DE69717976D1 - Gewinnung von epsilon-caprolactam aus wässrigen gemischen - Google Patents

Gewinnung von epsilon-caprolactam aus wässrigen gemischen

Info

Publication number
DE69717976D1
DE69717976D1 DE69717976T DE69717976T DE69717976D1 DE 69717976 D1 DE69717976 D1 DE 69717976D1 DE 69717976 T DE69717976 T DE 69717976T DE 69717976 T DE69717976 T DE 69717976T DE 69717976 D1 DE69717976 D1 DE 69717976D1
Authority
DE
Germany
Prior art keywords
caprolactam
aqueous mixtures
epsilon
obtaining
obtaining epsilon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE69717976T
Other languages
English (en)
Other versions
DE69717976T3 (de
DE69717976T2 (de
Inventor
Rudolf Philippus Maria Guit
Yvonne Helene Frentzen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Invista Technologies SARL Switzerland
Original Assignee
DSM NV
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=56289731&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE69717976(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Priority claimed from MYPI96000650A external-priority patent/MY116498A/en
Priority claimed from EP96202436A external-priority patent/EP0826665A1/de
Application filed by DSM NV, EI Du Pont de Nemours and Co filed Critical DSM NV
Application granted granted Critical
Publication of DE69717976D1 publication Critical patent/DE69717976D1/de
Publication of DE69717976T2 publication Critical patent/DE69717976T2/de
Publication of DE69717976T3 publication Critical patent/DE69717976T3/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/08—Preparation of lactams from carboxylic acids or derivatives thereof, e.g. hydroxy carboxylic acids, lactones or nitriles
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16—Separation or purification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Polyamides (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE69717976T 1996-02-17 1997-02-05 Gewinnung von epsilon-caprolactam aus wässrigen gemischen Expired - Lifetime DE69717976T3 (de)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
MY9600650 1996-02-17
MYPI96000650A MY116498A (en) 1995-03-01 1996-02-17 Process for the preparation of é - caprolactam
EP96202436 1996-09-02
EP96202436A EP0826665A1 (de) 1996-09-02 1996-09-02 Gewinnung von epsilon-Caprolactam aus wässrigen Gemischen
EP96202931 1996-10-21
EP96202931 1996-10-21
PCT/NL1997/000033 WO1997030028A2 (en) 1996-02-17 1997-02-05 Recovery of epsilon-caprolactam from aqueous mixtures

Publications (3)

Publication Number Publication Date
DE69717976D1 true DE69717976D1 (de) 2003-01-30
DE69717976T2 DE69717976T2 (de) 2003-11-06
DE69717976T3 DE69717976T3 (de) 2008-09-18

Family

ID=56289731

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69717976T Expired - Lifetime DE69717976T3 (de) 1996-02-17 1997-02-05 Gewinnung von epsilon-caprolactam aus wässrigen gemischen

Country Status (12)

Country Link
US (1) US6191274B1 (de)
EP (1) EP0891327B2 (de)
JP (1) JP2000512615A (de)
KR (1) KR100459817B1 (de)
CN (1) CN1085978C (de)
AU (1) AU1673997A (de)
CA (1) CA2246459A1 (de)
DE (1) DE69717976T3 (de)
ES (1) ES2188891T3 (de)
ID (1) ID16013A (de)
TW (1) TW420662B (de)
WO (1) WO1997030028A2 (de)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU3870097A (en) 1996-10-21 1998-05-15 Dsm N.V. Process to separate epsilon-caprolactam from 6-aminocaproamide and 6-aminocaproamide oligomers
BE1011047A3 (nl) 1997-03-17 1999-04-06 Dsm Nv Werkwijze voor het zuiveren van caprolactam.
DE10021199A1 (de) * 2000-05-03 2001-11-08 Basf Ag Verfahren zur Herstellung von Caprolactam
US9418186B2 (en) 2012-05-23 2016-08-16 Exxonmobil Research And Engineering Company Assessment of solute partitioning in crude oils
CN104387322A (zh) * 2014-10-21 2015-03-04 湖南百利工程科技股份有限公司 一种低副产硫酸铵的己内酰胺的制备方法
CN111122720B (zh) * 2019-12-11 2022-09-02 湖北三宁碳磷基新材料产业技术研究院有限公司 己内酰胺、6-氨基己酰胺和6-氨基己腈的分析方法

