EA200800275A1 - Способ непрерывного производства гидроксиламмония - Google Patents

Способ непрерывного производства гидроксиламмония

Info

Publication number
EA200800275A1
EA200800275A1 EA200800275A EA200800275A EA200800275A1 EA 200800275 A1 EA200800275 A1 EA 200800275A1 EA 200800275 A EA200800275 A EA 200800275A EA 200800275 A EA200800275 A EA 200800275A EA 200800275 A1 EA200800275 A1 EA 200800275A1
Authority
EA
Eurasian Patent Office
Prior art keywords
hydroxyl ammonium
zone
synthesis zone
cyclohexanone oxime
production
Prior art date
Application number
EA200800275A
Other languages
English (en)
Other versions
EA014243B1 (ru
Inventor
Хендрик Эверинг
Олаф Портер
Original Assignee
ДСМ АйПи АССЕТС Б.В.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ДСМ АйПи АССЕТС Б.В. filed Critical ДСМ АйПи АССЕТС Б.В.
Publication of EA200800275A1 publication Critical patent/EA200800275A1/ru
Publication of EA014243B1 publication Critical patent/EA014243B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/54—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/56—Platinum group metals
    • B01J23/62—Platinum group metals with gallium, indium, thallium, germanium, tin or lead
    • B01J23/622—Platinum group metals with gallium, indium, thallium, germanium, tin or lead with germanium, tin or lead
    • B01J23/624—Platinum group metals with gallium, indium, thallium, germanium, tin or lead with germanium, tin or lead with germanium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1409—Preparation
    • C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C239/00—Compounds containing nitrogen-to-halogen bonds; Hydroxylamino compounds or ethers or esters thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrane Compounds (AREA)
  • Catalysts (AREA)

Abstract

Способ и оборудование для непрерывного производства гидроксиламмония восстановлением ионов нитрата или оксидов азота водородом в присутствии катализатора, в соответствии с которым гидроксиламмоний производится в двух или более параллельно включенных установках по производству гидроксиламмония, где способ необязательно является частью способа производства циклогексаноноксима, в котором неорганическая рабочая жидкость циркулирует из зоны синтеза гидроксиламмония (А) в зону синтеза циклогексаноноксима (В) и обратно в зону синтеза гидроксиламмония через, например, экстракционную зону (С) и зону производства азотной кислоты (D), в котором гидроксиламмоний зоны синтеза гидроксиламмония образуется восстановлением ионов нитрата или оксидов азота водородом в присутствии катализатора и в котором гидроксиламмоний зоны синтеза циклогексаноноксима реагирует с циклогексаноном для получения циклогексаноноксима.
EA200800275A 2005-07-08 2006-07-04 Способ непрерывного производства гидроксиламмония EA014243B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL2005000491 2005-07-08
PCT/EP2006/006507 WO2007006458A1 (en) 2005-07-08 2006-07-04 Process for the continuous production of hydroxylammonium

Publications (2)

Publication Number Publication Date
EA200800275A1 true EA200800275A1 (ru) 2008-06-30
EA014243B1 EA014243B1 (ru) 2010-10-29

Family

ID=35229877

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200800275A EA014243B1 (ru) 2005-07-08 2006-07-04 Способ непрерывного производства гидроксиламмония

Country Status (15)

