DE69703021D1 - Schäumbare und härtbare Organosiloxan Zusammensetzungen mit verbesserter Haftung - Google Patents
Schäumbare und härtbare Organosiloxan Zusammensetzungen mit verbesserter HaftungInfo
- Publication number
- DE69703021D1 DE69703021D1 DE69703021T DE69703021T DE69703021D1 DE 69703021 D1 DE69703021 D1 DE 69703021D1 DE 69703021 T DE69703021 T DE 69703021T DE 69703021 T DE69703021 T DE 69703021T DE 69703021 D1 DE69703021 D1 DE 69703021D1
- Authority
- DE
- Germany
- Prior art keywords
- foamable
- improved adhesion
- curable organosiloxane
- organosiloxane compositions
- compositions
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000203 mixture Substances 0.000 title 1
- 125000005375 organosiloxane group Chemical group 0.000 title 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
- C08J9/12—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent
- C08J9/14—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent organic
- C08J9/142—Compounds containing oxygen but no halogen atom
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L83/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon only; Compositions of derivatives of such polymers
- C08L83/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/06—Preparatory processes
- C08G77/08—Preparatory processes characterised by the catalysts used
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/20—Polysiloxanes containing silicon bound to unsaturated aliphatic groups
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
- C08J9/02—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by the reacting monomers or modifying agents during the preparation or modification of macromolecules
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/15—Heterocyclic compounds having oxygen in the ring
- C08K5/151—Heterocyclic compounds having oxygen in the ring having one oxygen atom in the ring
- C08K5/1515—Three-membered rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/54—Silicon-containing compounds
- C08K5/541—Silicon-containing compounds containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
- C08G77/04—Polysiloxanes
- C08G77/12—Polysiloxanes containing silicon bound to hydrogen
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2383/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
- C08J2383/04—Polysiloxanes
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/775,123 US5683527A (en) | 1996-12-30 | 1996-12-30 | Foamable organosiloxane compositions curable to silicone foams having improved adhesion |
Publications (2)
Publication Number | Publication Date |
---|---|
DE69703021D1 true DE69703021D1 (de) | 2000-10-12 |
DE69703021T2 DE69703021T2 (de) | 2001-05-03 |
Family
ID=25103396
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69703021T Expired - Lifetime DE69703021T2 (de) | 1996-12-30 | 1997-12-18 | Schäumbare und härtbare Organosiloxan Zusammensetzungen mit verbesserter Haftung |
Country Status (7)
Country | Link |
---|---|
US (2) | US5683527A (de) |
EP (1) | EP0851002B1 (de) |
JP (1) | JP4018219B2 (de) |
KR (1) | KR100580799B1 (de) |
AU (1) | AU726202B2 (de) |
DE (1) | DE69703021T2 (de) |
TW (1) | TW455624B (de) |
