EP0814153A3 - Feste waschaktive Zubereitung mit verbessertem Einspülverhalten - Google Patents

Feste waschaktive Zubereitung mit verbessertem Einspülverhalten Download PDF

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Publication number
EP0814153A3
EP0814153A3 EP97116694A EP97116694A EP0814153A3 EP 0814153 A3 EP0814153 A3 EP 0814153A3 EP 97116694 A EP97116694 A EP 97116694A EP 97116694 A EP97116694 A EP 97116694A EP 0814153 A3 EP0814153 A3 EP 0814153A3
Authority
EP
European Patent Office
Prior art keywords
prepd
opt
pref
washing
rounding
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
EP97116694A
Other languages
English (en)
French (fr)
Other versions
EP0814153A2 (de
Inventor
Bernd Dipl.-Chem. Dr. Larson
Kathrin Dipl.-Chem. Dr. Schnepp
Jochen Dipl.-Chem. Dr. Jacobs
Norbert Kühne
Hubert Dipl.-Chem. Dr. Pawelczyk
Volker Runge
Wolfgang Dipl.-Chem. Dr. Seiter
Rene-Andres Dipl.-Chem. Dr. Artiga Gonzalez
Monika Dipl.-Chem. Dr. Böcker
Günther Dipl.-Chem. Dr. Vogt
Eduard Dipl.-Chem. Dr. Smulders
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henkel AG and Co KGaA
Original Assignee
Henkel AG and Co KGaA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=6462334&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=EP0814153(A3) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA
Publication of EP0814153A2 publication Critical patent/EP0814153A2/de
Publication of EP0814153A3 publication Critical patent/EP0814153A3/de
Withdrawn legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents
    • C11D11/0082Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • C11D1/12Sulfonic acids or sulfuric acid esters; Salts thereof
    • C11D1/14Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
    • C11D1/146Sulfuric acid esters
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/72Ethers of polyoxyalkylene glycols
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D10/00Compositions of detergents, not provided for by one single preceding group
    • C11D10/04Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D11/00Special methods for preparing compositions containing mixtures of detergents
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/06Powder; Flakes; Free-flowing mixtures; Sheets
    • C11D17/065High-density particulate detergent compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246Silicates, e.g. diatomaceous earth
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246Silicates, e.g. diatomaceous earth
    • C11D3/1253Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/18Hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2003Alcohols; Phenols
    • C11D3/2006Monohydric alcohols
    • C11D3/201Monohydric alcohols linear
    • C11D3/2013Monohydric alcohols linear fatty or with at least 8 carbon atoms in the alkyl chain
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2079Monocarboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3703Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/373Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicones
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/02Anionic compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Emergency Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

Bei einem Verfahren zur Herstellung einer waschaktiven Zubereitung mit hohem Schüttgewicht in Granulatform, hergestellt durch strangförmiges Verpressen eines homogenen Vorgemisches über Lochformen, anschließendes Zerkleinern des Extrudats mittels einer Schneidevorrichtung und nachfolgende Behandlung in einem Rondiergerät sollte ein Nachbehandlungsverfahren zur Verbesserung des Auflöseverhaltens ausgebildet werden. Dies gelingt dadurch, daß man das vorgefertige Granulat mit einem Schüttgewicht über 500 g/l unter Mischen mit einer flüssigen oder festen, hydrophoben und/oder wasserunlöslichen Komponente, welche kein Zeolith ist und aus der Gruppe umfassend Paraffine, inerte Siloxane, Fettsäuresalze, Alkohole mit 10 bis 22 C-Atomen, welche auch sulfatiert sein können, Kieselsäuren, anorganische anionische Schichtverbindungen, anorganische kationische Schichtverbindungen sowie deren Gemische ausgewählt wird, in Kontakt bringt, wobei das Gewichtsverhältnis von vorgefertigtem Granulat zu flüssigem oder festem, hydrophobem und/oder wasserunlöslichem Behandlungsmittel zwischen 20 : 1 und 2000 : 1 eingestellt wird.
EP97116694A 1992-07-02 1993-06-24 Feste waschaktive Zubereitung mit verbessertem Einspülverhalten Withdrawn EP0814153A3 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE4221736A DE4221736A1 (de) 1992-07-02 1992-07-02 Feste waschaktive Zubereitung mit verbessertem Einspülverhalten
DE4221736 1992-07-02
EP93914715A EP0648259B1 (de) 1992-07-02 1993-06-24 Feste waschaktive zubereitung mit verbessertem einspülverhalten

Related Parent Applications (2)

Application Number Title Priority Date Filing Date
EP93914715A Division EP0648259B1 (de) 1992-07-02 1993-06-24 Feste waschaktive zubereitung mit verbessertem einspülverhalten
EP93914715.3 Division 1994-01-20

Publications (2)

Publication Number Publication Date
EP0814153A2 EP0814153A2 (de) 1997-12-29
EP0814153A3 true EP0814153A3 (de) 1999-05-06

Family

ID=6462334

Family Applications (2)

Application Number Title Priority Date Filing Date
EP93914715A Revoked EP0648259B1 (de) 1992-07-02 1993-06-24 Feste waschaktive zubereitung mit verbessertem einspülverhalten
EP97116694A Withdrawn EP0814153A3 (de) 1992-07-02 1993-06-24 Feste waschaktive Zubereitung mit verbessertem Einspülverhalten

Family Applications Before (1)

