EP0517068B1 - Mixing kneader - Google Patents
Mixing kneader Download PDFInfo
- Publication number
- EP0517068B1 EP0517068B1 EP92108829A EP92108829A EP0517068B1 EP 0517068 B1 EP0517068 B1 EP 0517068B1 EP 92108829 A EP92108829 A EP 92108829A EP 92108829 A EP92108829 A EP 92108829A EP 0517068 B1 EP0517068 B1 EP 0517068B1
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- EP
- European Patent Office
- Prior art keywords
- shaft
- main shaft
- kneading
- stripping
- mixing kneader
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F31/00—Mixers with shaking, oscillating, or vibrating mechanisms
- B01F31/40—Mixers with shaking, oscillating, or vibrating mechanisms with an axially oscillating rotary stirrer
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/60—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis
- B01F27/70—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms
- B01F27/701—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers
- B01F27/702—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a horizontal or inclined axis with paddles, blades or arms comprising two or more shafts, e.g. in consecutive mixing chambers with intermeshing paddles
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/92—Heating or cooling systems for heating the outside of the receptacle, e.g. heated jackets or burners
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F35/95—Heating or cooling systems using heated or cooled stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/90—Heating or cooling systems
- B01F2035/99—Heating
Definitions
- the invention relates to a mixer kneader for carrying out mechanical, chemical and / or thermal processes with at least two axially parallel rotating shafts, disk surfaces with kneading bars arranged on their periphery being provided on the one shaft referred to as main shaft, which are coated by kneading bars which are on disk surfaces are arranged on the other shaft referred to as the cleaning shaft, the kneading bars of two adjacent disk surfaces on the main shaft or on the cleaning shaft maintaining a distance from one another through which the disk surface with the kneading bar on the cleaning shaft or the main shaft passes.
- Such a multi-spindle mixing and kneading machine is known, for example, from CH-A-506 322.
- One of the shafts is provided with radial disk elements and axially aligned kneading bars arranged between the disks and is referred to as a disk shaft. Kneading elements shaped like frames engage between these disks and are arranged on the second parallel stirrer shaft. These kneading elements clean the discs and kneading bars of the disc shaft.
- the agitator shaft In order to achieve a reasonably sufficient cleaning of the disc surfaces, the agitator shaft must rotate faster than the disc shaft by an intended speed ratio. This speed ratio depends primarily on the number of kneading bars on the disc elements, since the kneading elements have to intervene in the spaces between the kneading bars. This results in an insufficient cleaning effect of the pane surfaces, which in turn has a negative effect on the heat transfer to the product to be treated.
- star-shaped or cross-shaped elements are placed on two shafts rotating in the same direction and have axially extending rods on their outer circumference. These elements can only be used for stirring, but no mixing or kneading effect can be achieved.
- a mixing device is known from Patent Abstracts of Japan, vol. 13, no. 29 (C562) 3377, January 23, 1989, in which elliptical disk elements are seated on two adjacent shafts which carry bars at their outer ends. With these elliptical disk elements, there is only a small area for heat transfer.
- a mixer kneader of the type mentioned at the outset is known from EP-A-0 460 466 with the filing date 24.05.91, the priority date 05.06.90 and the publication date 11.12.91.
- the present invention has for its object to significantly improve the cleaning of all areas and parts within the mixing kneader and at the same time the kneading effect exerted on the product.
- thermal treatment of the product there is also the task that the heat exchanger area within the mixing kneader is increased and the heat transfer to the product is significantly improved.
- wings are formed on both sides of the kneading bar, which run radially at a short distance from the disk surfaces of the main shaft or cleaning shaft, and that the disk surfaces of at least the main shaft are sawtooth-like on their outer circumference or are provided with wavy indentations.
- the disk surfaces are sawtooth-shaped, or they have wavy bulges.
- the carrier for the kneading bars on the cleaning shaft does not necessarily have to be designed as a disk surface.
- the kneading bar and cleaning shaft could also be connected by a simple stem that can slide through the above-mentioned distance of the kneading bars of two adjacent disc elements on the main shaft.
- pane surfaces are preferable because they contribute to increasing the heat exchange and improving the kneading effect.
- the distance between the kneading bars of adjacent disk elements of the main shaft in turn causes the disk surfaces of the cleaning shaft or an above-mentioned stem to be in gap with the disk surfaces of the main shaft. Even the disk surfaces or the stem are preferably arranged centrally between two disk surfaces of the main shaft. It goes without saying that if the kneading bars of the main shaft and cleaning shaft are preferably identical, not only are two adjacent kneading bars of the main shaft spaced apart, but this distance is also formed by two adjacent kneading bars of the cleaning shaft, but offset, by which then the Disc surface of the main shaft strokes.
- kneading bars are preferably of identical design, this can also apply to the disc surfaces of the main shaft and cleaning shaft, but they can also be designed differently, depending on the user's request, so that product transport through the cleaning shaft is different from that through the main shaft.
- the invention leaves many possibilities open here.
- the main shaft and cleaning shaft rotate in the same clockwise direction.
- the disc or cleaning elements according to the invention also allow the main shaft and Cleaning wave in the counterclockwise direction. It is also possible to rotate the main shaft and cleaning shaft at the same or different speeds. When rotating, whether in the same direction or in opposite directions, at the same speed, the number of kneading bars on the main shaft should correspond to that on the cleaning shaft. This enables the most economical cleaning for this speed without interfering with the kneading bars.
- the number of kneading bars arranged on the main shaft and on the cleaning shaft should be inversely proportional to the speed ratio. For example, if the speed ratio of the main shaft to the cleaning shaft is 1: 4, then four kneading bars are arranged on the main shaft and only one kneading bar on the cleaning shaft. Eight kneading bars can also be provided on the main shaft and two kneading bars on the cleaning shaft.
- the speed ratio is odd, for example 1: 1.25, five kneading bars are arranged on the main shaft and four kneading bars on the cleaning shaft.
- the present mixer kneader is extremely flexible.
