EP1603675B1 - Dispositif de laboratoire pourvu de rainures d'ecoulement sur un plan de travail - Google Patents

Dispositif de laboratoire pourvu de rainures d'ecoulement sur un plan de travail Download PDF

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Publication number
EP1603675B1
EP1603675B1 EP04720836A EP04720836A EP1603675B1 EP 1603675 B1 EP1603675 B1 EP 1603675B1 EP 04720836 A EP04720836 A EP 04720836A EP 04720836 A EP04720836 A EP 04720836A EP 1603675 B1 EP1603675 B1 EP 1603675B1
Authority
EP
European Patent Office
Prior art keywords
drain
worktop
laboratory
laboratory equipment
grooves
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP04720836A
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German (de)
English (en)
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EP1603675A1 (fr
Inventor
Thomas Maetzke
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Individual
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Individual
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Publication date
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L9/00Supporting devices; Holding devices
    • B01L9/02Laboratory benches or tables; Fittings therefor

Definitions

  • the invention relates to a laboratory device according to the preamble of patent claim 1.
  • Such a laboratory device is used, for example, to operate a preparative high-pressure liquid chromatography (HPLC) system in which, for example, flow rates of up to 100 ml / min and more usually occur in the research laboratory.
  • HPLC high-pressure liquid chromatography
  • the liquids used are usually volatile organic solvents which can be toxic and explosive.
  • a laboratory device which has three connected service towers, wherein at least one movable table extends adjacent to a side edge of the towers connecting substructure.
  • a device for the disposal of liquid waste at a laboratory workstation comprises a receptacle which is located at the laboratory workstation and / or a work table and has an inlet for the waste, a suction connection and a venting closure. Furthermore, this device has arranged on a carriage collecting container.
  • a laboratory table which is designed to be mobile and has a work surface and a storage space. Furthermore, a supply device is provided in this device, which is housed in the storage space of the laboratory table.
  • a laboratory device for example from US 3,041,957.
  • the work surface has a basin-like drain, which is connected to a waste container.
  • the waste container is housed in a cabinet-like substructure of the mobile, designed as a car laboratory table.
  • On the work surface there is a discharge hood, which is connected to an exhaust air system, which is partially guided by the base of the mobile laboratory table.
  • the invention has for its object to provide a laboratory device of the type mentioned, which is safer to handle.
  • the at least one working surface of the laboratory device according to the invention has a plurality of drainage grooves provided on its surface, which are connected to the at least one drain.
  • any leaking solvent can not spread over the entire work surface, but only to the next drainage channel.
  • the safety of the laboratory equipment according to the invention is considerably increased, since the outflowing or overflowing solvent is partly very volatile and toxic. If the solvent could spread over a larger area, more solvent would evaporate. However, by letting it go into the grooves, it can only spread over a relatively limited part of the work surface.
  • the drainage channels are designed and arranged distributed over the surface in such a way that a segment-like division results for the at least one working surface, wherein the drainage grooves are preferably also provided on the edge of the at least one working surface.
  • the drainage grooves are preferably also provided on the edge of the at least one working surface.
  • the at least one drain is located approximately in the middle of the at least one working surface, wherein a drain preferably made of Teflon drain pipe is connected to the at least one drain, which preferably below the at least one working surface to the rear, then vertically downwards and led to a waste container.
  • the outflowing liquid which, as mentioned above, is mostly an organic solvent in the applications of interest here, therefore quickly passes through the drainage channels and the at least one drain into a closed space, so that as little solvent as possible reaches the atmospheric environment of the laboratory device can.
  • the laboratory device according to the invention can additionally be designed to be extremely compact.
  • drains per work surface are preferably each about in the middle and at the rear edge of the work surface.
  • internal drainage holes lead the solvent running in the horizontal direction to the rear.
  • the outflows to these drainage holes are preferably located at the intersection points of the drainage grooves with the drainage holes in the at least one working surface.
  • the drainage holes are first connected to a horizontally extending manifold of an inert plastic, such as Teflon, which is connected via a vertically downwardly extending drain line to the waste container.
  • the drainage channels are inclined towards the at least one outlet.
  • the liquid located in the drainage channels has only a short residence time there, so that only little time is available for evaporation of the liquid. Rather, the liquid flows off quickly and can be collected in the aforementioned waste container.
  • a ventilated laboratory cabinet for liquid containers preferably solvent containers
  • the laboratory cabinet is preferably made of non-combustible material and has a grounded ground made of stainless steel.