Families Citing this family (65)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5990187A (en) * | 1997-03-26 | 1999-11-23 | Th. Goldschmidt Ag | Method of preparing polyurethane foam utilizing organofunctionally modified polysiloxanes |
FR2770220B1 (fr) * | 1997-10-29 | 2003-01-31 | Rhodia Chimie Sa | Composition silicone reticulable en gel adhesif et amortisseur avec microspheres |
US6034179A (en) * | 1998-08-28 | 2000-03-07 | Dow Corning Corporations | Polyolefin compositions containing organosilicon compounds as adhesion additives |
US5973044A (en) * | 1998-08-28 | 1999-10-26 | Dow Corning Corporation | Adhesion promoting organosilicon compositions |
US6060559A (en) * | 1998-09-04 | 2000-05-09 | Dow Corning Corporation | Curable polyolefin compositions containing organosilicon compounds as adhesion additives |
US6077892A (en) * | 1998-09-04 | 2000-06-20 | Dow Corning Corporation | Curable polyolefin compositions containing organosilicon compounds as adhesion additives |
FR2791693B1 (fr) * | 1999-03-30 | 2003-05-16 | Rhodia Chimie Sa | Promoteur d'adherence, notamment pour composition silicone |
DE10103446C5 (de) * | 2001-01-25 | 2007-06-28 | Kettenbach Gmbh & Co. Kg | Zweistufig härtbare mischergängige Materialien |
US6482888B1 (en) | 2001-06-06 | 2002-11-19 | Dow Corning Corporation | Silicone composition and cured silicone product |
EP1502572B1 (de) * | 2003-08-01 | 2012-03-07 | 3M Deutschland GmbH | Automischbare Kitt-Abformmasse |
US7045586B2 (en) * | 2003-08-14 | 2006-05-16 | Dow Corning Corporation | Adhesives having improved chemical resistance and curable silicone compositions for preparing the adhesives |
US20050038183A1 (en) * | 2003-08-14 | 2005-02-17 | Dongchan Ahn | Silicones having improved surface properties and curable silicone compositions for preparing the silicones |
US20050038188A1 (en) * | 2003-08-14 | 2005-02-17 | Dongchan Ahn | Silicones having improved chemical resistance and curable silicone compositions having improved migration resistance |
CA2575238C (en) | 2004-08-11 | 2015-04-21 | Dow Corning Corporation | Photopolymerizable silicone materials forming semipermeable membranes for sensor applications |
JP4704434B2 (ja) * | 2004-10-08 | 2011-06-15 | ダウ・コーニング・コーポレイション | 相変化組成物を使用するリトグラフィープロセス及びパターン |
US7541264B2 (en) * | 2005-03-01 | 2009-06-02 | Dow Corning Corporation | Temporary wafer bonding method for semiconductor processing |
US20070060661A1 (en) * | 2005-09-15 | 2007-03-15 | Clark Roger C | High mobility low emission surfactants for polyurethane foams |
KR20080104279A (ko) * | 2006-02-24 | 2008-12-02 | 다우 코닝 코포레이션 | 실리콘으로 캡슐화된 발광 장치 및 실리콘 제조용의 경화성실리콘 조성물 |
JP5239122B2 (ja) * | 2006-03-03 | 2013-07-17 | 信越化学工業株式会社 | オルガノポリシロキサン粉体処理剤及び該処理剤により処理された粉体並びに該粉体を含有する化粧料 |
FR2902107A1 (fr) * | 2006-06-07 | 2007-12-14 | Rhodia Recherches & Tech | Composition organopolysiloxane pour mousse elastomere |
EP2043865B1 (de) * | 2006-07-13 | 2010-03-31 | Telecom Italia S.p.A. | Tintenstrahlpatrone mit einer aus einer härtbaren harzzusammensetzung hergestellten schicht |
GB0616021D0 (en) * | 2006-08-14 | 2006-09-20 | Dow Corning | Silicone release coating compositions |
JP5350267B2 (ja) * | 2006-12-21 | 2013-11-27 | ダウ・コーニング・コーポレイション | デュアル硬化ポリマー、その調製方法およびその使用 |
