DK170027B1 - Fremgangsmåder til fremstilling af 1,3-di-(6-0-saccharose)-1,1,3,3-tetra(hydrocarbyl)distannoxan og saccharose-6-estere - Google Patents

Fremgangsmåder til fremstilling af 1,3-di-(6-0-saccharose)-1,1,3,3-tetra(hydrocarbyl)distannoxan og saccharose-6-estere Download PDF

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Publication number
DK170027B1
DK170027B1 DK352689A DK352689A DK170027B1 DK 170027 B1 DK170027 B1 DK 170027B1 DK 352689 A DK352689 A DK 352689A DK 352689 A DK352689 A DK 352689A DK 170027 B1 DK170027 B1 DK 170027B1
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Prior art keywords
sucrose
hydrocarbyl
distannoxane
reaction
tetra
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Application number
DK352689A
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Danish (da)
English (en)
Other versions
DK352689D0 (da
DK352689A (da
Inventor
Juan L Navia
Original Assignee
Noramco Inc
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Filing date
Publication date
Application filed by Noramco Inc filed Critical Noramco Inc
Publication of DK352689D0 publication Critical patent/DK352689D0/da
Publication of DK352689A publication Critical patent/DK352689A/da
Application granted granted Critical
Publication of DK170027B1 publication Critical patent/DK170027B1/da

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H11/00—Compounds containing saccharide radicals esterified by inorganic acids; Metal salts thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C07H13/06—Fatty acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H23/00—Compounds containing boron, silicon, or a metal, e.g. chelates, vitamin B12

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Saccharide Compounds (AREA)
  • Steroid Compounds (AREA)
DK352689A 1988-07-18 1989-07-17 Fremgangsmåder til fremstilling af 1,3-di-(6-0-saccharose)-1,1,3,3-tetra(hydrocarbyl)distannoxan og saccharose-6-estere DK170027B1 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US22064188 1988-07-18
US07/220,641 US4950746A (en) 1988-07-18 1988-07-18 Process for synthesizing sucrose derivatives by regioselective reaction

Publications (3)

Publication Number Publication Date
DK352689D0 DK352689D0 (da) 1989-07-17
DK352689A DK352689A (da) 1990-01-19
DK170027B1 true DK170027B1 (da) 1995-05-01

Family

ID=22824357

Family Applications (1)

Application Number Title Priority Date Filing Date
DK352689A DK170027B1 (da) 1988-07-18 1989-07-17 Fremgangsmåder til fremstilling af 1,3-di-(6-0-saccharose)-1,1,3,3-tetra(hydrocarbyl)distannoxan og saccharose-6-estere

Country Status (24)

Country Link
US (1) US4950746A (tr)
EP (1) EP0352048B1 (tr)
JP (1) JP2725710B2 (tr)
KR (1) KR0143234B1 (tr)
AR (1) AR245136A1 (tr)
AT (1) ATE114664T1 (tr)
AU (1) AU618107B2 (tr)
CA (1) CA1323625C (tr)
DE (1) DE68919566T2 (tr)
DK (1) DK170027B1 (tr)
ES (1) ES2065386T3 (tr)
FI (1) FI91874C (tr)
GR (1) GR1002250B (tr)
IE (1) IE65990B1 (tr)
IL (1) IL91004A (tr)
MX (1) MX172793B (tr)
NO (1) NO171855C (tr)
NZ (1) NZ229823A (tr)
PH (1) PH26098A (tr)
PT (1) PT91186B (tr)
RU (1) RU2041233C1 (tr)
TR (1) TR27628A (tr)
YU (1) YU47159B (tr)
ZA (1) ZA895427B (tr)

