DK2635616T3 - Fremgangsmåde til fremstilling af aerogeler eller xerogeler - Google Patents

Fremgangsmåde til fremstilling af aerogeler eller xerogeler

Info

Publication number
DK2635616T3
DK2635616T3 DK11779144.2T DK11779144T DK2635616T3 DK 2635616 T3 DK2635616 T3 DK 2635616T3 DK 11779144 T DK11779144 T DK 11779144T DK 2635616 T3 DK2635616 T3 DK 2635616T3
Authority
DK
Denmark
Prior art keywords
xerogels
procedure
aerogels
manufacturing
manufacturing aerogels
Prior art date
Application number
DK11779144.2T
Other languages
English (en)
Inventor
Marc Fricke
Mark Elbing
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Application granted granted Critical
Publication of DK2635616T3 publication Critical patent/DK2635616T3/da

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7657—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings
    • C08G18/7664—Polyisocyanates or polyisothiocyanates cyclic aromatic containing two or more aromatic rings containing alkylene polyphenyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
    • C08G18/092—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture oligomerisation to isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C08G18/20—Heterocyclic amines; Salts thereof
    • C08G18/2009—Heterocyclic amines; Salts thereof containing one heterocyclic ring
    • C08G18/2036—Heterocyclic amines; Salts thereof containing one heterocyclic ring having at least three nitrogen atoms in the ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C08G18/3237—Polyamines aromatic
    • C08G18/3243—Polyamines aromatic containing two or more aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C08J3/075—Macromolecular gels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00—Use of ingredients characterised by shape
    • C08K7/22—Expanded, porous or hollow particles
    • H—ELECTRICITY
    • H01—ELECTRIC ELEMENTS
    • H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
    • H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
    • H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
    • H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2101/00—Manufacture of cellular products
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0091—Aerogels; Xerogels
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2115/00—Oligomerisation
    • C08G2115/02—Oligomerisation to isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2330/00—Thermal insulation material
    • C08G2330/50—Evacuated open-celled polymer material

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DK11779144.2T 2010-11-04 2011-10-27 Fremgangsmåde til fremstilling af aerogeler eller xerogeler DK2635616T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP10189932 2010-11-04
PCT/EP2011/068811 WO2012059388A1 (de) 2010-11-04 2011-10-27 Verfahren zur herstellung von aerogelen oder xerogelen

Publications (1)

Publication Number Publication Date
DK2635616T3 true DK2635616T3 (da) 2017-11-20

Family

ID=43736252

Family Applications (1)

Application Number Title Priority Date Filing Date
DK11779144.2T DK2635616T3 (da) 2010-11-04 2011-10-27 Fremgangsmåde til fremstilling af aerogeler eller xerogeler

Country Status (12)

Country Link
EP (1) EP2635616B1 (da)
JP (1) JP5937606B2 (da)
KR (1) KR101883022B1 (da)
CN (1) CN103314028B (da)
AU (1) AU2011325338B2 (da)
BR (1) BR112013010740A2 (da)
CA (1) CA2816739C (da)
DK (1) DK2635616T3 (da)
MX (1) MX2013004870A (da)
PL (1) PL2635616T3 (da)
RU (1) RU2577862C2 (da)
WO (1) WO2012059388A1 (da)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120235070A1 (en) 2011-03-18 2012-09-20 Basf Se Process for producing flame-retardant porous materials based on polyurea
US9188384B2 (en) 2011-03-31 2015-11-17 Basf Se Dynamically evacuable devices comprising organic aerogels or xerogels
US9321876B2 (en) 2012-09-27 2016-04-26 Basf Se Process for producing porous materials based on isocyanate
WO2014048778A1 (de) 2012-09-27 2014-04-03 Basf Se Verfahren zur herstellung von porösen materialien auf basis von isocyanat
RU2641083C2 (ru) 2012-11-05 2018-01-15 Басф Се Способ изготовления профилированных элементов
US10100513B2 (en) 2012-11-05 2018-10-16 Basf Se Process for producing profiled elements
KR102223500B1 (ko) * 2013-05-24 2021-03-08 바스프 에스이 다공질 재료의 제조 방법
MX2016003442A (es) 2013-09-16 2016-06-21 Basf Se Metodo para la produccion de aerogeles organicos a base de isocianato.
JP6559698B2 (ja) 2014-03-24 2019-08-14 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 多孔性材料の製造方法
CN106795315B (zh) * 2014-07-18 2020-08-14 巴斯夫欧洲公司 制备多孔材料的方法
US10336040B2 (en) 2014-09-25 2019-07-02 Basf Se Method for manufacturing a composite element for vacuum insulation elements
JP2018512488A (ja) 2015-03-24 2018-05-17 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 多孔性材料の製造方法
MX2017013786A (es) 2015-04-27 2018-03-27 Huntsman Int Llc Materiales porosos a base de isocianato funcionalizado.
KR20180069864A (ko) 2015-10-16 2018-06-25 바스프 에스이 무기산을 사용한 이소시아네이트에 기초한 크세로겔 및 에어로겔의 제조 방법
US11248101B2 (en) 2016-01-18 2022-02-15 Basf Se Process for producing porous materials
CN108473659A (zh) * 2016-01-18 2018-08-31 巴斯夫欧洲公司 制备多孔材料的方法
EP3315529B1 (en) * 2016-10-28 2019-12-04 Henkel AG & Co. KGaA Copolymer hybrid aerogels based on isocyanate - cyclic ether - clay networks
WO2019012127A1 (en) 2017-07-13 2019-01-17 Basf Se POROUS MATERIALS HAVING SUPERIOR REVERSIBLE WATER ABSORPTION
US20210139633A1 (en) 2017-07-17 2021-05-13 Basf Se Process for producing porous materials
EP3911694A1 (en) 2019-01-17 2021-11-24 Basf Se Process for producing porous materials