WO2008088523A1 (en) * | 2006-12-21 | 2008-07-24 | Dow Corning Corporation | Dual curing polymers and methods for their preparation and use |
DE102007047864A1 (de) * | 2007-11-26 | 2009-05-28 | Wacker Chemie Ag | Selbsthaftende expandierbare Siliconzusammensetzungen für die Herstellung von Siliconschaum-Verbundteilen |
EP2636705B1 (de) * | 2008-10-29 | 2018-12-19 | 3M Innovative Properties Company | Mit Elektronenstrahl gehärtete Haftklebemittel aus nichtfunktionalisiertem Silikon |
US8822560B2 (en) | 2008-10-29 | 2014-09-02 | 3M Innovative Properties Company | Electron beam cured silicone release materials |
WO2010056544A1 (en) | 2008-10-29 | 2010-05-20 | 3M Innovative Properties Company | Gentle to skin adhesive |
BRPI0919627A8 (pt) | 2008-10-29 | 2018-12-18 | 3M Innovative Properties Co | materiais de silicone curados com feixe de elétrons |
JP5594991B2 (ja) | 2009-07-29 | 2014-09-24 | 旭化成ワッカーシリコーン株式会社 | 接着性シリコーンゴム組成物 |
US9593209B2 (en) | 2009-10-22 | 2017-03-14 | Dow Corning Corporation | Process for preparing clustered functional polyorganosiloxanes, and methods for their use |
TWI502004B (zh) * | 2009-11-09 | 2015-10-01 | Dow Corning | 群集官能性聚有機矽氧烷之製法及其使用方法 |
KR20120132624A (ko) | 2010-02-12 | 2012-12-06 | 다우 코닝 코포레이션 | 반도체 가공을 위한 임시 웨이퍼 접합 방법 |
EP2563962B1 (de) | 2010-04-29 | 2017-09-13 | 3M Innovative Properties Company | Elektronenstrahlgehärtete silikonisierte faserbahnen |
KR20130140815A (ko) | 2010-12-08 | 2013-12-24 | 다우 코닝 코포레이션 | 봉지재의 형성에 적합한 실록산 조성물 |
US20140008697A1 (en) | 2010-12-08 | 2014-01-09 | Brian R. Harkness | Siloxane Compositions Including Titanium Dioxide Nanoparticles Suitable For Forming Encapsulants |
CN103314038A (zh) | 2010-12-08 | 2013-09-18 | 道康宁公司 | 适合形成封装物的包含金属氧化物纳米粒子的硅氧烷组合物 |
ITMI20111011A1 (it) | 2011-06-06 | 2012-12-07 | Telecom Italia Spa | Testina di stampa a getto d'inchiostro comprendente uno strato realizzato con una composizione di resina reticolabile |
WO2013036548A2 (en) | 2011-09-07 | 2013-03-14 | Dow Corning Corporation | Zirconium containing complex and condensation reaction catalysts, methods for preparing the catalysts, and compositions containing the catalysts |
CN103781823B (zh) | 2011-09-07 | 2016-08-17 | 道康宁公司 | 含钛络合物和缩合反应催化剂、制备该催化剂的方法以及包含该催化剂的组合物 |
US9545624B2 (en) | 2011-09-20 | 2017-01-17 | Dow Corning Corporation | Nickel containing hydrosilylation catalysts and compositions containing the catalysts |
JP6117211B2 (ja) | 2011-09-20 | 2017-04-19 | ダウ コーニング コーポレーションDow Corning Corporation | ルテニウム含有ヒドロシリル化触媒及びこの触媒を含有する組成物 |
JP6117210B2 (ja) | 2011-09-20 | 2017-04-19 | ダウ コーニング コーポレーションDow Corning Corporation | イリジウムを含有するヒドロシリル化触媒及びその触媒を含有する組成物 |
US9139699B2 (en) | 2012-10-04 | 2015-09-22 | Dow Corning Corporation | Metal containing condensation reaction catalysts, methods for preparing the catalysts, and compositions containing the catalysts |
WO2013081794A1 (en) | 2011-12-01 | 2013-06-06 | Dow Corning Corporation | Hydrosilylation reaction catalysts and curable compositions and methods for their preparation and use |
WO2013085882A1 (en) | 2011-12-06 | 2013-06-13 | Dow Corning Corporation | Curable silicone composition, cured material, manufactured articles, methods and uses |
CN104755542B (zh) | 2012-09-07 | 2017-12-26 | 3M创新有限公司 | 有机硅组合物及相关方法 |
