DE69929998D1 - Verfahren zur herstellung von estern - Google Patents
Verfahren zur herstellung von esternInfo
- Publication number
- DE69929998D1 DE69929998D1 DE69929998T DE69929998T DE69929998D1 DE 69929998 D1 DE69929998 D1 DE 69929998D1 DE 69929998 T DE69929998 T DE 69929998T DE 69929998 T DE69929998 T DE 69929998T DE 69929998 D1 DE69929998 D1 DE 69929998D1
- Authority
- DE
- Germany
- Prior art keywords
- water
- alcohol
- ester
- liquid effluent
- vessel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US196266 | 1980-10-22 | ||
US09/196,266 US6664413B1 (en) | 1998-11-19 | 1998-11-19 | Process for production of esters |
PCT/US1999/026957 WO2000031016A1 (en) | 1998-11-19 | 1999-11-16 | Process for production of esters |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69929998D1 true DE69929998D1 (de) | 2006-04-27 |
DE69929998T2 DE69929998T2 (de) | 2006-11-09 |
Family
ID=22724678
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69929998T Expired - Fee Related DE69929998T2 (de) | 1998-11-19 | 1999-11-16 | Verfahren zur herstellung von estern |
Country Status (10)
Country | Link |
---|---|
US (1) | US6664413B1 (de) |
EP (1) | EP1131278B8 (de) |
JP (1) | JP2002530362A (de) |
AT (1) | ATE318255T1 (de) |
AU (1) | AU1623700A (de) |
BR (1) | BR9916754A (de) |
CA (1) | CA2347689C (de) |
DE (1) | DE69929998T2 (de) |
ES (1) | ES2258861T3 (de) |
WO (1) | WO2000031016A1 (de) |
Families Citing this family (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2802923B1 (fr) * | 1999-12-28 | 2002-03-08 | Roquette Freres | Procede de preparation d'une composition d'ester d'acide lactique et son utilisation en tant que solvant |
FR2838435B1 (fr) * | 2002-04-12 | 2004-06-18 | Atofina | Composition comprenant un melange de mono et polylactyllactates d'alkyle |
FR2848209B1 (fr) * | 2002-12-05 | 2006-10-13 | Atofina | Procede continu de preparation de lactate d'ethyle |
FR2848208B1 (fr) * | 2002-12-05 | 2005-01-14 | Atofina | Procede continu de preparation de lactate d'ethyle |
CN100427453C (zh) * | 2004-08-27 | 2008-10-22 | 清华大学 | 催化精馏法合成乳酸乙酯工艺 |
US8557950B2 (en) | 2005-06-16 | 2013-10-15 | Grupo Petrotemex, S.A. De C.V. | High intrinsic viscosity melt phase polyester polymers with acceptable acetaldehyde generation rates |
CN101263185B (zh) * | 2005-09-16 | 2012-05-02 | 奇派特石化有限公司 | 聚合物熔体中添加剂的添加方法 |
US7838596B2 (en) | 2005-09-16 | 2010-11-23 | Eastman Chemical Company | Late addition to effect compositional modifications in condensation polymers |
US9267007B2 (en) * | 2005-09-16 | 2016-02-23 | Grupo Petrotemex, S.A. De C.V. | Method for addition of additives into a polymer melt |
FR2902095B1 (fr) * | 2006-06-09 | 2008-12-05 | Rhodia Recherches & Tech | Procede de transformation de composes nitriles en acides carboxyliques et esters correspondants |
US8901272B2 (en) | 2007-02-02 | 2014-12-02 | Grupo Petrotemex, S.A. De C.V. | Polyester polymers with low acetaldehyde generation rates and high vinyl ends concentration |
CN101092358B (zh) * | 2007-07-13 | 2012-02-29 | 先尼科化工(上海)有限公司 | 丁二酸二异丙酯的间歇制备方法 |
CN102209706B (zh) * | 2008-10-01 | 2014-07-23 | 普拉克生化公司 | 制造n,n-二烷基乳酰胺的方法 |
CN105950673A (zh) | 2010-06-18 | 2016-09-21 | 布特马斯先进生物燃料有限责任公司 | 在提取发酵中用于醇移除的来源于油的提取溶剂 |
US9040263B2 (en) | 2010-07-28 | 2015-05-26 | Butamax Advanced Biofuels Llc | Production of alcohol esters and in situ product removal during alcohol fermentation |
EP2614152A4 (de) * | 2010-09-07 | 2015-04-15 | Myriant Corp | Katalytische dehydrierung von milchsäure und milchsäureestern |
EP2723486A4 (de) * | 2011-06-27 | 2015-04-29 | Burton Rachel | Reaktorsystem |
US9139505B2 (en) | 2013-11-08 | 2015-09-22 | Eastman Chemical Company | Production of terephthalic acid di-esters using alcohol-amine promoters |
CN107032984A (zh) * | 2016-02-03 | 2017-08-11 | 天津中福工程技术有限公司 | 一种连续催化精馏制备乳酸乙酯的方法 |
JP6692229B2 (ja) * | 2016-06-28 | 2020-05-13 | 大阪瓦斯株式会社 | 3hbエステルの製造方法 |