- the main advantages are improved self-cleaning, a larger specific heat exchange surface, a more effective one Surface renewal with diffusion-determined evaporation processes, a more intensive mixing effect with gentle kneading and less compacting as well as a narrow residence time spectrum.
- a mixer kneader P has gem.
- Fig. 1 a housing 1, which consists of several housing sections 1 a, 1 b and 1 c. The housing sections are coupled to one another by corresponding flange connections 2.
- a feed nozzle 3 for a product to be treated in the mixing kneader and in the housing section 1 c an outlet nozzle 4 for the treated product.
- the product is transported from the feed nozzle 3 to the outlet nozzle 4 by means of two shafts 5 and 6 and kneading and transport elements 7 arranged thereon.
- the product is mixed and kneaded, and preferably a thermal treatment takes place.
- the shafts 5 and 6 and optionally also the kneading and transport elements 7 and, not shown in more detail, the housing wall 8 are heated.
- connections 9 and 10 are provided, these connections 9 and 10 around corresponding outlet nipples 11 and 12 for the heating medium guided through the shafts 5 and 6 are arranged. Appropriate routing of the heating medium in the lateral surfaces of the shafts 5 and 6 and a corresponding return through the outlet nipples 11 and 12 are prior art and are therefore not described further.
- shaft lugs 13 and 14 connected to the shafts 5 and 6 pass through a lantern 15, a stuffing box 16 and 17 being provided against the housing 1 for sealing the shafts 5 and 6, respectively.
- the shaft journals 13 and 14 are coupled to one another outside the lantern via corresponding gear elements 17 and 18, for example gear wheels, the gear element 17 being connected to a drive 20 via a gear 19. Via this drive 20 and the gear 19, at least the gear element 17 is rotated, which is transmitted to the shaft 5.
- This rotary movement can be transmitted to the gear element 18 in the same or opposite directions and at the same or different speed.
- Corresponding transmission gears are customary in the trade and should not be described in more detail here.
- shaft 5 is also referred to below as the main shaft and shaft 6 as the cleaning shaft.
- Kneading and transport elements 7 are placed on each shaft 5 and 6, which have disc surfaces 21 as the basis for the respective shaft 5 and 6.
- Various exemplary embodiments of disk surfaces 21 are shown in FIGS. 5 to 7.
- FIGS. 13 and 14 and 18 and 19 A further variant of a disk surface 21 e can be found in FIGS. 13 and 14 and 18 and 19. There, a disk surface circumference 23 is no longer circular, but has wavy indentations 24.
- the kneading and transport elements 7 on the main shaft 5 as well as on the cleaning shaft 6 are identical except for the configuration of the disk surfaces 21, they should be provided with the same reference numbers below. Of course, this leaves open within the scope of the present invention that the kneading and transport elements 7 on the main shaft 5 are configured differently than those on the cleaning shaft 6.
- an actual support leg 26 sits on the disk surface circumference 23, while wings 27 and 28 protrude from this support leg 26 on both sides of the respective shaft 5 or 6. This then results in a kneading and transport element 7, as shown in particular in FIG. 2, which has a T-shaped configuration when viewed from above.
- the disk surfaces 21 of the main shaft 5 and cleaning shaft 6 are arranged offset to one another.
- This offset is preferably such that a disk surface 21 of the cleaning shaft 6 engages approximately centrally between two disk surfaces 21 of the main shaft 5.
- this offset can also occur off-center, in which case knee spaces 29 of different widths then arise.
- the design of identical knee spaces 29 is preferred.
- kneading bars 25 are inclined in relation to the axial direction of the shafts 5 and 6, respectively. This improves the transport effect. Furthermore, arrows 30 and 31 indicate that the main shaft and cleaning shaft rotate in opposite directions.
- the number of kneading bars on the disc surfaces of the cleaning shaft is normally the same as the kneading bars on the Disc areas of the main shaft in the inverse ratio of the speeds of both shafts.
- the traces of the main shaft's kneading bars on the cleaning shaft can be identical, the number of kneading bars on the main shaft can also be reduced, if desired.
- FIGS. 8 and 9 The advantageous cleaning effect of the present invention compared to, for example, CH-PS 506 322 can be clearly seen when comparing FIGS. 8 and 9.
- Fig. 8 hatched, not cleaned surfaces 32 are still present on a disk surface 21 to a relatively large extent.
- 9 on the other hand, it can be seen that there are no more contiguous, uncleaned surfaces, but that only certain areas 32 a near the main shaft 5 and certain areas 32 b around the kneading bars 25 have not been cleaned.
- the areas which have not been cleaned are thus so minimal that the heat exchange between the disk surface 21 and the product to be treated is improved to a very excellent degree.
- FIGS. 10 to 14 differ from those just described in that the main shaft 5 is synchronized with the cleaning shaft 6. This is shown by the two arrows 30 a and 30 b. Furthermore, both shafts 5 and 6 run at the same speed, so that the number of kneading bars 25 arranged on the disk surfaces 21 is also the same. Only the disk surfaces 21 are on the two Shafts 5 and 6 are offset from each other or stand on a gap.
- the wavy indentations 24 in the disc surfaces 21 e acc. 13 and 14 allow faster product transport or faster passage of gases or vapors.
Abstract
Description
Die Erfindung betrifft einen Mischkneter zur Durchführung von mechanischen, chemischen und/oder thermischen Prozessen mit mindestens zwei achsparallelen rotierenden Wellen, wobei auf der als Hauptwelle bezeichneten einen Welle Scheibenflächen mit an ihrem Umfang angeordneten Knetbarren vorgesehen sind, welche von Knetbarren bestrichen werden, die an Scheibenflächen auf der als Putzwelle bezeichneten anderen Welle angeordneten sind, wobei die Knetbarren zweier benachbarter Scheibenflächen auf der Hauptwelle bzw. auf der Putzwelle einen Abstand zueinander einhalten, durch welchen die Scheibenfläche mit dem Knetbarren auf der Putzwelle bzw. der Hauptwelle hindurchfährt.The invention relates to a mixer kneader for carrying out mechanical, chemical and / or thermal processes with at least two axially parallel rotating shafts, disk surfaces with kneading bars arranged on their periphery being provided on the one shaft referred to as main shaft, which are coated by kneading bars which are on disk surfaces are arranged on the other shaft referred to as the cleaning shaft, the kneading bars of two adjacent disk surfaces on the main shaft or on the cleaning shaft maintaining a distance from one another through which the disk surface with the kneading bar on the cleaning shaft or the main shaft passes.
