DE69915952D1 - Methode zur katalytischen Dampfphasenoxidation und Rohrbündelreaktor mit Wärmeaustausch - Google Patents

Methode zur katalytischen Dampfphasenoxidation und Rohrbündelreaktor mit Wärmeaustausch

Info

Publication number
DE69915952D1
DE69915952D1 DE69915952T DE69915952T DE69915952D1 DE 69915952 D1 DE69915952 D1 DE 69915952D1 DE 69915952 T DE69915952 T DE 69915952T DE 69915952 T DE69915952 T DE 69915952T DE 69915952 D1 DE69915952 D1 DE 69915952D1
Authority
DE
Germany
Prior art keywords
heat exchange
vapor phase
tube bundle
phase oxidation
bundle reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE69915952T
Other languages
English (en)
Other versions
DE69915952T2 (de
Inventor
Yousuke Ogata
Takehiro Takashima
Osamu Dodo
Hidefumi Haramaki
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=17414555&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69915952(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Publication of DE69915952D1 publication Critical patent/DE69915952D1/de
Application granted granted Critical
Publication of DE69915952T2 publication Critical patent/DE69915952T2/de
Anticipated expiration legal-status Critical
Revoked legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B33/00—Oxidation in general
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
    • C07C51/313—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting with molecular oxygen
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B01J2219/00777—Baffles attached to the reactor wall horizontal
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
DE69915952T 1998-09-18 1999-09-17 Verfahren zur katalytischen Dampfphasenoxidation und Röhrenkesselreaktor Revoked DE69915952T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP26524598 1998-09-18
JP26524598A JP3559456B2 (ja) 1998-09-18 1998-09-18 接触気相酸化方法及び多管式反応器

Publications (2)

Publication Number Publication Date
DE69915952D1 true DE69915952D1 (de) 2004-05-06
DE69915952T2 DE69915952T2 (de) 2005-02-10

Family

ID=17414555

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69915952T Revoked DE69915952T2 (de) 1998-09-18 1999-09-17 Verfahren zur katalytischen Dampfphasenoxidation und Röhrenkesselreaktor

Country Status (7)

Country Link
US (1) US6582667B1 (de)
EP (1) EP0987057B1 (de)
JP (1) JP3559456B2 (de)
KR (1) KR100379218B1 (de)
CN (1) CN1170624C (de)
DE (1) DE69915952T2 (de)
SG (1) SG134960A1 (de)