CN112844249B (zh) * | 2020-12-24 | 2022-10-25 | 河南金丹乳酸科技股份有限公司 | 催化酯化制备乳酸乙酯工艺 |
Family Cites Families (21)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE206373C (de) | ||||
US1668806A (en) | 1926-11-29 | 1928-05-08 | Commercial Solvents Corp | Normal butyl lactate |
US2029694A (en) | 1934-07-30 | 1936-02-04 | Commercial Soivents Corp | Esterification process |
US2334524A (en) | 1942-04-14 | 1943-11-16 | Apex Chem Co Inc | Purifying hydroxy aliphatic acids |
US2465772A (en) | 1944-02-17 | 1949-03-29 | Nat Dairy Res Lab Inc | Preparation of alkyl lactates |
US2565487A (en) | 1948-12-27 | 1951-08-28 | Edward M Filachione | Production of esters |
US2722541A (en) | 1950-08-02 | 1955-11-01 | Henry E Schulz | Process of esterifying butyl lactate |
FR2308611A1 (fr) | 1975-04-24 | 1976-11-19 | Rhone Poulenc Ind | Procede de recuperation de l'acide acetique a partir de ses solutions aqueuses de faible concentration |
JPS54106412A (en) * | 1978-02-08 | 1979-08-21 | Kyowa Yuka Kk | Method of purifying ester |
US4452969A (en) * | 1983-06-09 | 1984-06-05 | General Electric Company | Poly(alkylene dicarboxylate) process and catalysts for use therein |
US4868329A (en) * | 1986-08-01 | 1989-09-19 | Hoechst Celanese Corp. | Accelerated preparation of carboxylic acid esters |
US4780527A (en) * | 1987-05-06 | 1988-10-25 | Industrial Technology Research Institute | Preparation of polyesters from terephthalic acid |
US5071754A (en) | 1990-01-23 | 1991-12-10 | Battelle Memorial Institute | Production of esters of lactic acid, esters of acrylic acid, lactic acid, and acrylic acid |
US5252473A (en) | 1990-01-23 | 1993-10-12 | Battelle Memorial Institute | Production of esters of lactic acid, esters of acrylic acid, lactic acid, and acrylic acid |
US5210296A (en) | 1990-11-19 | 1993-05-11 | E. I. Du Pont De Nemours And Company | Recovery of lactate esters and lactic acid from fermentation broth |
US5426219A (en) | 1993-07-26 | 1995-06-20 | A.E. Staley Manufacturing Co. | Process for recovering organic acids |
DE4341770A1 (de) | 1993-12-08 | 1995-06-14 | Basf Ag | Verfahren zur Herstellung von Milchsäureestern |
US5502240A (en) * | 1995-06-09 | 1996-03-26 | Aristech Chemical Corporation | Esterification process using a titamium zeolite catalyst |
US5723639A (en) | 1995-10-16 | 1998-03-03 | University Of Chicago | Esterification of fermentation-derived acids via pervaporation |
GB9612161D0 (en) | 1996-06-11 | 1996-08-14 | Tioxide Specialties Ltd | Esterification process |
US5766439A (en) | 1996-10-10 | 1998-06-16 | A. E. Staley Manufacturing Co. | Production and recovery of organic acids |
-
1998
- 1998-11-19 US US09/196,266 patent/US6664413B1/en not_active Expired - Fee Related
-
1999
- 1999-11-16 JP JP2000583845A patent/JP2002530362A/ja active Pending
- 1999-11-16 DE DE69929998T patent/DE69929998T2/de not_active Expired - Fee Related
- 1999-11-16 AT AT99958972T patent/ATE318255T1/de not_active IP Right Cessation
- 1999-11-16 CA CA002347689A patent/CA2347689C/en not_active Expired - Fee Related
- 1999-11-16 ES ES99958972T patent/ES2258861T3/es not_active Expired - Lifetime
- 1999-11-16 EP EP99958972A patent/EP1131278B8/de not_active Expired - Lifetime
- 1999-11-16 WO PCT/US1999/026957 patent/WO2000031016A1/en active IP Right Grant
- 1999-11-16 AU AU16237/00A patent/AU1623700A/en not_active Abandoned
- 1999-11-16 BR BR9916754-9A patent/BR9916754A/pt not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
EP1131278B8 (de) | 2006-06-21 |
EP1131278A4 (de) | 2002-07-24 |
AU1623700A (en) | 2000-06-13 |
US6664413B1 (en) | 2003-12-16 |
WO2000031016A1 (en) | 2000-06-02 |
ATE318255T1 (de) | 2006-03-15 |
CA2347689A1 (en) | 2000-06-02 |
ES2258861T3 (es) | 2006-09-01 |
JP2002530362A (ja) | 2002-09-17 |
BR9916754A (pt) | 2001-08-14 |
EP1131278B1 (de) | 2006-02-22 |
EP1131278A1 (de) | 2001-09-12 |
DE69929998T2 (de) | 2006-11-09 |
CA2347689C (en) | 2009-01-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |