DK0970096T3 - Kromatografisk oprensning af chloreret saccharose - Google Patents

Kromatografisk oprensning af chloreret saccharose

Info

Publication number
DK0970096T3
DK0970096T3 DK98906453T DK98906453T DK0970096T3 DK 0970096 T3 DK0970096 T3 DK 0970096T3 DK 98906453 T DK98906453 T DK 98906453T DK 98906453 T DK98906453 T DK 98906453T DK 0970096 T3 DK0970096 T3 DK 0970096T3
Authority
DK
Denmark
Prior art keywords
chlorinated sucrose
adsorbent
chromatographic purification
chlorinated
sucrose
Prior art date
Application number
DK98906453T
Other languages
Danish (da)
English (en)
Inventor
Stephen J Catani
Duane Leinhos
Thomas O'connor
Original Assignee
Tate & Lyle Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc
Application granted granted Critical
Publication of DK0970096T3 publication Critical patent/DK0970096T3/da

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Treatment Of Liquids With Adsorbents In General (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DK98906453T 1997-02-13 1998-02-11 Kromatografisk oprensning af chloreret saccharose DK0970096T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US4698097P 1997-02-13 1997-02-13
PCT/US1998/002927 WO1998035974A1 (en) 1997-02-13 1998-02-11 Chromatographic purification of chlorinated sucrose

Publications (1)

Publication Number Publication Date
DK0970096T3 true DK0970096T3 (da) 2005-03-21

Family

ID=21946404

Family Applications (1)

Application Number Title Priority Date Filing Date
DK98906453T DK0970096T3 (da) 1997-02-13 1998-02-11 Kromatografisk oprensning af chloreret saccharose

Country Status (17)

Country Link
US (1) US5977349A (no)
EP (1) EP0970096B1 (no)
JP (2) JP4623763B2 (no)
KR (2) KR100619874B1 (no)
AT (1) ATE282044T1 (no)
AU (1) AU6167598A (no)
BR (1) BR9807377B1 (no)
CA (1) CA2280784A1 (no)
DE (1) DE69827482T2 (no)
DK (1) DK0970096T3 (no)
ES (1) ES2231964T3 (no)
IL (1) IL131394A0 (no)
NO (1) NO313553B1 (no)
NZ (1) NZ337573A (no)
PT (1) PT970096E (no)
TR (1) TR199902413T2 (no)
WO (1) WO1998035974A1 (no)