Eine derartige mehrspindelige Misch- und Knetmaschine ist beispielsweise aus der CH-A-506 322 bekannt. Deren eine Welle ist mit radialen Scheibenelementen und zwischen den Scheiben angeordneten axial ausgerichteten Knetbarren versehen und wird als Scheibenwelle bezeichnet. Zwischen diese Scheiben greifen rahmenartig geformte Knetelemente ein, welche auf der zweiten parallelen Rührwelle angeordnet sind. Diese Knetelemente reinigen die Scheiben und Knetbarren der Scheibenwelle.Such a multi-spindle mixing and kneading machine is known, for example, from CH-A-506 322. One of the shafts is provided with radial disk elements and axially aligned kneading bars arranged between the disks and is referred to as a disk shaft. Kneading elements shaped like frames engage between these disks and are arranged on the second parallel stirrer shaft. These kneading elements clean the discs and kneading bars of the disc shaft.
Um eine einigermassen ausreichende Reinigung der Scheibenflächen zu erzielen, muss die Rührwelle um ein vorgesehenes Drehzahlverhältnis schneller drehen als die Scheibenwelle. Dieses Drehzahlverhältnis hängt vor allem von der Anzahl der Knetbarren auf den Scheibenelementen ab, da die Knetelemente in die Zwischenräume zwischen die Knetbarren eingreifen müssen. Hierdurch ergibt sich eine zu geringe Reinigungswirkung der Scheibenflächen, was sich wiederum negativ auf die Wärmeübertragung auf das zu behandelnde Produkt auswirkt.In order to achieve a reasonably sufficient cleaning of the disc surfaces, the agitator shaft must rotate faster than the disc shaft by an intended speed ratio. This speed ratio depends primarily on the number of kneading bars on the disc elements, since the kneading elements have to intervene in the spaces between the kneading bars. This results in an insufficient cleaning effect of the pane surfaces, which in turn has a negative effect on the heat transfer to the product to be treated.
Ähnliches gilt auch für eine Vorrichtung entsprechend der DE-A-20 12 294, der EP-A-0 144 092 und der CH-A-565 585.The same applies to a device according to DE-A-20 12 294, EP-A-0 144 092 and CH-A-565 585.
Aus der FR-A 1 197 720 sind auf zwei gleichläufig drehende Wellen stern- oder kreuzförmige Elemente aufgesetzt, die an ihrem äußeren Umfang axial verlaufende Stangen besitzen. Mit diesen Elementen kann lediglich gerührt, aber keine Mischung bzw. Knetwirkung erzielt werden.From FR-A 1 197 720, star-shaped or cross-shaped elements are placed on two shafts rotating in the same direction and have axially extending rods on their outer circumference. These elements can only be used for stirring, but no mixing or kneading effect can be achieved.
Aus Patent Abstracts of Japan, vol 13, Nr. 29 (C562) 3377, 23.01.1989 ist eine Mischeinrichtung bekannt, bei der auf zwei benachbarten Wellen elliptische Scheibenelemente sitzen, die an ihren äusseren Enden Barren tragen. Bei diesen elliptischen Scheibenelementen ist nur eine geringe Fläche für eine Wärmeübertragung gegeben.A mixing device is known from Patent Abstracts of Japan, vol. 13, no. 29 (C562) 3377, January 23, 1989, in which elliptical disk elements are seated on two adjacent shafts which carry bars at their outer ends. With these elliptical disk elements, there is only a small area for heat transfer.
Ein Mischkneter der eingangs erwähnten Art ist aus der EP-A-0 460 466 mit dem Anmeldedatum 24.05.91, dem Prioritätsdatum 05.06.90 und dem Veröffentlichungsdatum 11.12.91 bekannt. Dort sind auf zwei benachbarten Wellen kreisförmige Scheiben aufgesetzt, die verteilt auf ihrem Umfang Knetbarren tragen. Da beide Wellen gleich schnell rotieren, ergeben sich bezüglich der Abreinigung ähnliche Probleme, wie bei dem Mischkneter nach der CH-A-506 322. Weite Bereiche der Scheibenflächen werden nicht abgereinigt.A mixer kneader of the type mentioned at the outset is known from EP-A-0 460 466 with the filing date 24.05.91, the priority date 05.06.90 and the publication date 11.12.91. There are circular discs placed on two adjacent shafts, which carry kneading bars distributed over their circumference. Since both shafts rotate at the same speed, cleaning problems arise similar to those with the mixer kneader according to CH-A-506 322. Large areas of the disk surfaces are not cleaned.
Der vorliegenden Erfindung liegt die Aufgabe zugrunde, die Reinigung sämtlicher Bereiche und Teile innerhalb des Mischkneters und gleichzeitig die auf das Produkt ausgeübte Knetwirkung wesentlich zu verbessern. Bei einer thermischen Behandlung des Produktes kommt als Aufgabe hinzu, dass die Wärmetauscherfläche innerhalb des Mischkneters erhöht und die Wärmeübertragung auf das Produkt wesentlich verbessert wird.The present invention has for its object to significantly improve the cleaning of all areas and parts within the mixing kneader and at the same time the kneading effect exerted on the product. In the case of thermal treatment of the product, there is also the task that the heat exchanger area within the mixing kneader is increased and the heat transfer to the product is significantly improved.
Zur Lösung dieser Aufgabe führt, dass dem Knetbarren beidseits Flügel angeformt sind, welche radial in geringem Abstand zu den Scheibenflächen der Hauptwelle bzw. Putzwelle verlaufen, und daß die Scheibenflächen zumindest der Hauptwelle an ihrem äußeren Umfang sägezahnartig ausgebildet oder mit wellenförmigen Einbuchtungen versehen sind.To achieve this object, wings are formed on both sides of the kneading bar, which run radially at a short distance from the disk surfaces of the main shaft or cleaning shaft, and that the disk surfaces of at least the main shaft are sawtooth-like on their outer circumference or are provided with wavy indentations.
Im Gegensatz zum Stand der Technik braucht damit nicht mehr Rücksicht auf einen durchgehenden Knetbarren genommen zu werden, so dass auch Bereiche der Scheibenflächen bzw. der Hauptwelle gereinigt werden können, die bislang dem Reinigungselement nicht zugänglich waren. Durch die Knetbarren auf den Scheibenelementen der Hauptwelle wird auch die Putzwelle gereinigt. Aus diesem Grunde ist es möglich in einem thermischen Prozess auch die Scheibenflächen der Putzwelle zu beheizen, da hier die Wärmeaustauschfläche der Putzwelle ebenfalls gereinigt wird und somit Anbackungen vermieden werden.In contrast to the prior art, it is no longer necessary to take into account a continuous kneading bar, so that areas of the disk surfaces or the main shaft can also be cleaned that were previously not accessible to the cleaning element. The cleaning shaft is also cleaned by the kneading bars on the disc elements of the main shaft. For this reason, it is possible to heat the disk surfaces of the cleaning shaft in a thermal process, since the heat exchange surface of the cleaning shaft is also cleaned here and caking is thus avoided.
Werden nun den Knetbarren beiseits Flügel angeformt, die sich radial in geringem Abstand zwischen der Haupt- bzw. Putzwelle und dem Knetbarren erstrecken, so werden die Scheibenflächen auf der Hauptwelle und der Putzwelle nahezu vollständig gereinigt. Damit bietet es sich an, auch diese Scheibenflächen beheizbar auszubilden, so dass nochmals eine Erhöhung der Wärmeübertragungsflächen stattfindet. Dabei versteht es sich von selbst, dass sowohl zwischen den Flügeln als auch den Knetbarren sowie auch der Innenwand des Mischkneters eine Vielzahl von Knetspalten gebildet werden, durch welche die Knetung des Produktes in dem erfindungsgemässen Mischkneter wesentlich verbessert wird.If wings are now formed on the kneading bars which extend radially at a short distance between the main or cleaning shaft and the kneading bar, the disk surfaces on the main shaft and the cleaning shaft are almost completely cleaned. It is therefore advisable to also design these disc surfaces to be heatable, so that the heat transfer surfaces are increased again. It goes without saying that A large number of kneading gaps are formed both between the blades and the kneading bars and also the inner wall of the mixing kneader, by means of which the kneading of the product in the mixing kneader according to the invention is substantially improved.
Wird ein schnellerer Transport des Produktes gewünscht, so sind die Scheibenflächen sägezahnartig, ausgebildet oder weisen wellenförmige Ausbuchtungen auf.If a faster transport of the product is desired, the disk surfaces are sawtooth-shaped, or they have wavy bulges.
Es soll nicht unerwähnt bleiben, dass der Träger für die Knetbarren auf der Putzwelle nicht unbedingt als Scheibenfläche ausgebildet sein muss. Je nach Kundenwunsch könnte die Verbindung von Knetbarren und Putzwelle auch durch einen einfachen Stamm erfolgen, der durch den oben erwähnten Abstand der Knetbarren zweier benachbarter Scheibenelemente auf der Hauptwelle hindurchgleiten kann. In vielen Fällen sind aber Scheibenflächen vorzuziehen, da sie zur Erhöhung des Wärmeaustausches und zur Verbesserung der Knetwirkung beitragen.It should not go unmentioned that the carrier for the kneading bars on the cleaning shaft does not necessarily have to be designed as a disk surface. Depending on the customer's requirements, the kneading bar and cleaning shaft could also be connected by a simple stem that can slide through the above-mentioned distance of the kneading bars of two adjacent disc elements on the main shaft. In many cases, however, pane surfaces are preferable because they contribute to increasing the heat exchange and improving the kneading effect.
Durch den Abstand zwischen den Knetbarren von benachbarten Scheibenelementen der Hauptwelle wird wiederum bewirkt, dass die Scheibenflächen der Putzwelle bzw. ein oben erwähnter Stamm auf Lücke mit den Scheibenflächen der Hauptwelle stehen. Bevorzugt sind sogar die Scheibenflächen bzw. der Stamm mittig zwischen jeweils zwei Scheibenflächen der Hauptwelle angeordnet. Es versteht sich von selbst, dass bei einer bevorzugt identischen Ausbildung der Knetbarren von Hauptwelle und Putzwelle nicht nur zwei benachbarte Knetbarren der Hauptwelle einen Abstand einhalten, sondern dieser Abstand auch von zwei benachbarten Knetbarren der Putzwelle, allerdings versetzt, gebildet wird, durch den dann die Scheibenfläche der Hauptwelle streicht.The distance between the kneading bars of adjacent disk elements of the main shaft in turn causes the disk surfaces of the cleaning shaft or an above-mentioned stem to be in gap with the disk surfaces of the main shaft. Even the disk surfaces or the stem are preferably arranged centrally between two disk surfaces of the main shaft. It goes without saying that if the kneading bars of the main shaft and cleaning shaft are preferably identical, not only are two adjacent kneading bars of the main shaft spaced apart, but this distance is also formed by two adjacent kneading bars of the cleaning shaft, but offset, by which then the Disc surface of the main shaft strokes.
Während die Knetbarren bevorzugt identisch ausgebildet sind, kann dies zwar auch für die Scheibenflächen von Hauptwelle und Putzwelle gelten, sie können jedoch je nach Wunsch des Anwenders auch unterschiedlich ausgebildet sein, so dass ein Produkttransport durch die Putzwelle anders vonstatten geht als durch die Hauptwelle. Hier lässt die Erfindung viele Möglichkeiten offen.While the kneading bars are preferably of identical design, this can also apply to the disc surfaces of the main shaft and cleaning shaft, but they can also be designed differently, depending on the user's request, so that product transport through the cleaning shaft is different from that through the main shaft. The invention leaves many possibilities open here.