Application Number Title Priority Date Filing Date
EP93914715A Revoked EP0648259B1 (de) 1992-07-02 1993-06-24 Feste waschaktive zubereitung mit verbessertem einspülverhalten

Country Status (5)

Country Link
EP (2) EP0648259B1 (de)
AT (1) ATE170918T1 (de)
DE (2) DE4221736A1 (de)
ES (1) ES2122028T3 (de)
WO (1) WO1994001526A1 (de)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9313878D0 (en) * 1993-07-05 1993-08-18 Unilever Plc Detergent composition or component containing anionic surfactant and process for its preparation
EP0708855A4 (de) * 1993-07-14 1996-07-17 Procter & Gamble Perkarbonat enthaltende waschmittel und verfahren zu deren herstellung
EP0701605B2 (de) 1994-02-24 2017-02-22 Basf Se Verbesserte enzyme und diese enthaltene detergentien
ES2364774T3 (es) * 1994-02-24 2011-09-14 HENKEL AG & CO. KGAA Enzimas mejoradas y detergentes que las contienen.
CA2189752A1 (en) * 1994-05-16 1995-11-23 Charles Louis Stearns Granular detergent composition containing admixed fatty alcohols for improved cold water solubility
DE4434500A1 (de) * 1994-09-27 1996-03-28 Henkel Kgaa Verbessertes Extrusionsverfahren zur Herstellung von Waschmitteln
DE4435742A1 (de) * 1994-10-06 1996-04-11 Henkel Kgaa Verfahren zur Herstellung wasch- oder reinigungsaktiver Extrudate
DE19524287A1 (de) * 1995-07-06 1997-01-09 Henkel Kgaa Von Staub- und Feinanteilen freie granulare Wasch- und Reinigungsmittel hoher Schüttdichte
DE19627427A1 (de) * 1996-07-08 1998-01-15 Henkel Kgaa Wasch- oder Reinigungsmitteladditiv sowie ein Verfahren zu seiner Herstellung
EP0888450B2 (de) * 1996-07-08 2003-01-15 Henkel Kommanditgesellschaft auf Aktien Wasch- oder reinigungsmitteladditiv sowie ein verfahren zu seiner herstellung
DE19722767A1 (de) * 1997-06-02 1998-12-03 Henkel Kgaa Wasch- oder Reinigungsmittel mit erhöhter Reinigungsleistung
ATE310075T1 (de) * 1999-09-10 2005-12-15 Henkel Kgaa Reinigungsmittelkomponente mit feinteiligen feststoffen
DE10002009A1 (de) * 2000-01-19 2001-07-26 Cognis Deutschland Gmbh Tensidgranulate
GB0111862D0 (en) 2001-05-15 2001-07-04 Unilever Plc Granular composition
GB0111863D0 (en) 2001-05-15 2001-07-04 Unilever Plc Granular composition
KR20030091474A (ko) * 2002-05-28 2003-12-03 주식회사 세종파마텍 청소가 용이한 정제 코팅장치
ES2473967T3 (es) 2009-04-24 2014-07-08 Unilever N.V. Fabricación de partículas de detergente con alto contenido en agente activo
BR112019003035A2 (pt) 2016-09-07 2019-05-14 Ecolab Usa Inc. bloco de detergente sólido, composição de bloco de detergente sólido, e, métodos para limpeza, sanitização e/ou branqueamento e para ajustar a taxa de dispensação de uma composição de detergente sólido existente

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0337330A2 (de) * 1988-04-15 1989-10-18 Henkel Kommanditgesellschaft auf Aktien Verfahren zur Erhöhung der Dichte sprühgetrockneter, phosphatreduzierter Waschmittel
EP0360330A2 (de) * 1988-09-23 1990-03-28 Unilever N.V. Herstellungsverfahren für Waschmittelpulver mit Spendereigenschaften
DE4123195A1 (de) * 1991-07-12 1993-01-14 Henkel Kgaa Waschaktive zubereitung mit verzoegertem aufloeseverhalten und verfahren zu ihrer herstellung

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NZ188469A (en) * 1977-10-06 1980-12-19 Colgate Palmolive Co Detergent composition comprising a univalent cation-exchanging zeolite a nonionic detergent and builder salts
ES2020949B3 (es) * 1986-01-17 1991-10-16 Kao Corp Composicion detergente granular de alta densidad.
GB8810193D0 (en) * 1988-04-29 1988-06-02 Unilever Plc Detergent compositions & process for preparing them

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0337330A2 (de) * 1988-04-15 1989-10-18 Henkel Kommanditgesellschaft auf Aktien Verfahren zur Erhöhung der Dichte sprühgetrockneter, phosphatreduzierter Waschmittel
EP0360330A2 (de) * 1988-09-23 1990-03-28 Unilever N.V. Herstellungsverfahren für Waschmittelpulver mit Spendereigenschaften
DE4123195A1 (de) * 1991-07-12 1993-01-14 Henkel Kgaa Waschaktive zubereitung mit verzoegertem aufloeseverhalten und verfahren zu ihrer herstellung

Also Published As

Publication number Publication date
WO1994001526A1 (de) 1994-01-20
EP0648259B1 (de) 1998-09-09
ES2122028T3 (es) 1998-12-16
DE4221736A1 (de) 1994-01-05
DE59308975D1 (de) 1998-10-15
EP0648259A1 (de) 1995-04-19
ATE170918T1 (de) 1998-09-15
EP0814153A2 (de) 1997-12-29

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