EP0854336A1 - Procédé pour tourner des petits objets dans un récipient et dispositif pour la mise en oeuvre de ce procédé - Google Patents

Procédé pour tourner des petits objets dans un récipient et dispositif pour la mise en oeuvre de ce procédé Download PDF

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Publication number
EP0854336A1
EP0854336A1 EP98100096A EP98100096A EP0854336A1 EP 0854336 A1 EP0854336 A1 EP 0854336A1 EP 98100096 A EP98100096 A EP 98100096A EP 98100096 A EP98100096 A EP 98100096A EP 0854336 A1 EP0854336 A1 EP 0854336A1
Authority
EP
European Patent Office
Prior art keywords
process container
air
closure elements
container
support
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP98100096A
Other languages
German (de)
English (en)
Other versions
EP0854336B2 (fr
EP0854336B1 (fr
Inventor
Harald Wittler
Olaf Horner
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Atec Pharmatechnik GmbH
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7817432&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP0854336(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Individual filed Critical Individual
Publication of EP0854336A1 publication Critical patent/EP0854336A1/fr
Application granted granted Critical
Publication of EP0854336B1 publication Critical patent/EP0854336B1/fr
Publication of EP0854336B2 publication Critical patent/EP0854336B2/fr
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B9/00—Machines or apparatus for drying solid materials or objects at rest or with only local agitation; Domestic airing cupboards
    • F26B9/06—Machines or apparatus for drying solid materials or objects at rest or with only local agitation; Domestic airing cupboards in stationary drums or chambers
    • F26B9/08—Machines or apparatus for drying solid materials or objects at rest or with only local agitation; Domestic airing cupboards in stationary drums or chambers including agitating devices, e.g. pneumatic recirculation arrangements
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26—DRYING
    • F26B—DRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B21/00—Arrangements or duct systems, e.g. in combination with pallet boxes, for supplying and controlling air or gases for drying solid materials or objects
    • F26B21/06—Controlling, e.g. regulating, parameters of gas supply
    • F26B21/12—Velocity of flow; Quantity of flow, e.g. by varying fan speed, by modifying cross flow area

Definitions

  • the invention relates to a method for drying small objects in a process container, such as closure elements for pharmaceutical purposes (stoppers), after treating the small items as well as a device to carry out this procedure, in which under an air-permeable pad is arranged for the small objects is processed inside the process container preheated air is supplied and the small items thus rearranged relative to the process container by air be that a complete drying takes place.
  • Closure elements for pharmaceutical purposes for example Stoppers are treated in such a way that they are in a Wash phase first washed with high-purity, germ-free water will. Washing can be done with or without the addition of detergents respectively.
  • the Process container first filled with the closure elements and water is added.
  • the closure elements by means of the process container supplied compressed air moves.
  • the wash water is after the Treatment process drained again. Possibly. includes in siliconizing in a second phase. To do this again hot, high-purity water is supplied, the water dosed with silicone. Then the water away.
  • a subsequent one Phase is sterilized using steam.
  • Fluid bed dryers are also known, for example from “K. Kröll: dryer and drying process, Springer publishing house 1959, p. 275 ff ", in which air constantly with such Speed up through a layer of particles flows that the particles are slightly lifted and loosened, but not to be carried away. All parts are included constantly on the move. This allows free-flowing goods, too which can also include plastics, are dried. Another disadvantage here is that the particles due to their Frequently encounter movement while doing a considerable amount Generate abrasion. In addition, these are fluid bed dryers not suitable for particles that clump together or compacting.
  • DE 42 11 485 C2 describes a method for removing Moisture from inside a solid, for example described in wood.
  • the wood is initially included a high pressure applied to the liquid mechanically drives out of the solid, and then periodically rapidly changing pressure exposed to the rest To remove moisture.
  • a high pressure applied to the liquid mechanically drives out of the solid, and then periodically rapidly changing pressure exposed to the rest To remove moisture.
  • constant Pressure changes give the risk of severe particle abrasion.
  • the present invention is based on the object Method and device for carrying out this method of the type mentioned at the outset with which with the one with the least possible technical effort achieved complete drying of small objects and as far as possible particle abrasion and compacting is avoided.
  • the invention provides that the small items pre-warmed by the processed Air dried while lying on the pad, and that at least once briefly during drying an additional air mass flow passed under the pad who lifts the small objects and turns them over.
  • the single figure shows a schematic representation of a Process container and a pressure air vessel with the corresponding Line connections. The necessary for process control Valves are not shown.
  • a process container designated 1 is for the treatment of Closure elements provided for pharmaceutical purposes.
  • the Treatment has a washing phase, possibly a siliconization phase, a subsequent sterilization phase and one itself then drying phase.
  • Subject of the present The invention is only the drying phase.
  • the process container 1 has a perforated designated 2 Support for the closure elements, e.g. Stopper (not shown).
  • the closure elements are in the process container 1 inserted through an opening (not shown).
  • the process container 1 is shown schematically by a Connection 3 off via a pipe connection and a Media tube 4 high-purity water (WFI, Water for Injection) fed. Possibly. 5 detergents are added via a connection.
  • WFI high-purity water
  • Possibly. 5 detergents are added via a connection.
  • compressed air is connected 6 via a line 7 and the media tube 4 the inside of the process container supplied, whereby the closure elements be moved in the water and thereby the washing process takes place.
  • the compressed air escapes via an exhaust air connection 15. After the washing process, the water is over a Drain 8 derived.
  • siliconization can then be carried out.
  • water is supplied to the inside of the container, which Silicone was added via a metering device 9. Then the closure elements are fed again by means of Compressed air moves. After completion of the siliconization process the water is drained again.
  • a sterilization process then takes place.
  • the Process container 1 from the top of pure steam over a Port 10 supplied.
  • the sterilization takes place at about 120 ° C for about 20 minutes at elevated pressure. After this The process container will be sterilized again to atmospheric pressure brought.
  • closure elements are then dried.
  • the inside of the process container via the Media tube 4 heated sterile air supplied via a connection 11.