In einem Ausführungsbeispiel der Erfindung drehen Hauptwelle und Putzwelle im gleichen Uhrzeigersinn. Genau so lassen die erfindungsgemässen Scheiben- bzw. Reinigungselemente jedoch auch ein Drehen der Hauptwelle und Putzwelle im gegenläufigen Uhrzeigersinn zu. Ferner ist es möglich, Hauptwelle und Putzwelle mit gleicher oder aber auch mit unterschiedlicher Drehzahl zu drehen. Bei einer Drehung, sei es gleichläufig oder gegenläufig, mit gleicher Drehzahl sollte die Anzahl der Knetbarren auf der Hauptwelle derjenigen auf der Putzwelle entsprechen. Dadurch lässt sich die für diese Drehzahl günstigste Reinigung ermöglichen, ohne dass sich die gegenseitigen Knetbarren stören.In one embodiment of the invention, the main shaft and cleaning shaft rotate in the same clockwise direction. However, the disc or cleaning elements according to the invention also allow the main shaft and Cleaning wave in the counterclockwise direction. It is also possible to rotate the main shaft and cleaning shaft at the same or different speeds. When rotating, whether in the same direction or in opposite directions, at the same speed, the number of kneading bars on the main shaft should correspond to that on the cleaning shaft. This enables the most economical cleaning for this speed without interfering with the kneading bars.
Drehen dagegen Hauptwelle und Putzwelle mit unterschiedlicher Drehzahl, so sollte die Anzahl der auf der Hauptwelle und der auf der Putzwelle angeordneten Knetbarren umgekehrt proportional zum Drehzahlverhältnis sein. Ist beispielsweise das Drehzahlverhältnis von Hauptwelle zu Putzwelle 1 : 4, so sind auf der Hauptwelle vier Knetbarren und auf der Putzwelle nur ein Knetbarren augeordnet. Es können auch auf der Hauptwelle acht und auf der Putzwelle zwei Knetbarren vorgesehen sein.On the other hand, if the main shaft and cleaning shaft rotate at different speeds, the number of kneading bars arranged on the main shaft and on the cleaning shaft should be inversely proportional to the speed ratio. For example, if the speed ratio of the main shaft to the cleaning shaft is 1: 4, then four kneading bars are arranged on the main shaft and only one kneading bar on the cleaning shaft. Eight kneading bars can also be provided on the main shaft and two kneading bars on the cleaning shaft.
Ist das Drehzahlverhältnis ungerade, beispielsweise 1 : 1,25, so sind auf der Hauptwelle fünf Knetbarren und auf der Putzwelle vier Knetbarren angeordnet.If the speed ratio is odd, for example 1: 1.25, five kneading bars are arranged on the main shaft and four kneading bars on the cleaning shaft.
Zusammenfassend muss hervorgehoben werden, dass der vorliegende Mischkneter eine grosse Flexibilität bezügl. der Anordnung der Wellenelemente, der Anzahl der Knetbarren und des Drehzahlverhältnisses erlaubt. Die Hauptvorteile bestehen in einer verbesserten Selbstreinigung, einer grösseren spezifischen Wärmeaustauschfläche, einer wirksameren Oberflächenerneuerung bei diffusionbestimmten Ausdampfprozessen, einer intensiveren Mischwirkung bei schonender Knetung und geringerer Kompaktierung sowie einem engen Verweilzeitspektrum.In summary, it must be emphasized that the present mixer kneader is extremely flexible. the arrangement of the shaft elements, the number of kneading bars and the speed ratio allowed. The main advantages are improved self-cleaning, a larger specific heat exchange surface, a more effective one Surface renewal with diffusion-determined evaporation processes, a more intensive mixing effect with gentle kneading and less compacting as well as a narrow residence time spectrum.
Weitere Vorteile, Merkmale und Einzelheiten der Erfindung ergeben sich aus der nachfolgenden Beschreibung bevorzugter Ausführungsbeispiele sowie anhand der Zeichnung; diese zeigt in
- Fig. 1
- eine Draufsicht auf einen erfindungsgemässen Mischkneter mit einem teilweise aufgeschnittenen Gehäuse;
- Fig. 2
- eine Draufsicht auf einen Ausschnitt von zwei zusammenwirkenden Wellen;
- Fig. 3
- eine Draufsicht auf einen Ausschnitt einer Abwicklung der einen Welle gem. Fig.2;
- Fig. 4
- eine Draufsicht auf einen Ausschnitt einer Abwicklung der anderen Welle gem. Fig. 2;
- Fig. 5
- einen Querschnitt durch die beiden Wellen gem. Fig. 2 entlang Linie V - V;
- Fig. 6 und 7
- Querschnitte durch weitere Ausführungsbeispiele von Wellen entsprechend Fig. 5;
- Fig. 8
- einen Querschnitt durch eine Hauptwelle mit schraffiert angedeuteter Darstellung von nicht gereinigten Flächen auf Scheibenelementen nach der CH - PS 506 322;
- Fig. 9
- einen Querschnitt durch eine Hauptwelle mit schraffiert angedeuteten nicht gereinigten Flächen entsprechend der vorliegenden Erfindung;
- Fig. 10
- eine Draufsicht auf einen Ausschnitt aus einem weiteren Ausführungsbeispiel eines erfindungsgemässen Mischkneters im Bereich von zwei zusammenwirkenden Wellen;
- Fig. 11
- eine Draufsicht auf einen Ausschnitt einer Abwicklung der einen Welle aus Fig. 10;
- Fig. 12
- eine Draufsicht auf einen Ausschnitt einer Abwicklung der anderen Welle gem. Fig. 10;
- Fig. 13
und 14 - schematisch dargestellte Querschnitte durch die beiden Wellen gem. Fig. 10 entlang Linie XIV - XIV;
- Fig. 15
- eine Draufsicht auf einen Ausschnitt eines weiteren Ausführungsbeispiels eines Mischkneters im Bereich von zwei zusammenwirkenden Wellen;
- Fig. 16
- eine Draufsicht auf einen Ausschnitt aus einer Abwicklung der einen Welle nach Fig. 16;
- Fig. 17
- eine Draufsicht auf einen Ausschnitt aus der Abwicklung der anderen Welle gem. Fig. 16;
- Fig. 18
und 19 - Querschnitte durch die beiden Wellen entlang Linie XX - XX in Fig. 16.
