T3 (da) 1997-09-15
ES2105904T3 (es) 1997-10-16
JP2000256273A (ja) 2000-09-19
ATE158569T1 (de) 1997-10-15
IL116443A (en) 1997-06-10
IL100387A0 (en) 1992-09-06
AU9008291A (en) 1992-07-02
HU914162D0 (en) 1992-03-30
KR920012013A (ko) 1992-07-25
GR3024518T3 (en) 1997-11-28
HUT61264A (en) 1992-12-28
ATE157079T1 (de) 1997-09-15
EP0712833A3 (es) 1996-06-05
EP0718279B1 (de) 1997-09-24
DK0712833T3 (da) 1997-10-06

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