GR890100456A - Μεθοδος για την συνθεση παραγωγων σακχαροζης με επιλεκτικης περιοχης αντιδραση. - Google Patents

Μεθοδος για την συνθεση παραγωγων σακχαροζης με επιλεκτικης περιοχης αντιδραση.

Info

Publication number
GR890100456A
GR890100456A GR890100456A GR890100456A GR890100456A GR 890100456 A GR890100456 A GR 890100456A GR 890100456 A GR890100456 A GR 890100456A GR 890100456 A GR890100456 A GR 890100456A GR 890100456 A GR890100456 A GR 890100456A
Authority
GR
Greece
Prior art keywords
sucrose derivatives
regioselective reaction
synthesizing sucrose
synthesizing
sucrose
Prior art date
Application number
GR890100456A
Other languages
English (en)
Other versions
GR1002250B (en
Inventor
L Navia Juan
Original Assignee
Noramco Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Noramco Inc filed Critical Noramco Inc
Publication of GR890100456A publication Critical patent/GR890100456A/el
Publication of GR1002250B publication Critical patent/GR1002250B/el

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H11/00—Compounds containing saccharide radicals esterified by inorganic acids; Metal salts thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • C07H13/06—Fatty acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H23/00—Compounds containing boron, silicon, or a metal, e.g. chelates, vitamin B12

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Saccharide Compounds (AREA)
  • Steroid Compounds (AREA)

Abstract

Σακχαρόζη αντιδρά με 1,3-δι(υδροκαρβυλοξυ)-1,1,3,3- τετρα(υδροκαρβυλ) δικασσιτεροξάνιο για την παραγωγή 1,3-δι-(6-0-σακχαρόζη)-1,1,3,3-τετρα(υδροκαρβυλ) δικασσιτεροξάνιου, που μπορεί να ακυλιωθεί για την παραγωγή του εστέρα 6- σακχαρόζης. ω
GR890100456A 1988-07-18 1989-07-17 Method for synthesizing sucrose derivatives by regioselective reaction GR1002250B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US07/220,641 US4950746A (en) 1988-07-18 1988-07-18 Process for synthesizing sucrose derivatives by regioselective reaction

Publications (2)

Publication Number Publication Date
GR890100456A true GR890100456A (el) 1990-06-27
GR1002250B GR1002250B (en) 1996-04-23

Family

ID=22824357

Family Applications (1)

Application Number Title Priority Date Filing Date
GR890100456A GR1002250B (en) 1988-07-18 1989-07-17 Method for synthesizing sucrose derivatives by regioselective reaction

Country Status (24)

Country Link
US (1) US4950746A (el)
EP (1) EP0352048B1 (el)
JP (1) JP2725710B2 (el)
KR (1) KR0143234B1 (el)
AR (1) AR245136A1 (el)
AT (1) ATE114664T1 (el)
AU (1) AU618107B2 (el)
CA (1) CA1323625C (el)
DE (1) DE68919566T2 (el)
DK (1) DK170027B1 (el)
ES (1) ES2065386T3 (el)
FI (1) FI91874C (el)
GR (1) GR1002250B (el)
IE (1) IE65990B1 (el)
IL (1) IL91004A (el)
MX (1) MX172793B (el)
NO (1) NO171855C (el)
NZ (1) NZ229823A (el)
PH (1) PH26098A (el)
PT (1) PT91186B (el)
RU (1) RU2041233C1 (el)
TR (1) TR27628A (el)
YU (1) YU47159B (el)
ZA (1) ZA895427B (el)