- Fig. 1
- a plan view of an inventive mixer kneader with a partially cut housing;
- Fig. 2
- a plan view of a section of two interacting shafts;
- Fig. 3
- a plan view of a section of a settlement of a wave acc. Fig.2;
- Fig. 4
- a plan view of a section of a settlement of the other wave acc. Fig. 2;
- Fig. 5
- a cross section through the two waves acc. 2 along line V - V;
- 6 and 7
- Cross sections through further embodiments of waves according to Fig. 5;
- Fig. 8
- a cross section through a main shaft with hatched representation of not cleaned surfaces on disc elements according to CH - PS 506 322;
- Fig. 9
- a cross section through a main shaft with hatched, not cleaned surfaces according to the present invention;
- Fig. 10
- a plan view of a section of a further embodiment of a mixer kneader according to the invention in the region of two interacting shafts;
- Fig. 11
- a plan view of a section of a development of the one shaft from FIG. 10;
- Fig. 12
- a plan view of a section of a settlement of the other wave acc. Fig. 10;
- 13 and 14
- schematically illustrated cross sections through the two waves acc. 10 along line XIV - XIV;
- Fig. 15
- a plan view of a section of a further embodiment of a mixer kneader in the region of two interacting shafts;
- Fig. 16
- a plan view of a section of a development of the one shaft of FIG. 16;
- Fig. 17
- a plan view of a section of the development of the other wave acc. Fig. 16;
- 18 and 19
- Cross sections through the two waves along line XX - XX in FIG. 16.
Ein Mischkneter P weist gem. Fig. 1 ein Gehäuse 1 auf, welches aus mehreren Gehäuseabschnitten 1 a, 1 b und 1 c besteht. Die Gehäuseabschnitte sind miteinander durch entsprechende Flanschverbindungen 2 gekoppelt. Im Gehäuseabschnitt 1 a ist ein Aufgabestutzen 3 für ein in dem Mischkneter zu behandelndes Produkt und in dem Gehäuseabschnitt 1 c ein Auslassstutzen 4 für das behandelte Produkt vorgesehen.A mixer kneader P has gem. Fig. 1, a housing 1, which consists of several housing sections 1 a, 1 b and 1 c. The housing sections are coupled to one another by corresponding
Das Produkt wird vom Aufgabestutzen 3 zum Auslassstutzen 4 mittels zweier Wellen 5 und 6 sowie daran angeordneten Knet- und Transportelementen 7 transportiert. Während des Transportes findet eine Mischung und Knetung des Produktes sowie bevorzugt eine thermische Behandlung statt. Hierzu sind die Wellen 5 und 6 und gegebenenfalls auch die Knet- und Transportelemente 7 sowie, nicht näher gezeigt, die Gehäusewandung 8 beheizt. Zum Einbringen eines Heizmediums in die Wellen 5 und 6 und von dort gegebenenfalls in das Innere der Knet- und Transportelemente 7 sind Anschlüsse 9 und 10 vorgesehen, wobei diese Anschlüsse 9 und 10 um entsprechende Auslassnippel 11 und 12 für das durch die Wellen 5 und 6 geführte Heizmedium angeordnet sind. Eine entsprechende Führung des Heizmediums in Mantelflächen der Wellen 5 und 6 und eine entsprechende Rückführung durch die Auslassnippel 11 und 12 sind Stand der Technik und werden deshalb nicht weiter beschrieben.The product is transported from the feed nozzle 3 to the outlet nozzle 4 by means of two
Zwischen den Anschlüssen 9 und 10 durchgreifen mit den Wellen 5 und 6 verbundene Wellenzapfen 13 und 14 eine Laterne 15, wobei gegen das Gehäuse 1 jeweils eine Stopfbüchse 16 und 17 zur Abdichtung der Welle 5 bzw. 6 vorgesehen ist. Die Wellenzapfen 13 und 14 sind ausserhalb der Laterne über entsprechende Getriebeelemente 17 und 18, beispielsweise Zahnräder, miteinander gekoppelt, wobei das Getriebeelement 17 über ein Getriebe 19 mit einem Antrieb 20 verbunden ist. Über diesen Antrieb 20 und das Getriebe 19 wird zumindest das Getriebeelement 17 in Drehbewegung versetzt, welche auf die Welle 5 übertragen wird. Eine Übertragung dieser Drehbewegung auf das Getriebeelement 18 kann gleich- oder gegensinnig sowie mit gleicher oder unterschiedlicher Drehzahl erfolgen. Entsprechende Übersetzungsgetriebe sind handelsüblich und sollen hier nicht näher beschrieben sein.Between the
Wesentlich im Rahmen der vorliegenden Erfindung ist die Ausgestaltung der Knet- und Transportelemente 7 und ihre Anordnung auf den Wellen 5 und 6. Der Übersichtlichkeit halber wird im folgenden die Welle 5 auch als Hauptwelle und die Welle 6 auch als Putzwelle bezeichnet. Jeder Welle 5 bzw. 6 sind Knet- und Transportelemente 7 aufgesetzt, welche als Basis zur jeweiligen Welle 5 bzw. 6 hin Scheibenflächen 21 besitzen. In den Figuren 5 bis 7 sind verschiedene Ausführungsbeispiele von Scheibenflächen 21 gezeigt.The design of the kneading and
Einen besseren Produkttransport ermöglicht eine sägezahnartig ausgebildete Scheibenfläche 21 b gem. Fig. 5. In Fig. 6 ist dargestellt, dass die Scheibenflächen 21 c auf der Putzwelle 6 nur noch als Flügel ausgebildet sind, während Scheibenflächen 21 d nach Fig. 7 Ausnehmungen 22 aufweisen, durch welche hindurch das zu bearbeitende Produkt transportiert werden kann.A sawtooth-like disc surface 21 b according to FIG. FIG. 5. It is shown in FIG. 6 that the disc surfaces 21c on the