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Drying Of Solid Materials (AREA)
  • Apparatus For Disinfection Or Sterilisation (AREA)
  • Control And Other Processes For Unpacking Of Materials (AREA)
EP98100096A 1997-01-15 1998-01-07 Procédé pour tourner des petits objets dans un récipient et dispositif pour la mise en oeuvre de ce procédé Expired - Lifetime EP0854336B2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19701154 1997-01-15
DE19701154A DE19701154B4 (de) 1997-01-15 1997-01-15 Verfahren zum Trocknen von in einem Prozeßbehälter befindlichen kleinen Gegenständen sowie Vorrichtung zur Durchführung dieses Verfahrens

Publications (3)

Publication Number Publication Date
EP0854336A1 true EP0854336A1 (fr) 1998-07-22
EP0854336B1 EP0854336B1 (fr) 2001-07-18
EP0854336B2 EP0854336B2 (fr) 2005-07-27

Family

ID=7817432

Family Applications (1)

Application Number Title Priority Date Filing Date
EP98100096A Expired - Lifetime EP0854336B2 (fr) 1997-01-15 1998-01-07 Procédé pour tourner des petits objets dans un récipient et dispositif pour la mise en oeuvre de ce procédé

Country Status (5)

Country Link
US (1) US6006441A (fr)
EP (1) EP0854336B2 (fr)
AT (1) ATE203318T1 (fr)
DE (2) DE19701154B4 (fr)
DK (1) DK0854336T4 (fr)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3111453A (en) * 1961-08-31 1963-11-19 Crown Zellerbach Corp Drying of pulp
FR2247388A1 (fr) * 1973-10-12 1975-05-09 Anrep Rene
EP0423377A1 (fr) * 1989-09-15 1991-04-24 International Business Machines Corporation Procédé et dispositif pour le séchage d'objets
DE4139860A1 (de) * 1990-12-04 1992-06-11 Murata Manufacturing Co Komponententrockner
DE4211485A1 (de) 1992-04-06 1993-10-07 Stahl Werner Prof Dr Ing Verfahren zum Entfeuchten von Feststoffen
EP0609498A1 (fr) * 1992-10-28 1994-08-10 Anneliese Cramer Trocknerbau Dessiccateur pour granulat de matière thermodurcissable

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA609127A (en) * 1960-11-22 Skoglund Bengt Turbulent pneumatic drying
US1472314A (en) * 1918-04-27 1923-10-30 Perry & Webster Inc Process of and apparatus for drying and treating materials
US1524567A (en) * 1921-12-14 1925-01-27 Scott Hutchinson W Method of drying objects
US2974419A (en) * 1956-03-24 1961-03-14 Hoechst Ag Method of and apparatus for drying solid particles
CH504892A (de) * 1969-03-31 1971-03-31 Buehler Ag Geb Verfahren zur Behandlung von Schüttgut und Gutauflage zur Ausführung des Verfahrens
US3717434A (en) * 1971-08-19 1973-02-20 R Black Autoclave
US4934392A (en) * 1987-11-20 1990-06-19 Shubert Systems Limited Cleaning apparatus
US4939850A (en) * 1989-03-29 1990-07-10 Atlantic Richfield Company Method and apparatus to conduct fluidization of cohesive solids by pulsating vapor flow
US5019994A (en) * 1989-05-31 1991-05-28 Universal Dynamics Corporation Method and apparatus for drying articles in a continuous feed process

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3111453A (en) * 1961-08-31 1963-11-19 Crown Zellerbach Corp Drying of pulp
FR2247388A1 (fr) * 1973-10-12 1975-05-09 Anrep Rene
EP0423377A1 (fr) * 1989-09-15 1991-04-24 International Business Machines Corporation Procédé et dispositif pour le séchage d'objets
DE4139860A1 (de) * 1990-12-04 1992-06-11 Murata Manufacturing Co Komponententrockner
DE4211485A1 (de) 1992-04-06 1993-10-07 Stahl Werner Prof Dr Ing Verfahren zum Entfeuchten von Feststoffen
DE4211485C2 (de) * 1992-04-06 1994-09-08 Stahl Werner Verfahren zum Trocknen eines feuchten Feststoffes
EP0609498A1 (fr) * 1992-10-28 1994-08-10 Anneliese Cramer Trocknerbau Dessiccateur pour granulat de matière thermodurcissable

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
"TROCKNER UND TROCKNUNGSVERFAHREN", 1959, SPRINGER-VERLAG, pages: 275 FF

Also Published As

Publication number Publication date
DE19701154B4 (de) 2006-02-16
EP0854336B2 (fr) 2005-07-27
ATE203318T1 (de) 2001-08-15
US6006441A (en) 1999-12-28
DE59801023D1 (de) 2001-08-23
DE19701154A1 (de) 1998-07-16
EP0854336B1 (fr) 2001-07-18
DK0854336T3 (da) 2001-11-05
DK0854336T4 (da) 2005-11-28

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