ES2054905T3 - Proceso para la preparacion de bisfenol a de alta pureza. - Google Patents

Proceso para la preparacion de bisfenol a de alta pureza.

Info

Publication number
ES2054905T3
ES2054905T3 ES89104252T ES89104252T ES2054905T3 ES 2054905 T3 ES2054905 T3 ES 2054905T3 ES 89104252 T ES89104252 T ES 89104252T ES 89104252 T ES89104252 T ES 89104252T ES 2054905 T3 ES2054905 T3 ES 2054905T3
Authority
ES
Spain
Prior art keywords
stage
crystals
crystal
high purity
main process
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
ES89104252T
Other languages
English (en)
Inventor
Shigeru Iimuro
Yoshio Morimoto
Takashi Kitamura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Toatsu Chemicals Inc
Original Assignee
Mitsui Toatsu Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP63056335A external-priority patent/JPH01230538A/ja
Priority claimed from JP63060277A external-priority patent/JPH01238550A/ja
Application filed by Mitsui Toatsu Chemicals Inc filed Critical Mitsui Toatsu Chemicals Inc
Application granted granted Critical
Publication of ES2054905T3 publication Critical patent/ES2054905T3/es
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/15—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by reduction of oxides of carbon exclusively
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/68—Purification; separation; Use of additives, e.g. for stabilisation
    • C07C37/70—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment
    • C07C37/84—Purification; separation; Use of additives, e.g. for stabilisation by physical treatment by crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C37/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring
    • C07C37/11—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms
    • C07C37/20—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom of a six-membered aromatic ring by reactions increasing the number of carbon atoms using aldehydes or ketones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
    • C07C39/12—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings
    • C07C39/15—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring polycyclic with no unsaturation outside the aromatic rings with all hydroxy groups on non-condensed rings, e.g. phenylphenol
    • C07C39/16—Bis-(hydroxyphenyl) alkanes; Tris-(hydroxyphenyl)alkanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

UN METODO PARA PREPARAR BISFEROL A DE ALTA PUREZA QUE COMPRENDE UN PROCESO PRINCIPAL QUE CONSISTE EN UNA PRIMERA ETAPA PARA HACER REACCIONAR FENOL CON ACETONA, UNA PRIMERA ETAPA DE AJUSTE DE CONCENTRACION, UNA PRIMERA ETAPA DE CRISTALIZACION PARA PRECIPITAR CRISTALES DEL ADUCTO DE BISFENOL A CON FENOL, UNA PRIMERA ETAPA DE SEPARACION PARA SEPARAR UNA SOLUCION CONTENIEDNDO LOS CRISTALES DEL ADUCTO EN LOS CRISTALES Y EL LICOR MADRE Y UNA ETAPA PARA SEPARAR EL FENOL DE LOS CRISTALES DEL ADUCTO; Y UN SUB - PROCESO COMPRENDIENDO UNA SEGUNDA ETAPA DE REACCION PARA HACER BETA - ISOPROPENILFENOL CON FENOL, UNA SEGUNDA ETAPA DE AJUSTE DE CONCENTRACION PARA SEPARAR UNA SOLUCION CONTENIENDO LOS SEGUNDOS CRISTALES DEL ADUCTO EN LOS SEGUNDOS CRISTALES Y EL SEGUNDO LICOR MADRE Y UNA ETAPA DE DESCOMPOSICION, SIENDO ALIMENTADO AL SUBPROCESO EL PRIMER LICOR MADRE DEL PROCESO PRINCIPAL Y LOS SEGUNDOS CRISTALES DEL ADUCTO DESDE EL SUBPROCESO SE SUMINISTRAN AL PROCESO PRINCIPAL. TAMBIEN UN METODO PARA PREPARAR BISFENOL A DE ALTA PUREZA QUE COMPRENDE UN PROCESO PRINCIPAL CON UNA PRIMERA ETAPA DE SEPARACION DE CATALIZADOR/REACCION
ES89104252T 1988-03-11 1989-03-10 Proceso para la preparacion de bisfenol a de alta pureza. Expired - Lifetime ES2054905T3 (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP63056335A JPH01230538A (ja) 1988-03-11 1988-03-11 高純度ビスフェノールａの製造方法
JP63060277A JPH01238550A (ja) 1988-03-16 1988-03-16 高純度ビスフェノールａの製造方法

Publications (1)

Publication Number Publication Date
ES2054905T3 true ES2054905T3 (es) 1994-08-16

Family

ID=26397281

Family Applications (1)

Application Number Title Priority Date Filing Date
ES89104252T Expired - Lifetime ES2054905T3 (es) 1988-03-11 1989-03-10 Proceso para la preparacion de bisfenol a de alta pureza.

Country Status (7)