Family Cites Families (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BE791310A (fr) * 1971-11-13 1973-05-14 Bayer Ag Procede de preparation de pieces moulees en mousse
DE2940738A1 (de) * 1979-10-08 1981-04-16 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von gegebenenfalls zellhaltigen polyurethan-polyharnstoff-formkoerpern
DE3613973A1 (de) * 1986-04-25 1987-10-29 Bayer Ag Verfahren zur herstellung von polyharnstoffschaum-formteilen
GB8800281D0 (en) * 1988-01-07 1988-02-10 Univ Manchester Production of polyureas
US5478867A (en) 1993-07-07 1995-12-26 The Dow Chemical Company Microporous isocyanate-based polymer compositions and method of preparation
CA2166073A1 (en) * 1993-07-22 1995-02-02 Rik De Vos Organic aerogels
US5587448A (en) * 1994-12-29 1996-12-24 Minnesota Mining And Manufacturing Reaction system for producing a polyurethane and method of using same to seal a surface
EP0812310A1 (en) * 1995-02-27 1997-12-17 Imperial Chemical Industries Plc Novel di- and polyamino compounds for use in the preparation of polyurethane materials
JP3112250B2 (ja) * 1996-07-31 2000-11-27 アイシーケイ株式会社 現場施工用ポリウレタン系防水塗膜形成材料
JPH10195163A (ja) * 1996-11-14 1998-07-28 Asahi Glass Co Ltd 二液型硬化性組成物
ID22835A (id) * 1997-04-01 1999-12-09 Huntsman Ici Chemicals Lls Xerogel berbasis poliisosianat
JP2001263926A (ja) * 2000-03-17 2001-09-26 Matsushita Refrig Co Ltd 有機多孔体の製造方法および断熱パネルと断熱箱体
DK1523512T3 (da) * 2002-07-22 2020-03-30 Aspen Aerogels Inc Polyimide-aerogeler, carbon-aerogeler, og metalcar-bidaerogeler og fremgangsmåder til fremstilling af samme
US7704422B2 (en) * 2004-08-16 2010-04-27 Electromaterials, Inc. Process for producing monolithic porous carbon disks from aromatic organic precursors
US20060089093A1 (en) * 2004-10-27 2006-04-27 Swisher Robert G Polyurethane urea polishing pad
ES2354593T3 (es) * 2007-05-16 2011-03-16 Basf Se Xerogeles sobre la base de poliurea aromática.
DE502008003187D1 (de) * 2007-08-28 2011-05-26 Basf Se Xerogele auf basis von polyharnstoff
PL2448986T3 (pl) 2009-06-29 2014-05-30 Basf Se Porowate żele na bazie aromatycznego polimocznika
PT2510026E (pt) * 2009-12-11 2014-04-02 Basf Se Materiais porosos melhorados, à base de aminas aromáticas
EP2399945A1 (de) * 2010-06-28 2011-12-28 Basf Se Verfahren zur Herstellung von Porösen materialien auf basis von Polyharnstoff

Also Published As

Publication number Publication date
EP2635616B1 (de) 2017-08-02
CA2816739C (en) 2019-08-06
KR20140009233A (ko) 2014-01-22
MX2013004870A (es) 2013-05-22
CN103314028A (zh) 2013-09-18
CA2816739A1 (en) 2012-05-10
CN103314028B (zh) 2015-06-17
JP2013543034A (ja) 2013-11-28
BR112013010740A2 (pt) 2016-08-09
AU2011325338B2 (en) 2015-04-30
AU2011325338A1 (en) 2013-05-30
EP2635616A1 (de) 2013-09-11
JP5937606B2 (ja) 2016-06-22
KR101883022B1 (ko) 2018-07-27
RU2013125527A (ru) 2014-12-10
RU2577862C2 (ru) 2016-03-20
PL2635616T3 (pl) 2018-01-31
WO2012059388A1 (de) 2012-05-10

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