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE913172C (de) † 1942-08-19 1954-06-10 Bobingen Ag Fuer Textil Faser Verfahren zur Wiedergewinnung von Lactamen aus verduennten waessrigen Loesungen
DE953168C (de) † 1953-03-19 1956-11-29 Stamicarbon Verfahren zur Reinigung von Caprolactam
DE1092018B (de) † 1957-10-26 1960-11-03 Stamicarbon Verfahren zur Gewinnung von lactamoligomerhaltigen Lactamen
CH446342A (de) † 1963-11-29 1967-11-15 Bayer Ag Verfahren zum Herstellen reiner Lactame
FR1419684A (fr) 1964-09-03 1965-12-03 Electrochimie Soc Procédé perfectionné de fabrication d'epsilon-caprolactames
LU55528A1 (de) * 1967-04-22 1968-05-03
US3485821A (en) * 1967-05-29 1969-12-23 Techni Chem Co The Process for preparing caprolactam and its alkyl substituted derivatives
GB1198428A (en) * 1967-07-18 1970-07-15 Bp Chem Int Ltd Solvent Extraction Process for Caprolactam
FR2005035A1 (de) 1968-03-29 1969-12-05 Basf Ag
US3761467A (en) * 1971-02-11 1973-09-25 Allied Chem Recovery of epsilon-caprolactam
IT956940B (it) 1972-06-28 1973-10-10 Snia Viscosa Procedimento per l estrazione di lattami da miscele acide di rea zione
DE2333973A1 (de) † 1973-07-04 1975-01-23 Nikex Nehezipari Kulkere Verfahren fuer die herstellung von lichtdurchlaessigen, dichten polykristallinischen aluminium-sinter-koerpern vornehmlich fuer leuchtroehren
US4013640A (en) * 1974-04-11 1977-03-22 Union Carbide Corporation Process for the recovery of amides
NL7505130A (nl) * 1975-05-01 1976-11-03 Stamicarbon Werkwijze voor de winning van zuiver epsilon- -caprolactam uit een waterige oplossing hiervan.
JPS523261A (en) 1975-06-24 1977-01-11 Sumitomo Chem Co Ltd Purification method for polluted water
NL7700234A (nl) 1977-01-12 1978-07-14 Stamicarbon Werkwijze voor het winnen van epsilon-caprolac- tam uit epsilon-caprolactam- bevattend destil- latieresidu.
JPS6021146B2 (ja) * 1977-05-10 1985-05-25 宇部興産株式会社 ε−カプロラクタムの分離法
JPS6026103B2 (ja) * 1978-03-29 1985-06-21 三菱化学株式会社 ε−カプロラクタム及び硫安の回収方法
US4366306A (en) * 1980-02-01 1982-12-28 The Dow Chemical Company Melt polymerization of ε-caprolactam
SU1028668A1 (ru) * 1981-04-14 1983-07-15 Предприятие П/Я В-8919 Способ извлечени капролактама из загр зненного органического растворител
JPS60199873A (ja) * 1984-03-23 1985-10-09 Ube Ind Ltd ε−カプロラクタムの回収方法
DE3534817A1 (de) † 1985-09-30 1987-04-02 Davy Mckee Ag Verfahren zur herstellung von polyamid
DE3602377A1 (de) 1986-01-28 1987-07-30 Basf Ag Verfahren zur herstellung von caprolactam
US5109104A (en) † 1990-10-04 1992-04-28 E. I. Du Pont De Nemours And Company Preparation of polyamides from omega-aminonitriles
RU1777600C (ru) * 1991-02-25 1992-11-23 Владимир Александрович Линев Способ выделени капролактама из отработанного трихлорэтилена в производстве капролактама
DE4215087A1 (de) * 1992-05-07 1993-11-11 Basf Ag Verfahren zur Rückgewinnung von Caprolactam aus Polycaprolactam
DE4441962A1 (de) † 1994-11-25 1996-05-30 Basf Ag Verfahren zur Herstellung von Caprolactam
NL1000781C2 (nl) † 1995-07-12 1997-01-14 Dsm Nv Werkwijze voor het winnen van caprolactam uit nylon-6 bevattende afval.

Also Published As

Publication number Publication date
DE69717976T3 (de) 2008-09-18
EP0891327B1 (de) 2002-12-18
ID16013A (id) 1997-08-28
US6191274B1 (en) 2001-02-20
DE69717976T2 (de) 2003-11-06
CN1217712A (zh) 1999-05-26
WO1997030028A2 (en) 1997-08-21
KR100459817B1 (ko) 2005-05-16
ES2188891T3 (es) 2003-07-01
WO1997030028A3 (en) 1997-09-25
CA2246459A1 (en) 1997-08-21
EP0891327A2 (de) 1999-01-20
AU1673997A (en) 1997-09-02
CN1085978C (zh) 2002-06-05
JP2000512615A (ja) 2000-09-26
KR19990082629A (ko) 1999-11-25
EP0891327B2 (de) 2007-06-27
TW420662B (en) 2001-02-01

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Legal Events

Date Code Title Description
8363 Opposition against the patent
8327 Change in the person/name/address of the patent owner

Owner name: DSM IP ASSETS B.V., HEERLEN, NL

Owner name: E.I. DU PONT DE NEMOURS AND CO., WILMINGTON, DEL.,

8327 Change in the person/name/address of the patent owner

Owner name: INVISTA TECHNOLOGIES S.A.R.L., ZWEIGNIEDERLASSUNG

Owner name: E.I. DUPONT DE NEMOURS AND CO., WILMINGTON, DEL.,

8327 Change in the person/name/address of the patent owner

Owner name: INVISTA TECHNOLOGIES S.A.R.L., ZWEIGNIEDERLASSUNG

8366 Restricted maintained after opposition proceedings
8328 Change in the person/name/address of the agent

Representative=s name: MAIWALD GMBH PATENTANWAELTE, 80335 MUENCHEN

8332 No legal effect for de