Eine weitere Variante von einer Scheibenfläche 21 e findet sich in den Figuren 13 und 14 sowie 18 und 19. Dort ist ein Scheibenflächenumfang 23 nicht mehr kreisförmig ausgebildet, sondern weist wellenförmige Einbuchtungen 24 auf.A further variant of a
Da bevorzugt die Knet- und Transportelemente 7 sowohl auf der Hauptwelle 5 als auch auf der Putzwelle 6 bis auf die Ausgestaltung der Scheibenflächen 21 identisch ausgebildet sind, sollen sie nachfolgend mit den gleichen Bezugszahlen versehen sein. Dies lässt natürlich im Rahmen der vorliegenden Erfindung offen, dass die Knet- und Transportelemente 7 auf der Hauptwelle 5 anders ausgestaltet sind als diejenigen auf der Putzwelle 6.Since preferably the kneading and
Wesentlich ist, dass sich auf dem Scheibenflächenumfang 23 sowohl der Hauptwelle 5 wie auch, sofern eine Scheibenfläche 21 vorgesehen ist, der Putzwelle 6 Knetbarren 25 befinden, welche U-förmig ausgestaltet sind. D.h., ein eigentlicher Tragschenkel 26 sitzt auf dem Scheibenflächenumfang 23, während zur jeweiligen Welle 5 bzw. 6 hin von diesem Tragschenkel 26 beidseits Flügel 27 und 28 abragen. Auf diese Weise ergibt dann ein Knet- und Transportelement 7, wie insbesondere in Fig. 2 gezeigt, welches bei einer Draufsicht eine T-förmige Ausgestaltung aufweist.It is essential that both the
Wesentlich ist ferner, dass zwei benachbarte Knet- und Transportelemente 7 bzw. deren benachbarte Flügel 27 einen Abstand a voneinander einhalten, der es erlaubt, dass eine Scheibenfläche 21 der gegenüberliegenden Welle 5 bzw. 6 durch ihn hindurchfahren kann. Dementsprechend ist dieser Abstand a geringfügig grösser als die Dicke d einer Scheibenfläche 21.It is also essential that two adjacent kneading and
Ferner sind die Scheibenflächen 21 von Hauptwelle 5 und Putzwelle 6 versetzt zueinander angeordnet. Vorzugsweise ist dieser Versatz so, dass eine Scheibenfläche 21 der Putzwelle 6 etwa mittig zwischen zwei Scheibenflächen 21 der Hauptwelle 5 eingreift. Allerdings kann dieser Versatz auch aussermittig erfolgen, wobei dann entsprechend unterschiedlich breite Kneträume 29 entstehen. Bevorzugt wird allerdings die Ausgestaltung gleicher Kneträume 29.Furthermore, the disk surfaces 21 of the
In Fig. 3 und 4 ist erkennbar, dass die Knetbarren 25 im Verhältnis zur Axialrichtung der Wellen 5 bzw. 6 schräg angestellt sind. Hierdurch wird die Transportwirkung verbessert. Ferner ist durch die Pfeile 30 und 31 angedeutet, dass Hauptwelle und Putzwelle gegenläufig drehen.3 and 4 it can be seen that the kneading bars 25 are inclined in relation to the axial direction of the
In den Fig. 5 bis 7 ist das Zusammenspiel der Knet- und Transportelemente von Hauptwelle 5 und Putzwelle 6 gezeigt. Dabei findet eine gegenläufige Bewegung von Hauptwelle 5 zu Putzwelle 6 im Verhältnis 1 : 4 statt, d.h., die Putzwelle 6 dreht viermal so schnell wie die Hauptwelle 5. Somit ergibt sich, dass auf der Hauptwelle bzw. den dort angeordneten Scheibenflächen 21 b acht Knetbarren 25 vorgesehen sind, während auf den Scheibenflächen 21 a-d der Putzwelle 6 zwei Knetbarren genügen, welche diametral gegenüberliegen. Hier wäre auch die Möglichkeit gegeben, auf den Scheibenflächen der Putzwelle nur einen Knetbarren anzuordnen, während auf den Scheibenflächen der Hauptwelle vier Knetbarren vorgesehen sind. D.h.,die Anzahl der Knetbarren auf den Scheibenflächen der Putzwelle steht im Normalfall zu den Knetbarren auf den Scheibenflächen der Hauptwelle im umgekehrten Verhältnis der Drehzahlen beider Wellen. Da allerdings die Spuren der Knetbarren der Hauptwelle auf der Putzwelle identisch sein können, kann die Anzahl der Knetbarren auf der Hauptwelle, falls gewünscht, auch reduziert werden.5 to 7, the interaction of the kneading and transport elements of the
Die vorteilhafte Reinigungswirkung der vorliegenden Erfindung gegenüber beispielsweise der CH-PS 506 322 ist beim Vergleich der Fig. 8 und 9 deutlich zu erkennen. In Fig. 8 sind, schraffiert dargestellte, nicht gereinigte Flächen 32 in noch relativ grossem Ausmass auf einer Scheibenfläche 21 vorhanden. In Fig. 9 ist dagegen erkennbar, dass keine zusammenhängenden nicht gereinigten Flächen mehr vorkommen, sondern dass lediglich gewisse Bereiche 32 a nahe der Hauptwelle 5 und gewisse Bereiche 32 b um die Knetbarren 25 herum nicht gereinigt sind. Damit sind die nicht gereinigten Flächen so minimal, dass der Wärmeaustausch zwischen Scheibenfläche 21 und dem zu behandelnden Produkt in ganz hervorragendem Masse verbessert ist.The advantageous cleaning effect of the present invention compared to, for example, CH-PS 506 322 can be clearly seen when comparing FIGS. 8 and 9. In Fig. 8, hatched, not cleaned
Die Ausführungsbeispiele in den Fig. 10 bis 14 unterscheiden sich von den eben beschriebenen dadurch, dass die Hauptwelle 5 einen Gleichlauf mit der Putzwelle 6 aufweist. Dies ist durch die beiden Pfeile 30 a und 30 b dargestellt. Ferner laufen beide Wellen 5 bzw. 6 mit gleicher Drehzahl, so dass auch die Anzahl der auf den Scheibenflächen 21 angeordneten Knetbarren 25 gleich ist. Lediglich sind die Scheibenflächen 21 auf den beiden Wellen 5 bzw. 6 versetzt zueinander angeordnet bzw. stehen auf Lücke.The exemplary embodiments in FIGS. 10 to 14 differ from those just described in that the