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US5089608A (en) * 1990-03-23 1992-02-18 Mcneil-Ppc, Inc. Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5023329A (en) * 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
US5034551A (en) * 1990-04-23 1991-07-23 Noramco, Inc. Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
GR910100356A (el) * 1990-08-27 1992-08-31 Mcneil Ppc Inc Καταλυόμενη μέ?οδος εστέρος-6-σακχαρόζης.
US5470969A (en) * 1990-08-27 1995-11-28 Mcneil-Ppc, Inc. Catalyzed sucrose-6-ester process
FR2670493A1 (fr) * 1990-12-13 1992-06-19 Isochem Sa Nouveaux composes monoesters du saccharose tels que les 2-0-acylsaccharoses et les 6-0-acylsaccharoses, ainsi que leurs procedes de synthese.
US5298611A (en) * 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
WO1996001832A1 (en) 1994-07-11 1996-01-25 The United States Of America, Represented By The Secretary Of The Department Of Agriculture Chemically synthesized sugar esters for the control of soft-bodied arthropods
US6608039B1 (en) 1994-07-11 2003-08-19 The United States Of America As Represented By The Secretary Of Agriculture Chemically synthesized sugar esters for the control of soft-bodied arthropods
US5498709A (en) 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
ES2191745T3 (es) 1995-11-28 2003-09-16 Mcneil Ppc Inc Procedimiento de preparacion de 6-ester de sacarosa.
US6121430A (en) * 1998-12-28 2000-09-19 University Of Iowa Research Foundation Regiospecific synthesis of glucose-based surfactants
CN1245895C (zh) 2000-11-17 2006-03-22 塔特和莱利有限公司 含三氯蔗糖和丁磺氨钾的可熔混合物的甜味剂、含有它的食品以及它们的制备方法
EP1339728B1 (en) 2000-11-17 2013-02-27 Tate & Lyle Technology Limited Improved sucralose composition and process for the crystallization thereof
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
US6943248B2 (en) 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
CN1176094C (zh) * 2003-05-23 2004-11-17 广东省食品工业研究所 一种三氯蔗糖的合成方法
US20050214425A1 (en) * 2004-03-23 2005-09-29 Roma Vazirani Sugar substitute prepared with nutritive and high-intensity sweeteners
US20090105470A1 (en) * 2005-02-22 2009-04-23 Pharmed Medicare Private Limited , A Corporation Tin Mediated Regioselective Synthesis of Sucrose-6-Esters
US7750146B2 (en) 2005-03-18 2010-07-06 Tate & Lyle Plc Granular sucralose
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
CN100418976C (zh) * 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
CN101092438A (zh) * 2006-06-22 2007-12-26 南京莱因医药科技有限公司 6－o－苯甲酰三氯半乳型蔗糖四乙酯的制备方法
GB0702854D0 (en) * 2007-01-09 2007-03-28 Tate & Lyle Plc Method for the synthesis of sucrose-6-esters
US20080227971A1 (en) * 2007-01-19 2008-09-18 Leinhos Duane A Deacylation of sucralose-6-acylates
GB0702857D0 (en) * 2007-01-19 2007-03-28 Tate & Lyle Plc Improved sucralose production method
US20090076261A1 (en) * 2007-09-13 2009-03-19 Polymed Therapeutics, Inc. Novel process for preparing sucrose-6-esters
CN101245085B (zh) * 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
US8436156B2 (en) * 2008-01-04 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US7932380B2 (en) 2008-03-06 2011-04-26 Wanhe International (Group) Co. Ltd. Process for the preparation of sucralose
US8557976B2 (en) * 2008-03-13 2013-10-15 Tate & Lyle Technology Limited Microbial consortia and methods for their use
WO2009117317A1 (en) * 2008-03-20 2009-09-24 Tate & Lyle Technology Ltd Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
WO2009124113A1 (en) * 2008-04-03 2009-10-08 Tate & Lyle Technology Ltd. Extraction of less polar impurities from sucralose containing aqueous feed streams
US20090299055A1 (en) * 2008-04-03 2009-12-03 Tate & Lyle Technology Limited Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
CN101981044B (zh) * 2008-04-03 2014-08-06 塔特和莱利技术有限公司 碳水化合物浓度对三氯半乳蔗糖萃取效率的影响
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) * 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2471348B (en) 2009-06-22 2011-12-14 Tate & Lyle Technology Ltd A method for producing sucralose-6-acylate
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB2474310B (en) * 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
CN101759728B (zh) * 2010-01-08 2012-01-11 江苏巨邦制药有限公司 三氯蔗糖的生产及精制方法
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN105829332B (zh) 2013-12-16 2018-10-02 塔特和莱利技术有限公司 蔗糖-6-酯的氯化
GB2544217B (en) 2014-08-08 2020-03-25 Tate & Lyle Tech Ltd Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
WO2017091437A1 (en) 2015-11-24 2017-06-01 Archer Daniels Midland Company Organotin catalysts in esterification processes of furan-2,5-dicarboxylic acid (fdca)
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF

Family Cites Families (4)

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Publication number Priority date Publication date Assignee Title
US4435440A (en) * 1976-01-08 1984-03-06 Tate & Lyle Limited Sweeteners
DE3065399D1 (en) * 1979-12-18 1983-11-24 Tate & Lyle Plc Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3062467D1 (en) * 1979-12-20 1983-04-28 Tate & Lyle Plc Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
EP0043649B1 (en) * 1980-07-08 1984-09-12 TATE & LYLE PUBLIC LIMITED COMPANY Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)

Also Published As

Publication number Publication date
KR0143234B1 (ko) 1998-07-01
YU47159B (sh) 1995-01-31
YU139389A (en) 1991-02-28
FI893455A0 (fi) 1989-07-17
EP0352048A2 (en) 1990-01-24
US4950746A (en) 1990-08-21
NO892926L (no) 1990-01-19
JP2725710B2 (ja) 1998-03-11
DE68919566T2 (de) 1995-04-13
NO892926D0 (no) 1989-07-17
MX16842A (es) 1993-04-01
DK352689D0 (da) 1989-07-17
EP0352048B1 (en) 1994-11-30
JPH0273096A (ja) 1990-03-13
MX172793B (es) 1994-01-13
DK352689A (da) 1990-01-19
GR1002250B (en) 1996-04-23
AU618107B2 (en) 1991-12-12
IL91004A0 (en) 1990-02-09
ES2065386T3 (es) 1995-02-16
EP0352048A3 (en) 1991-09-04
KR910002884A (ko) 1991-02-26
PT91186A (pt) 1990-02-08
NZ229823A (en) 1991-01-29
ZA895427B (en) 1991-03-27
PT91186B (pt) 1995-03-01
NO171855C (no) 1993-05-12
IL91004A (en) 1994-04-12
AR245136A1 (es) 1993-12-30
GR890100456A (el) 1990-06-27
IE892310L (en) 1990-01-18
FI91874B (fi) 1994-05-13
AU3804889A (en) 1990-01-18
RU2041233C1 (ru) 1995-08-09
IE65990B1 (en) 1995-11-29
FI91874C (fi) 1994-08-25
DE68919566D1 (de) 1995-01-12
TR27628A (tr) 1995-06-14
CA1323625C (en) 1993-10-26
PH26098A (en) 1992-02-06
NO171855B (no) 1993-02-01
FI893455A (fi) 1990-01-19
ATE114664T1 (de) 1994-12-15

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B1 Patent granted (law 1993)
PUP Patent expired