Country Link
US (1) US20090221854A1 (ru)
EP (1) EP1901994B1 (ru)
JP (1) JP5256031B2 (ru)
KR (1) KR101311626B1 (ru)
CN (1) CN101218171B (ru)
AT (1) ATE456541T1 (ru)
BR (1) BRPI0613171A2 (ru)
DE (1) DE602006012048D1 (ru)
EA (1) EA014243B1 (ru)
MX (1) MX2008000324A (ru)
MY (1) MY143223A (ru)
PL (1) PL1901994T3 (ru)
TW (1) TWI402211B (ru)
UA (1) UA91708C2 (ru)
WO (1) WO2007006458A1 (ru)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120128569A1 (en) * 2008-10-10 2012-05-24 Hendrik Oevering Destruction of ammonium ions
KR101904568B1 (ko) * 2011-04-22 2018-10-04 캡 쓰리 비 브이 하이드록실아민의 제조 방법
WO2012143332A1 (en) * 2011-04-22 2012-10-26 Dsm Ip Assets B.V. Catalyzed hydroxylamine preparation
KR102080950B1 (ko) * 2011-12-29 2020-02-24 캡 쓰리 비 브이 하이드록실아민의 연속 제조방법
HUE044241T2 (hu) 2012-11-27 2019-10-28 Hampton Roads Sanitation Distr Gravimetriás elválasztással végzett szennyvízkezelési módszer és berendezés
CN103318858B (zh) * 2013-06-07 2016-01-27 常州大学 一种利用反应-萃取蒸馏耦合技术制备羟胺盐的方法
KR20170026495A (ko) 2014-06-30 2017-03-08 햄톤 로즈 새니테이션 디스트릭트 외부 선택을 이용한 폐수 처리 방법 및 장치
US9902635B2 (en) 2014-07-23 2018-02-27 Hampton Roads Sanitation District Method for deammonification process control using pH, specific conductivity, or ammonia

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE759915A (fr) * 1969-12-06 1971-06-04 Stamicarbon Procede de recyclage pour la preparation et le traitement d'unesolutionde sel d'hydroxylammonium
US3940442A (en) * 1969-12-06 1976-02-24 Stamicarbon B.V. Recycle process for the preparation and processing of a hydroxylammonium salt solution
NL7507911A (nl) * 1975-07-03 1977-01-05 Stamicarbon Werkwijze voor de bereiding van een hydroxylamine- zout.
DE3107702A1 (de) * 1981-02-28 1982-09-16 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen herstellung von hydroxylammoniumsalzen
KR830007476A (ko) * 1981-12-18 1983-10-21 전민제 에탄올의 탈수공정에 의한 에틸렌의 제조방법
FR2678944B1 (fr) * 1991-07-10 1993-11-19 Total Raffinage Distribution Sa Procede et dispositif pour le remplacement en continu du catalyseur dans une unite a lit mobile.
JP2604358Y2 (ja) * 1993-04-09 2000-05-08 ザ・ビーオーシー・グループ・インコーポレーテッド 窒素発生装置
BE1009767A3 (nl) * 1995-11-10 1997-08-05 Dsm Nv Werkwijze voor de bereiding van hydroxylammoniumzouten.
NL1013899C2 (nl) * 1999-12-21 2001-06-25 Dsm Nv Werkwijze voor het bereiden en zuiveren van een hydroxylammoniumzoutoplossing.
MXPA02011960A (es) * 2000-06-05 2003-07-14 Dsm Nv Procedimiento para la preparacion de ciclohexanona oxima.
CN1391981A (zh) * 2001-06-15 2003-01-22 中国石油化工股份有限公司巴陵分公司 一种延长羟胺催化剂使用寿命的方法
EP1275616A1 (en) * 2001-07-11 2003-01-15 Dsm N.V. Process for the preparation of hydroxylammonium
BR0214646B1 (pt) * 2001-12-04 2011-05-31 processo para preparar ácido nìtrico por meio do tratamento de um meio aquoso contendo compostos orgánicos e fosfato e processo para preparar cicloexanona oxima.

Also Published As

Publication number Publication date
EA014243B1 (ru) 2010-10-29
EP1901994B1 (en) 2010-01-27
MX2008000324A (es) 2008-03-11
CN101218171A (zh) 2008-07-09
CN101218171B (zh) 2012-09-26
TWI402211B (zh) 2013-07-21
JP5256031B2 (ja) 2013-08-07
PL1901994T3 (pl) 2010-06-30
TW200710023A (en) 2007-03-16
JP2009500280A (ja) 2009-01-08
ATE456541T1 (de) 2010-02-15
KR20080023725A (ko) 2008-03-14
DE602006012048D1 (de) 2010-03-18
BRPI0613171A2 (pt) 2010-12-21
US20090221854A1 (en) 2009-09-03
MY143223A (en) 2011-03-31
WO2007006458A1 (en) 2007-01-18
EP1901994A1 (en) 2008-03-26
KR101311626B1 (ko) 2013-09-26
UA91708C2 (ru) 2010-08-25

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Legal Events

Date Code Title Description
MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM AZ BY KZ KG MD TJ TM RU