Country Link
US (1) US4954661A (es)
EP (1) EP0332203B1 (es)
KR (1) KR910004133B1 (es)
CN (1) CN1022560C (es)
CA (1) CA1311498C (es)
DE (1) DE68906690T2 (es)
ES (1) ES2054905T3 (es)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL94554A (en) * 1990-05-29 1994-04-12 Bromine Compounds Ltd Process for the preparation of 4, (4) -dexyhydrophenyl clean by fractional refining of 4, 4 (- dibromobiphenyl after catalytic hydrolysis
US5248839A (en) * 1990-08-21 1993-09-28 Mitsui Toatsu Chemicals, Inc. Preparation process of bisphenol a
EP0496898A4 (en) * 1990-08-21 1993-03-10 Mitsui Toatsu Chemicals, Inc. Method of crystallizing bisphenol a having phenol added thereto
US5105026A (en) * 1990-11-15 1992-04-14 Shell Oil Company Process for preparing a bisphenol
PL164289B1 (pl) * 1990-11-24 1994-07-29 Inst Ciezkiej Syntezy Orga Sposób otrzymywani blsfenolu A PL PL
DE4105428A1 (de) * 1991-02-21 1992-08-27 Bayer Ag Verfahren zur reinigung von bisphenolen
EP0522700B1 (en) * 1991-07-10 1997-01-29 Chiyoda Corporation Process for the production of crystalline adduct of bisphenol A and phenol and apparatus therefor
US5368827A (en) * 1991-07-10 1994-11-29 Chiyoda Corporation Process for the production of crystalline adduct of bisphenol A and phenol and apparatus therefor
DE4213872A1 (de) * 1992-04-28 1993-11-04 Bayer Ag Verfahren zur herstellung von hochreinem bisphenol-a
CN1050828C (zh) * 1993-02-16 2000-03-29 中国石油化工总公司 制备高品位聚碳酸脂级双酚a的脱酚新方法
AU6105694A (en) * 1993-02-17 1994-09-14 China Petro-Chemical Corporation A multiple stage suspended reactive stripping process and apparatus
CN1080914A (zh) * 1993-02-17 1994-01-19 中国石油化工总公司 一种2,2-二(4-羟基苯基)丙烷的制造方法
US5300702A (en) * 1993-03-01 1994-04-05 Aristech Chemical Corporation Recovering values from heavy ends in bisphenol-A production
JP2885606B2 (ja) * 1993-05-12 1999-04-26 出光石油化学株式会社 ２，２−ビス（４−ヒドロキシフェニル）プロパンの製造方法
US5959158A (en) * 1996-04-12 1999-09-28 Gammill; Ben Method and system for bisphenol a production using water
US5874644A (en) * 1996-04-12 1999-02-23 Gammill; Ben Method and system for bisphenol a production using controlled turbulence
DE19720539A1 (de) 1997-05-16 1998-11-19 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Dihydroxydiarylalkanen
DE19720541A1 (de) 1997-05-16 1998-11-19 Bayer Ag Verfahren zur kontinuierlichen Herstellung von Dihydroxydiphenylalkanen
DE19900221A1 (de) * 1999-01-07 2000-07-13 Bayer Ag Verfahren und Vorrichtung zur Herstellung von Bisphenol-A-Prills und danach hergestellte Bisphenol-A-Prills
DE10015864A1 (de) * 2000-03-30 2001-10-11 Bayer Ag Stoffgemisch enthaltend Bisphenol A
US6703530B2 (en) 2002-02-28 2004-03-09 General Electric Company Chemical reactor system and process
JP4152655B2 (ja) * 2002-03-29 2008-09-17 出光興産株式会社 ビスフェノールａの製造方法
JP4419492B2 (ja) * 2002-10-28 2010-02-24 三菱化学株式会社 改善された連続晶析方法
CN100424060C (zh) * 2002-11-25 2008-10-08 陶氏环球技术公司 双酚-a的提纯方法
CN101370761B (zh) * 2006-01-25 2012-08-08 三菱化学株式会社 制备双酚a的方法
PL210812B1 (pl) * 2007-02-14 2012-03-30 Inst Ciężkiej Syntezy Organicznej Blachownia Sposób otrzymywania bisfenolu A
US7696388B2 (en) * 2008-07-09 2010-04-13 Sabic Innovative Plastics Ip B.V. Process for producing bisphenol-A
JP6055472B2 (ja) * 2012-06-28 2016-12-27 出光興産株式会社 ビスフェノールａの製造方法
CN109415284B (zh) * 2016-07-12 2022-06-17 沙特基础工业全球技术有限公司 双酚a的制备

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL301688A (es) * 1962-12-31
DE2064108B2 (de) * 1969-12-31 1974-09-26 Union Carbide Corp., New York, N.Y. (V.St.A.) Verfahren zur Herstellung von Phenol und p-Isopropenylphenol aus 2.4'-Bisphenol A
US4209646A (en) * 1974-10-31 1980-06-24 Rhone-Poulenc Industries Process for crystallizing an adduct of 2,2-di(4-hydroxyphenyl) propane and phenol
GB1565667A (en) * 1975-09-23 1980-04-23 Union Carbide Corp Deculouration of bipshenol-a recycle stream with cation exchange resin
US4180683A (en) * 1977-12-23 1979-12-25 General Electric Company Process for recovering 2,2-bis(4-hydroxyphenyl)propane from distillation residues from the preparation thereof
DD153680A5 (de) * 1980-10-27 1982-01-27 Inst Ciezkiej Syntezy Orga Herstellungsmethode von bisphenol a
US4354046A (en) * 1981-05-26 1982-10-12 The Dow Chemical Company Process for obtaining high purity bisphenol A
US4400553A (en) * 1981-06-24 1983-08-23 General Electric Company Recovery of BPA and phenol from aqueous effluent streams
US4400555A (en) * 1981-10-06 1983-08-23 General Electric Company Ion exchange catalyzed bisphenol synethesis

Also Published As

Publication number Publication date
EP0332203B1 (en) 1993-05-26
CN1022560C (zh) 1993-10-27
US4954661A (en) 1990-09-04
EP0332203A1 (en) 1989-09-13
KR910004133B1 (ko) 1991-06-22
DE68906690D1 (de) 1993-07-01
CN1036559A (zh) 1989-10-25
CA1311498C (en) 1992-12-15
KR890014418A (ko) 1989-10-23
DE68906690T2 (de) 1994-01-20

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