  • This is also another source of solvent vapors, namely the area in which, for example, the waste container is located ventilated, i. connected to an exhaust air system.
  • This refinement thus also improves the safety of the laboratory equipment according to the invention, since explosive vapors or gases are less easily formed in the stated range. Analogous versions also apply to toxic gases or vapors.
  • a discharge hood is provided on the at least one working surface. This makes it possible to connect another source of solvent vapors to the exhaust air system. It is clear that the exhaust ducts of the aforementioned laboratory cabinet or the cabinets for solvent containers can be merged with those of the exhaust hood, so that ultimately only one exhaust system with multiple branches is required.
  • a safety device which triggers an alarm in the case of a liquid flowing out through the drainage grooves.
  • the liquid may in particular be an organic solvent.
  • the triggering of an alarm can interrupt, for example, the entire power supply of the laboratory equipment, so that a possibly threatening uncontrolled solvent leakage is prevented.
  • the inventive laboratory device can also be operated completely automatically. This is therefore a leak-proof platform on which systems can work in a state without human supervision, since the monitoring is performed electronically, for example, automatically.
  • the at least one work surface is part of a mobile laboratory cart, which preferably has an upper and a lower work surface and a lower floor in the form of, for example, a low-lying support structure for receiving the laboratory cabinet.
  • a laboratory device is therefore extremely mobile and accessible from all sides. It can improve occupational safety where this is necessary in the case of locally changing workplaces.
  • the subfloor in the form of a special, low-lying support structure for receiving one or more cabinets for solvent containers the latter are arranged as close to the ground as possible, so that they usually heavy container not completely raise, but only to tilt, to then in the Sliding cabinet to be pushed into. As a result, the accessibility of the liquid - in particular solvent container is improved and their handling easier.
  • the at least one working surface is composed of a plurality of advantageously three partial surfaces, each partial surface preferably having at least one outflow and a plurality of drainage grooves.
  • the parts of a work surface can thus be more easily transported to the construction site of the laboratory cart.
  • Fig. 1 is a schematic front view of a laboratory device 1 is shown schematically.
  • the laboratory device 1 has at least one working surface 3 having at least one drain 2.
  • the at least one working surface 3 is part of a mobile laboratory cart 4, which has an upper working surface 3 and a lower working surface 5 arranged underneath Underbody 6 has in the form of a low-lying support structure.
  • each sub-surface 27 may have one or more outflows 2 and a surrounding drainage groove 10, so that no solvent can fall beyond a partial area addition.
  • An embodiment with three partial surfaces 27 is shown schematically in FIG. 4, wherein each partial surface 27 has four segment-like subdivisions 11.
  • detectors such as e.g. Mass spectrometer or UV spectrometer, as well as chromatography columns or a hood 7, as shown in Fig. 1, be positioned below which sampler or fraction collector can be arranged.
  • lower working surface 5 is insofar a second device level, in which preferably pumps or flat components of the system, such as a safety device 22 explained below, can be accommodated.
  • the at least one working surface 3 has a plurality of drainage grooves 9, 10 provided on its surface 8, which are connected to the at least one drain 2.
  • the drainage grooves 9 run transversely to the longitudinal axis of the laboratory cart 4, while the drainage grooves 10 extend according to FIG. 3 in the longitudinal direction of the laboratory cart. The latter are omitted in Fig. 1 for the sake of clarity.
  • each of these work surfaces has the drainage grooves 9, 10 respectively connected to the at least one drain 2.
  • FIG. 3 shows a schematic plan view of the laboratory device 1
  • the drainage grooves 9, 10 are designed and arranged distributed over the surface 8 such that for the work surfaces 3, 5 each results in a previously mentioned in the sub-areas 27 segmental subdivision 11.
  • the drainage grooves 9, 10 are also provided on the edge 26 of each work surface 3, 5, as can be seen from FIG. 3; Here they form a groove enclosing the respective working area.
  • the drains 2 are according to a first embodiment in the middle or approximately in the middle of each working surface 3, 5 and are indicated in Fig. 1 only schematically.
  • a drain line 12 (see FIG. 2) is connected, which is preferably made of Teflon.
  • Each drain line 12 is guided below the respective working surface 3, 5 to the rear, then vertically downwards and to a in Fig. 2 schematically indicated waste container 13.
  • FIG. 2 shows a schematic, partial front view of the laboratory device 1.
  • the at least one working surface 3, 5 has a plurality of outflows 2, which are preferably arranged in each outflow groove 9 running transversely to the longitudinal axis of the at least one working surface 3, 5 and in the rearmost flow-off groove 10.
  • the at least one working surface in its interior preferably has a plurality of drain holes 28 extending horizontally to the rear, connected to the at least one drain 2 of a drainage groove 9, 10.
  • These drainage bores 28 are horizontal in the working surface 3, 5 and extend horizontally to the rear the drain or drains 2 at or near intersection points 29 of the respective drainage bore 28 with the drainage grooves 9 preferably approximately in the middle and the rearmost drainage groove 10.