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US5089608A (en) * 1990-03-23 1992-02-18 Mcneil-Ppc, Inc. Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5034551A (en) * 1990-04-23 1991-07-23 Noramco, Inc. Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds
US5023329A (en) * 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
GR910100356A (el) * 1990-08-27 1992-08-31 Mcneil Ppc Inc Καταλυόμενη μέ?οδος εστέρος-6-σακχαρόζης.
US5470969A (en) * 1990-08-27 1995-11-28 Mcneil-Ppc, Inc. Catalyzed sucrose-6-ester process
FR2670493A1 (fr) * 1990-12-13 1992-06-19 Isochem Sa Nouveaux composes monoesters du saccharose tels que les 2-0-acylsaccharoses et les 6-0-acylsaccharoses, ainsi que leurs procedes de synthese.
US5298611A (en) * 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
IL114551A0 (en) 1994-07-11 1995-11-27 Us Agriculture Chemically synthesized sugar esters for the control of soft bodied arthropods
US6608039B1 (en) 1994-07-11 2003-08-19 The United States Of America As Represented By The Secretary Of Agriculture Chemically synthesized sugar esters for the control of soft-bodied arthropods
US5498709A (en) 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
RU2159773C2 (ru) 1995-11-28 2000-11-27 МакНЕЙЛ-ППС, ИНК. Способы получения сложного эфира сахарозы по положению 6
US6121430A (en) * 1998-12-28 2000-09-19 University Of Iowa Research Foundation Regiospecific synthesis of glucose-based surfactants
US7018667B2 (en) 2000-11-17 2006-03-28 Tate & Lyle Public Limited Company Meltable form of sucralose
RU2279437C2 (ru) * 2000-11-17 2006-07-10 Тейт Энд Лайл Паблик Лимитед Компани Усовершенствованная сукралозная композиция и способ ее получения
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
CN1176094C (zh) * 2003-05-23 2004-11-17 广东省食品工业研究所 一种三氯蔗糖的合成方法
US20050214425A1 (en) * 2004-03-23 2005-09-29 Roma Vazirani Sugar substitute prepared with nutritive and high-intensity sweeteners
US20090105470A1 (en) * 2005-02-22 2009-04-23 Pharmed Medicare Private Limited , A Corporation Tin Mediated Regioselective Synthesis of Sucrose-6-Esters
US7750146B2 (en) 2005-03-18 2010-07-06 Tate & Lyle Plc Granular sucralose
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
CN100418976C (zh) * 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
CN101092438A (zh) * 2006-06-22 2007-12-26 南京莱因医药科技有限公司 6－o－苯甲酰三氯半乳型蔗糖四乙酯的制备方法
GB0702854D0 (en) * 2007-01-09 2007-03-28 Tate & Lyle Plc Method for the synthesis of sucrose-6-esters
US20080227971A1 (en) * 2007-01-19 2008-09-18 Leinhos Duane A Deacylation of sucralose-6-acylates
GB0702857D0 (en) * 2007-01-19 2007-03-28 Tate & Lyle Plc Improved sucralose production method
US20090076261A1 (en) * 2007-09-13 2009-03-19 Polymed Therapeutics, Inc. Novel process for preparing sucrose-6-esters
CN101245085B (zh) 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
AR070082A1 (es) * 2008-01-04 2010-03-10 Tate & Lyle Technology Ltd Metodo para la produccion de sucralosa
US7932380B2 (en) 2008-03-06 2011-04-26 Wanhe International (Group) Co. Ltd. Process for the preparation of sucralose
US8557976B2 (en) * 2008-03-13 2013-10-15 Tate & Lyle Technology Limited Microbial consortia and methods for their use
EP2254677A1 (en) * 2008-03-20 2010-12-01 Tate & Lyle Technology Limited Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
US20090259036A1 (en) * 2008-04-03 2009-10-15 Tate & Lyle Technology Limited Extraction of less polar impurities from sucralose containing aqueous feed streams
TW200946683A (en) * 2008-04-03 2009-11-16 Tate & Lyle Technology Ltd A process for the purification of aqueous feed streams containing sucralose extraction efficiency
US20090299055A1 (en) * 2008-04-03 2009-12-03 Tate & Lyle Technology Limited Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) * 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2471348B (en) 2009-06-22 2011-12-14 Tate & Lyle Technology Ltd A method for producing sucralose-6-acylate
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB2474310B (en) * 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
CN101759728B (zh) * 2010-01-08 2012-01-11 江苏巨邦制药有限公司 三氯蔗糖的生产及精制方法
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2544217B (en) 2014-08-08 2020-03-25 Tate & Lyle Tech Ltd Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
WO2017091437A1 (en) 2015-11-24 2017-06-01 Archer Daniels Midland Company Organotin catalysts in esterification processes of furan-2,5-dicarboxylic acid (fdca)
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF

Citations (1)

* Cited by examiner, † Cited by third party
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EP0043649A1 (en) * 1980-07-08 1982-01-13 TATE & LYLE PUBLIC LIMITED COMPANY Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (TGS)

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US4435440A (en) * 1976-01-08 1984-03-06 Tate & Lyle Limited Sweeteners
EP0030804B1 (en) * 1979-12-18 1983-10-19 TATE & LYLE PUBLIC LIMITED COMPANY Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3062467D1 (en) * 1979-12-20 1983-04-28 Tate & Lyle Plc Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose

Patent Citations (1)

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EP0043649A1 (en) * 1980-07-08 1982-01-13 TATE & LYLE PUBLIC LIMITED COMPANY Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (TGS)

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Title
CHEMICAL ABSTRACTS, vol. 109, no. 7, 15th August 1988, page 727, column 1, abstract no. 55069d, Columbus, Ohio, US; M.H. KIM et al.: "Selective acylation of nucleosides and sugars. Regioselective benzoylation of glucofuranose via stannylene derivatives", & SOUL TAEHAKKYO YAKHAK NONMUNJIP 1986, 11, 71-3 *
CHEMICAL ABSTRACTS, vol. 69, no. 25, 16th December 1968, page 10038, column 2, abstract no. 106989u, Columbus, Ohio, US; E. REINEFELD et al.: "Selective acylation of sucrose: isolation and structure of partial esters of fatty acids", & ZUCKER 1968, 21(12), 330-8 *
CHEMICAL ABSTRACTS, vol. 87, no. 17, 24th October 1977, page 786, column 1, abstract no. 136200u, Columbus, Ohio, US; E. AVELA et al.: "Selective substitution of sucrose hydroxyl groups via chelates", & ACS SYMP. SER. 1977, 41(SUCROCHEM., SYMP., 1976), 62-76 *
CHEMICAL AND PHARMACEUTICAL BULLETIN, vol. 31, no. 5, 1983, pages 1612-1624, Tokyo, JP; Y. TSUDA et al.: "Regioselective monoacylation of some glycopyranosides via cyclic tin intermediates" *
CLAIMS SEARCHED: ALL *
PATENT JOURNAL OF SOUTH AFRICA, July 1982, page 133, column 2, 81/4724; & ZA-A-81 4724 (AECI LTD) *
TETRAHEDRON, vol. 37, no. 13, 1981, pages 2363-2369, Oxford, GB; T. OGAWA et al.: "Regioselective stannylation" *

Also Published As

Publication number Publication date
NO892926D0 (no) 1989-07-17
JP2725710B2 (ja) 1998-03-11
AU3804889A (en) 1990-01-18
EP0352048A2 (en) 1990-01-24
EP0352048B1 (en) 1994-11-30
DK352689D0 (da) 1989-07-17
ZA895427B (en) 1991-03-27
DE68919566T2 (de) 1995-04-13
FI893455A (fi) 1990-01-19
FI91874C (fi) 1994-08-25
AR245136A1 (es) 1993-12-30
IE892310L (en) 1990-01-18
AU618107B2 (en) 1991-12-12
PT91186B (pt) 1995-03-01
NZ229823A (en) 1991-01-29
US4950746A (en) 1990-08-21
FI893455A0 (fi) 1989-07-17
KR910002884A (ko) 1991-02-26
IL91004A0 (en) 1990-02-09
DE68919566D1 (de) 1995-01-12
DK170027B1 (da) 1995-05-01
TR27628A (tr) 1995-06-14
NO892926L (no) 1990-01-19
MX172793B (es) 1994-01-13
NO171855B (no) 1993-02-01
JPH0273096A (ja) 1990-03-13
IL91004A (en) 1994-04-12
YU139389A (en) 1991-02-28
ES2065386T3 (es) 1995-02-16
PH26098A (en) 1992-02-06
ATE114664T1 (de) 1994-12-15
DK352689A (da) 1990-01-19
YU47159B (sh) 1995-01-31
EP0352048A3 (en) 1991-09-04
GR1002250B (en) 1996-04-23
FI91874B (fi) 1994-05-13
KR0143234B1 (ko) 1998-07-01
IE65990B1 (en) 1995-11-29
CA1323625C (en) 1993-10-26
PT91186A (pt) 1990-02-08
NO171855C (no) 1993-05-12
MX16842A (es) 1993-04-01
RU2041233C1 (ru) 1995-08-09

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