Die wellenförmigen Einbuchtungen 24 in den Scheibenflächen 21 e gem. den Fig. 13 und 14 erlauben einen schnelleren Produkttransport bzw. einen schnelleren Durchlass von entstehenden Gasen oder Dämpfen.The
Selbstverständlich ist auch eine nicht ganzzahlige Teilung möglich, beispielsweise wenn das Drehzahlverhältnis von Hauptwelle 5 zu Putzwelle 6 1 : 1,25 ist. In diesem Falle sind dann auf der Hauptwelle, wie in den Fig. 15 bis 19 gezeigt, fünf Knetbarren 25 angeordnet, während sich auf den Scheibenflächen 21 der Putzwelle 6 lediglich vier Knetbarren symmetrisch verteilt befinden. Somit lässt die vorliegenden Erfindung eine ausserordentliche Vielfalt von Drehzahlverhältnissen und Anzahl der Knetbarren auf jeder Scheibenfläche zu.Of course, a non-integer division is also possible, for example if the speed ratio of
Claims (11)
- Mixing kneader for carrying out mechanical, chemical and/or thermal processes, having at least two rotating shafts (5, 6) with their axes parallel, disk surfaces (21) with kneading bars (25) arranged on their periphery being provided on the one shaft designated as the main shaft (5), which are swept by kneading bars (25) arranged on disk surfaces (21) on the other shaft designated as the stripping shaft (6), the kneading bars (25) of two neighbouring disk surfaces (21) on the main shaft (5) or on the cleaning shaft (6) maintaining mutual spacing (a) through which passes the disk surface (21) with the kneading bar (25) on the stripping shaft (6) or the main shaft (5), characterised in that wings (27) which extend radially at a small distance from the disk surfaces (21) of the main shaft (5) or stripping shaft (6) are moulded to the both sides of the kneading bar (25) and in that the disk surfaces (21b, 21e) at least of the main shaft (5) are formed in the manner of sawteeth or are provided with wavy indentations (24) on their external periphery.
- Mixing kneader according to claim 1, characterised in that the kneading bars (25) of the main shaft (5) and of the stripping shaft (6) are of identical design.
- Mixing kneader according to claim 1 or 2, characterised in that the disk surfaces (21) of the main shaft (5) and stripping shaft (6) are of different design.
- Mixing kneader according to one of claims 1 to 3, characterised in that the main shaft (5) and stripping shaft (6) rotate in the same clockwise direction.
- Mixing kneader according to one of claims 1 to 3, characterised in that the main shaft (5) and stripping shaft (6) rotate in opposite directions.
- Mixing kneader according to claim 4 or 5, characterised in that main shaft (5) and stripping shaft (6) rotate at the same speed of rotation.
- Mixing kneader according to claim 6, characterised in that the number of kneading bars (25) on the main shaft (5) corresponds to that on the stripping shaft (6).
- Mixing kneader according to claim 4 or 5, characterised in that the main shaft (5) and the stripping shaft (6) rotate at different speeds of rotation.
- Mixing kneader according to claim 8, characterised in that the number of the kneading bars fitted to the main shaft (5) and to the stripping shaft (6) is inversely proportional to the ratio of the speeds of rotation.
- Mixing kneader according to claim 9, characterised in that kneading bars (25) which leave the same track on the other shaft (5, 6) in each case, have been removed.
- Mixing kneader according to at least one of claims 1 to 10, characterised in that the disk surfaces (21) of the main shaft (5) and stripping shaft (6) can be heated, as can the main shaft (5) and the stripping shaft (6) themselves.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4118884A DE4118884A1 (en) | 1991-06-07 | 1991-06-07 | MIXING kneader |
DE4118884 | 1991-06-07 |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0517068A1 EP0517068A1 (en) | 1992-12-09 |
EP0517068B1 true EP0517068B1 (en) | 1995-09-06 |
Family
ID=6433494
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP92108829A Expired - Lifetime EP0517068B1 (en) | 1991-06-07 | 1992-05-26 | Mixing kneader |
Country Status (10)
Country | Link |
---|---|
US (1) | US5407266A (en) |
EP (1) | EP0517068B1 (en) |
JP (1) | JPH06233925A (en) |
AT (1) | ATE127364T1 (en) |
AU (1) | AU653818B2 (en) |
CA (1) | CA2070539C (en) |
DE (3) | DE4118884A1 (en) |
DK (1) | DK0517068T3 (en) |
ES (1) | ES2077918T3 (en) |
RU (1) | RU2070087C1 (en) |
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Also Published As
Publication number | Publication date |
---|---|
AU653818B2 (en) | 1994-10-13 |
DE4118884A1 (en) | 1992-12-10 |
DE59203529D1 (en) | 1995-10-12 |
RU2070087C1 (en) | 1996-12-10 |
AU1807692A (en) | 1992-12-10 |
ATE127364T1 (en) | 1995-09-15 |
DE4239424A1 (en) | 1994-05-26 |
DK0517068T3 (en) | 1995-12-11 |
JPH06233925A (en) | 1994-08-23 |
EP0517068A1 (en) | 1992-12-09 |
US5407266A (en) | 1995-04-18 |
ES2077918T3 (en) | 1995-12-01 |
CA2070539A1 (en) | 1992-12-08 |
CA2070539C (en) | 2004-08-31 |
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