  • only one drainage bore 28 is schematically indicated in FIG.
  • the drainage holes 28 are connected to the rear R and 30 of the working surface with a horizontally extending manifold (not shown), which is connected via a vertically downwardly leading drain line (see Fig. 2) with the waste container. All lines are preferably made of Teflon.
  • FIG. 5 A section along the line VV in Fig. 4 is shown schematically in Fig. 5. This figure illustrates that the drainage hole 28 embedded in the respective working surface 3, 5 and extends within this.
  • the drainage hole 28 is connected via outlets 2 with the drainage grooves 9, 10 in connection.
  • At the rear edge 30 of the work surface 3, 5 is an angular connection piece 31 is provided and screwed into the drainage hole 28, for example.
  • the free end of this connector 31 is connected to the manifold not shown in detail to the drain line 12 shown in FIG.
  • each connector 31 is located in a recess 32 at the rear edge 30 of the respective working surface 3, 5.
  • each connector 31 is housed well protected. It is clear that each work surface 3, 5 and also each partial surface 27 of the relevant work surface can have one or more internal drainage holes 28.
  • the drainage grooves 9, 10 are inclined to the respective outflow 2 and approximately horizontally draining drain lines 12 to the waste container 13. This can be done, for example, by the fact that the plate of the working surface is slightly bulged apart from its surface 8, wherein at the hole for the drain 2 is the lowest point. It is also possible that the entire surface 8 of the respective working surface 3, 5 including the drainage groove 9, 10 is slightly inclined to the respective outflow 2. It is also possible that the drainage channels are formed deeper becoming drain points.
  • Each work surface 3, 5 may for example be a polypropylene plate.
  • one of the liquid containers 15 is the aforementioned waste container 13.
  • the laboratory cabinet 14 is made of non-combustible material and has a grounded bottom 16 made of stainless steel sheet. This reduces the risk of electrostatic charging.
  • the laboratory cabinet 14 has two front-opening doors 17, 18 on, wherein the right door 18 is lockable with a lock 19.
  • further storage space is available on the subfloor 6 in the form of the low-lying support structure, in which case, for example, another cabinet for receiving liquid containers can be mounted.
  • the exhaust hood 7 is provided on the left half of the upper work surface 3, which can be provided via a feed opening 20 with the various sample and fraction carriers. Instead of a B e-feed opening, the exhaust hood can also have a front-slidable front window. On the left in Fig. 1 and left side and the back of the exhaust hood 7, a sliding door 21 is provided, via which also an access to the interior of the exhaust hood is possible. It is clear that both the extraction hood 7 and the ventilated laboratory cabinet 14 are connected to a not shown exhaust air system.
  • the laboratory device 1 may contain the previously mentioned safety device 22, which is indicated only by dashed lines in FIG. 1.
  • the safety device is designed such that it triggers an alarm in the case of a liquid flowing out through the drainage grooves 9, 10.
  • the safety device 22 can interrupt, for example, the entire power supply of the laboratory device 1 and thus prevent further liquid from flowing out and through the drainage channels 9, 10 and the drain lines 12.
  • the laboratory cart 4 has ultimately three levels, namely the upper working surface 3, including the lower working surface 5 and finally including the below the upper edges of the wheels 23 arranged subfloor 6 in the form of low-lying support structure for ventilated laboratory cabinets.
  • the support structure is open towards the front, so that the or the laboratory cabinets 14 tilted slightly forward with its trailing edge placed on the support structure and then can be pushed into the support structure without complete lifting into it.
  • Similar explanations apply to the liquid container 15 in relation to the respective laboratory cabinet 14 arranged on the underbody 6.
  • the two working surfaces 3, 5 are also provided at their edge 26 with the drainage grooves 9, 10 according to the invention.
  • the laboratory device 1 is only partly shown in comparison to the embodiment shown in FIG.
  • the cabinet 14 and the hood 7 are omitted, for example.
  • the drain lines 12 each extend from the drain 2 through each work surface 3, 5, as mentioned, first below the respective working surface to the rear and then down and finally open via a common line 24 in the liquid container 15, which here designed as a waste container 13 is.
  • a common line 24 in the liquid container 15 which here designed as a waste container 13 is.
  • the working surface drilled drainage holes 28 are present, which open into a running at the rear edge 30 of the working surface manifold, which connected via a downwardly leading drain line 12 to the waste container is.
  • the exhaust hood 7 is indicated only by dashed lines.
  • the drain grooves 9 and 10 extend around the individual segment-like subdivisions 11.
  • the drain 2 is located at an intersection of the drain grooves 9 and 10. It is clear that several drains can also be provided on each work surface.
  • the drainage grooves 9 and 10 and the segmental subdivisions 11 are also located in the region and in particular below the extraction hood 7, as indicated in phantom in FIG. 3, so that the safety device 22 (see FIG. 1) can also respond if a liquid in the region of the discharge hood 7 flows into one of the drainage grooves 9 or 10 and from there to the drain and via the drain lines 12 to the waste container 13 passes.
  • recesses 25, for example for cables and wires, are located on the rear side of the working surface designed as a table top.

Landscapes

  • Health & Medical Sciences (AREA)
  • Clinical Laboratory Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices For Use In Laboratory Experiments (AREA)
  • Knives (AREA)
  • Stringed Musical Instruments (AREA)
  • Finish Polishing, Edge Sharpening, And Grinding By Specific Grinding Devices (AREA)
  • Water Treatment By Sorption (AREA)

Claims (12)

  1. Dispositif de laboratoire comportant au moins une surface de travail (3, 5), laquelle surface de travail (3, 5) comporte plusieurs rainures d'écoulement (9, 10) prévues sur sa surface (8), et au moins une vidange (2), disposée dans l'une des rainures d'écoulement (9, 10), les rainures d'écoulement (9, 10) étant réalisées et disposées, en étant réparties sur la surface (8), de telle sorte qu'il en résulte, pour la ou les surfaces de travail (3, 5), une subdivision segmentée (11), et que les rainures d'écoulement (9, 10) s'étendent tout autour des subdivisions segmentées individuelles (11).
  2. Dispositif de laboratoire selon la revendication 1, caractérisé en ce que les rainures d'écoulement (9, 10) sont prévues aussi de façon à courir, sur le bord (26) de chaque surface de travail (3, 5), parallèlement au bord (26).
  3. Dispositif de laboratoire selon la revendication 1 ou 2, caractérisé en ce que la ou les vidanges (2) se trouvent approximativement au milieu de la ou des surfaces de travail (3, 5), et une conduite d'évacuation (12), de préférence réalisée en Teflon, communique avec la ou les vidanges (2), conduite d'évacuation qui court de préférence en dessous de la ou des surfaces de travail (3, 5) vers l'arrière, puis verticalement vers le bas, et vers une poubelle (13).
  4. Dispositif de laboratoire selon l'une des revendications 1 à 3, caractérisé en ce que la ou les surfaces de travail (3, 5) comprennent plusieurs vidanges (2), qui de préférence sont disposées dans chaque rainure d'écoulement (9) courant perpendiculairement à l'axe longitudinal de la ou des surfaces de travail (3, 5), et dans la rainure d'écoulement (10) située le plus en arrière.
  5. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce que la ou les surfaces de travail (3, 5) comportent dans leur volume intérieur plusieurs trous d'écoulement (28), courant horizontalement vers l'arrière, communiquant au moins avec les vidanges (2) d'une rainure d'écoulement (9, 10), trous d'écoulement qui de préférence, au niveau du bord arrière (30) de la ou des surfaces de travail (3, 5), communiquent avec un collecteur courant horizontalement, réalisé en Teflon, collecteur qui, par une conduite d'évacuation (12) courant verticalement vers le bas, communique avec une ou avec la poubelle (13).
  6. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce que les rainures d'écoulement (9, 10) sont inclinées vers la ou les vidanges (2).
  7. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce que, en dessous de la ou des surfaces de travail (3, 5), se trouve une armoire de laboratoire ventilée (14) destinée à des récipients pour liquides (15), de préférence des récipients pour solvants.
  8. Dispositif de laboratoire selon la revendication 7, caractérisé en ce que l'armoire de laboratoire (14) est réalisée en un matériau incombustible, et comprend un fond (16), mis à la terre, de préférence en tôle d'acier inoxydable.
  9. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce qu'une hotte aspirante (7) est prévue sur la ou les surfaces de travail (3, 5).
  10. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce qu'il est prévu un dispositif de sécurité (22), qui, en présence d'un liquide qui s'écoule par les rainures d'écoulement (9,10), déclenche une alarme.
  11. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce que la ou les surfaces de travail (3, 5) font partie d'un chariot mobile (4) de laboratoire, qui de préférence comprend une surface de travail supérieure et une surface de travail inférieure (3, 5), ainsi qu'un plancher (6), sous forme d'une construction portante surbaissée, pour recevoir l'armoire (14).
  12. Dispositif de laboratoire selon l'une des revendications précédentes, caractérisé en ce que la ou les surfaces de travail (3, 5) sont composées de plusieurs surfaces partielles (27), au moins trois, et que chaque surface partielle (27) comprend de préférence au moins une vidange (2), ainsi que plusieurs rainures d'écoulement (9, 10).
EP04720836A 2003-03-26 2004-03-16 Dispositif de laboratoire pourvu de rainures d'ecoulement sur un plan de travail Expired - Lifetime EP1603675B1 (fr)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
CH5222003 2003-03-26
CH00522/03A CH696232A5 (de) 2003-03-26 2003-03-26 Laboreinrichtung.
PCT/CH2004/000154 WO2004085066A1 (fr) 2003-03-26 2004-03-16 Dispositif de laboratoire pourvu de rainures d'ecoulement sur un plan de travail

Publications (2)

Publication Number Publication Date
EP1603675A1 EP1603675A1 (fr) 2005-12-14
EP1603675B1 true EP1603675B1 (fr) 2006-12-06

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Family Applications (1)

Application Number Title Priority Date Filing Date
EP04720836A Expired - Lifetime EP1603675B1 (fr) 2003-03-26 2004-03-16 Dispositif de laboratoire pourvu de rainures d'ecoulement sur un plan de travail

Country Status (6)

Country Link
US (1) US20060150317A1 (fr)
EP (1) EP1603675B1 (fr)
AT (1) ATE347445T1 (fr)
CH (1) CH696232A5 (fr)
DE (1) DE502004002235D1 (fr)
WO (1) WO2004085066A1 (fr)

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MX2008010408A (es) * 2008-08-13 2010-02-15 Dedutel Exportaciones E Imp Ac Sistema movil para practicas de laboratorio.
DE102014100526A1 (de) * 2013-11-27 2015-05-28 Düperthal Sicherheitstechnik Gmbh & Co. Kg Verfahren und Vorrichtung zur Ver- und/oder Entsorgung einer mit einem Gefahrstoff arbeitenden Einrichtung
DE202013105404U1 (de) * 2013-11-27 2015-03-02 Düperthal Sicherheitstechnik Gmbh & Co. Kg Kombination aus zumindest einer mit wenigstens einem Gefahrstoff arbeitenden Einrichtung und einem Sicherheitsschrank zur Aufbewahrung des betreffenden Gefahrstoffes
CN104190493A (zh) * 2014-09-26 2014-12-10 苏州萃田精密机械有限公司 一种可移动式配液操作台
DE202016102085U1 (de) 2016-04-20 2016-05-06 Düperthal Sicherheitstechnik Gmbh & Co. Kg Laboreinrichtung
CN106513073B (zh) * 2016-12-08 2018-09-11 楚辉 一种具有分流导水用实验台
CN110013896A (zh) * 2019-05-23 2019-07-16 张靖 一种多功能化学实验台
CN111558408A (zh) * 2020-06-24 2020-08-21 南通市肿瘤医院 一种防污染易清洁检验科检验操作台

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Also Published As

Publication number Publication date
DE502004002235D1 (de) 2007-01-18
ATE347445T1 (de) 2006-12-15
EP1603675A1 (fr) 2005-12-14
WO2004085066A1 (fr) 2004-10-07
US20060150317A1 (en) 2006-07-13
CH696232A5 (de) 2007-02-28

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