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DE19836792A1 (de) * 1998-08-13 2000-02-17 Basf Ag Reaktor mit einem Kontaktrohrbündel
ZA200004211B (en) 1999-08-31 2001-02-14 Nippon Catalytic Chem Ind Method for catalytic gas phase oxidation.
JP4451520B2 (ja) * 1999-11-08 2010-04-14 株式会社日本触媒 竪型熱交換器
KR100355845B1 (ko) * 1999-11-11 2002-10-12 삼성종합화학주식회사 에틸렌옥사이드 제조공정에서 반응억제제 주입 경로 개선공정
JP4648515B2 (ja) * 2000-05-02 2011-03-09 株式会社日本触媒 反応器のスタートアップ方法
JP4995373B2 (ja) * 2001-02-20 2012-08-08 三菱レイヨン株式会社 反応管、触媒の製造方法、不飽和アルデヒドおよび不飽和カルボン酸の製造方法
JP4824867B2 (ja) * 2001-05-30 2011-11-30 三菱レイヨン株式会社 メタクロレインおよびメタクリル酸の製造方法
TW572885B (en) * 2001-05-30 2004-01-21 Mitsubishi Rayon Co Method for producing (meth)acrolein and/or (meth)acrylic acid
JP4824871B2 (ja) * 2001-06-27 2011-11-30 三菱レイヨン株式会社 アクロレインおよびアクリル酸の製造方法
EP2361899B1 (de) 2002-01-11 2015-07-22 Mitsubishi Chemical Corporation Verfahren zur katalytischen Gasphasenoxidation mit einem Wärmetausch-Reaktor mit mehreren Rohren
US7115776B2 (en) † 2002-07-18 2006-10-03 Basf Aktiengesellschaft Heterogeneously catalyzed gas-phase partial oxidation of at least one organic compound
JP4145607B2 (ja) 2002-08-23 2008-09-03 三菱化学株式会社 多管式反応器を用いた気相接触酸化方法
DE10258180A1 (de) * 2002-12-12 2004-06-24 Basf Ag Verfahren zur Herstellung von Chlor durch Gasphasenoxidation von Chlorwasserstoff
JP4867129B2 (ja) * 2003-12-15 2012-02-01 三菱化学株式会社 （メタ）アクリル酸または（メタ）アクロレインの製造方法
US7371361B2 (en) * 2004-11-03 2008-05-13 Kellogg Brown & Root Llc Maximum reaction rate converter system for exothermic reactions
JP4947917B2 (ja) * 2005-04-18 2012-06-06 株式会社日本触媒 気相接触酸化用の固定床反応器およびアクロレインまたはアクリル酸の製造方法
JP2007161637A (ja) * 2005-12-13 2007-06-28 Mitsui Chemicals Inc メチルアミン類の製造方法
AU2006332008C1 (en) * 2005-12-21 2014-02-20 Virent, Inc. Catalysts and methods for reforming oxygenated compounds
KR100847199B1 (ko) * 2006-01-31 2008-07-17 주식회사 엘지화학 열전달 성능이 향상된 반응기, 이 반응기를 이용한 산화물 제조방법, 및 평행류의 열매체 유속 증가 방법
KR100584570B1 (ko) 2006-02-28 2006-05-30 한국기계연구원 플라즈마 반응장치
US7947232B2 (en) * 2006-12-07 2011-05-24 Exxonmobil Research & Engineering Company HF alkylation reactor
MX2009006509A (es) * 2006-12-20 2009-10-28 Virent Energy Systems Inc Sistema reactor para la produccion de productos gaseosos.
TW200902151A (en) * 2007-02-12 2009-01-16 Basf Ag Method for leakage monitoring in a tube bundle reactor
MY154790A (en) 2007-03-08 2015-07-31 Virent Inc Synthesis of liquid fuels and chemicals from oxygenated hydrocarbons
DE102007019597A1 (de) * 2007-04-24 2008-05-15 Basf Ag Verfahren der Inbetriebnahme einer heterogen katalysierten partiellen Gasphasenoxidation von Acrolein zu Acrylsäure oder von Methacrolein zu Methacrylsäure
DE102007025869A1 (de) 2007-06-01 2008-07-03 Basf Se Verfahren der Wiederbeschickung der Reaktionsrohre eines Rohrbündelreaktors mit einem neuen Katalysatorfestbett
DE102007028333A1 (de) 2007-06-15 2008-12-18 Basf Se Verfahren zum Einbringen einer wenigstens einer Produktionscharge von ringförmigen Schalenkatalysatoren K entnommenen Teilmenge in ein Reaktionsrohr eines Rohrbündelreaktors
AU2009218827B2 (en) * 2008-02-25 2014-03-27 Haldor Topsoe A/S Reactor for the preparation of methanol
JP2012501338A (ja) * 2008-08-27 2012-01-19 ヴァイレント エナジー システムズ インク． バイオマスからの液体燃料の合成
BRPI1010126A2 (pt) * 2009-06-30 2016-03-15 Virent Inc método de regeneração de um catalizador de hidrogenação e método para a hidrogenação de uma açucar e a regeneração em linha de um catalizador de hidrogenação que contém depósitos carbonáceos
KR101847674B1 (ko) 2010-12-29 2018-04-10 롬 앤드 하스 캄파니 프로판 산화를 위한 반응기 및 방법
US11504814B2 (en) 2011-04-25 2022-11-22 Holtec International Air cooled condenser and related methods
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Also Published As

Publication number Publication date
EP0987057A1 (de) 2000-03-22
KR100379218B1 (ko) 2003-04-08
SG134960A1 (en) 2007-09-28
CN1251319A (zh) 2000-04-26
US6582667B1 (en) 2003-06-24
EP0987057B1 (de) 2004-03-31
JP3559456B2 (ja) 2004-09-02
JP2000093784A (ja) 2000-04-04
CN1170624C (zh) 2004-10-13
KR20000023179A (ko) 2000-04-25
DE69915952T2 (de) 2005-02-10

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8363 Opposition against the patent
8331 Complete revocation