Families Citing this family (30)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IL131394A0 (en) * 1997-02-13 2001-01-28 Mcneil Ppc Inc Chromatographic purification of chlorinated sucrose
US7049435B2 (en) * 2002-03-08 2006-05-23 Tate & Lyle Public Limited Company Extractive methods for purifying sucralose
US6998480B2 (en) * 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
US20070270583A1 (en) * 2004-12-10 2007-11-22 Pharmed Medicare Private Limited Process for Purification of 6 Acetyl 4,1', 6' Trichlorogalactosucrose and 4,1', 6' Trichlorogalactosucrose by Chromatography on Silanized Silica Gel
US8148112B2 (en) * 2005-02-16 2012-04-03 National University Corporation Hokkaido University Sugar chain containing 4-position halogenated galactose and application thereof
US20060276639A1 (en) * 2005-06-01 2006-12-07 Healthy Brands, Llc Conversion of sucralose-6-ester to sucralose
KR20080048989A (ko) * 2005-06-06 2008-06-03 팜드 메디케어 프리베이트 리미티드 크로마토그래피에 의한 염소화 수크로스 유도체의 정제방법
BRPI0617101A2 (pt) * 2005-08-30 2011-07-12 Pharmed Medicare Pvt Ltd processo para produção de sacarose clorada baseado em separação bioquìmica hidrofóbica
JP2009538293A (ja) * 2006-05-23 2009-11-05 ヴイ ビー メディケア プライヴェート リミテッド トリクロロガラクトスクロース製造のプロセスストリームからのジメチルホルムアミド及び他の溶媒の回収
CN101029062B (zh) * 2007-04-09 2011-06-15 淄博联技甜味剂有限公司 三氯蔗糖的合成工艺
AR070082A1 (es) * 2008-01-04 2010-03-10 Tate & Lyle Technology Ltd Metodo para la produccion de sucralosa
US8476424B2 (en) * 2008-03-20 2013-07-02 Tate & Lyle Technology Limited Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
US20090259036A1 (en) * 2008-04-03 2009-10-15 Tate & Lyle Technology Limited Extraction of less polar impurities from sucralose containing aqueous feed streams
US8212022B2 (en) * 2008-04-03 2012-07-03 Tate & Lyle Technology Limited Effect of carbohydrate concentration on sucralose extraction efficiency
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
GB2468936B (en) 2009-03-27 2011-09-07 Mohamad Rami Radwan Jaber Chlorination of sucrose-6-esters
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2474311B (en) 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
US20120034366A1 (en) * 2010-08-05 2012-02-09 Tate & Lyle Ingredients Americas, Inc. Carbohydrate compositions
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN102830197B (zh) * 2012-07-25 2015-07-15 湖北省宏源药业科技股份有限公司 一种中控监测单酯法合成三氯蔗糖过程的方法
US10227367B2 (en) 2013-12-16 2019-03-12 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
WO2016020635A1 (en) 2014-08-08 2016-02-11 Tate & Lyle Technology Limited Chlorination of sucrose-6-esters
GB2536480B (en) 2015-03-17 2019-09-04 Tate & Lyle Tech Ltd DMF Distillation
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ZA807578B (en) * 1979-12-18 1981-11-25 Tate & Lyle Patent Holdings Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
DE3165986D1 (en) * 1980-07-08 1984-10-18 Tate & Lyle Plc Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs)
ZA817425B (en) * 1980-10-28 1982-10-27 Tate & Lyle Patent Holdings Sweet chlorine-substituted disaccharides
EP0067535B1 (en) * 1981-05-22 1985-01-30 TATE & LYLE PUBLIC LIMITED COMPANY Brominated sucrose derivatives
GB8316201D0 (en) * 1982-09-13 1983-07-20 Tate & Lyle Plc Sucrose derivatives
GB8822673D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Selective acylation of sugars
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
JPH06253879A (ja) * 1993-03-01 1994-09-13 Snow Brand Milk Prod Co Ltd グルクロン酸結合オリゴ糖の分離方法
US5530106A (en) * 1993-03-12 1996-06-25 Mcneil-Ppc, Inc. Recovery of sucralose intermediates
US5298611A (en) * 1993-03-12 1994-03-29 Mcneil-Ppc, Inc. Sucralose pentaester production
EP0687491A1 (en) * 1994-06-16 1995-12-20 Daicel Chemical Industries, Ltd. Simulated moving bed chromatographic separation process
US5498709A (en) * 1994-10-17 1996-03-12 Mcneil-Ppc, Inc. Production of sucralose without intermediate isolation of crystalline sucralose-6-ester
IL131394A0 (en) * 1997-02-13 2001-01-28 Mcneil Ppc Inc Chromatographic purification of chlorinated sucrose

Also Published As

Publication number Publication date
DE69827482T2 (de) 2005-12-15
EP0970096A1 (en) 2000-01-12
BR9807377B1 (pt) 2009-12-01
KR100531261B1 (ko) 2005-11-28
US5977349A (en) 1999-11-02
DE69827482D1 (de) 2004-12-16
PT970096E (pt) 2005-03-31
ATE282044T1 (de) 2004-11-15
EP0970096B1 (en) 2004-11-10
JP2001511812A (ja) 2001-08-14
KR20050093860A (ko) 2005-09-23
KR20000071081A (ko) 2000-11-25
NO993920L (no) 1999-10-11
JP5132665B2 (ja) 2013-01-30
IL131394A0 (en) 2001-01-28
TR199902413T2 (xx) 2000-01-21
NZ337573A (en) 2000-06-23
CA2280784A1 (en) 1998-08-20
JP4623763B2 (ja) 2011-02-02
KR100619874B1 (ko) 2006-09-06
NO993920D0 (no) 1999-08-13
AU6167598A (en) 1998-09-08
BR9807377A (pt) 2001-06-19
JP2010090160A (ja) 2010-04-22
ES2231964T3 (es) 2005-05-16
NO313553B1 (no) 2002-10-21
WO1998035974A1 (en) 1998-08-20

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