EP2954025B1 (de) | 2013-02-11 | 2019-12-11 | Dow Silicones Corporation | Verfahren zur herstellung von thermisch leitenden/ thermisch radikalen härtbaren silikonzusammensetzungen |
CN104968751B (zh) | 2013-02-11 | 2017-04-19 | 道康宁公司 | 包含簇合官能化聚有机硅氧烷和有机硅反应性稀释剂的可固化有机硅组合物 |
WO2014124364A1 (en) | 2013-02-11 | 2014-08-14 | Dow Corning Corporation | Stable thermal radical curable silicone adhesive compositions |
KR102172738B1 (ko) | 2013-02-11 | 2020-11-02 | 다우 실리콘즈 코포레이션 | 클러스터형 작용성 폴리오르가노실록산, 이의 형성 방법, 및 이의 사용 방법 |
KR102192489B1 (ko) * | 2013-02-11 | 2020-12-17 | 다우 실리콘즈 코포레이션 | 열 전도성 열 라디칼 경화 실리콘 조성물을 형성하는 원 위치 방법 |
KR102244164B1 (ko) | 2013-02-11 | 2021-04-26 | 다우 실리콘즈 코포레이션 | 알콕시-작용성 실록산 반응성 수지를 포함하는 수분-경화성 핫멜트 실리콘 접착제 조성물 |
US9862867B2 (en) | 2013-02-11 | 2018-01-09 | Dow Corning Corporation | Alkoxy-functional organopolysiloxane resin and polymer and related methods for forming same |
WO2015077912A1 (en) * | 2013-11-26 | 2015-06-04 | Dow Corning (China) Holding Co., Ltd. | Novel silicone emulsion, water-based anchorage additive thereof and silicone release coating composition |
EP3196229B1 (de) | 2015-11-05 | 2018-09-26 | Dow Silicones Corporation | Verzweigte polyorganosiloxane und zugehörige härtbare zusammensetzungen, verfahren, verwendungen und vorrichtungen |
TWI738743B (zh) | 2016-03-23 | 2021-09-11 | 美商道康寧公司 | 金屬-聚有機矽氧烷 |
WO2017186586A1 (en) | 2016-04-25 | 2017-11-02 | Dow Corning Corporation | Aqueous coating composition |
TWI722207B (zh) * | 2016-06-15 | 2021-03-21 | 日商邁圖高新材料日本合同公司 | 硬化性聚有機矽氧烷組成物及其用途 |
KR102131611B1 (ko) * | 2016-07-13 | 2020-08-06 | 다우 실리콘즈 코포레이션 | 금속 비양성자성 유기실란옥사이드 화합물을 함유하는 제형 |
TW202007730A (zh) | 2018-07-31 | 2020-02-16 | 美商陶氏全球科技公司 | 組成物、形成自該組成物之經發泡聚矽氧彈性體、及形成方法 |
US20210317335A1 (en) * | 2018-09-13 | 2021-10-14 | Momentive Performance Materials Gmbh | Functional polysiloxanes |
CN115135705A (zh) * | 2020-02-05 | 2022-09-30 | 陶氏环球技术有限责任公司 | 发泡有机硅弹性体的制备 |
KR20240045267A (ko) * | 2021-08-11 | 2024-04-05 | 다우 글로벌 테크놀로지스 엘엘씨 | 발포 실리콘 생성물의 제조 |
WO2023172340A1 (en) | 2022-03-07 | 2023-09-14 | Dow Silicones Corporation | Method for preparing a laminate including a silicone pressure sensitive adhesive adhered to fluorosilicone rubber or silicone foam |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL131800C (de) * | 1965-05-17 | |||
US3923705A (en) * | 1974-10-30 | 1975-12-02 | Dow Corning | Method of preparing fire retardant siloxane foams and foams prepared therefrom |
US4026835A (en) * | 1975-07-14 | 1977-05-31 | Dow Corning Corporation | Method of preparing heat cured siloxane foams using rhodium catalyst and foams prepared therefrom |
US4026843A (en) * | 1975-07-14 | 1977-05-31 | Dow Corning Corporation | Foamable silicone gum stock having less skin thickness |
US4087585A (en) * | 1977-05-23 | 1978-05-02 | Dow Corning Corporation | Self-adhering silicone compositions and preparations thereof |
US4189545A (en) * | 1978-03-13 | 1980-02-19 | General Electric Company | Silicone foam composition which has burn resistant properties |
JPS60101146A (ja) * | 1983-11-08 | 1985-06-05 | Toshiba Silicone Co Ltd | 接着性を有するポリオルガノシロキサン組成物 |
US4593049A (en) * | 1985-10-16 | 1986-06-03 | Dow Corning Corporation | Method of producing elastomeric silicone foam |
US4590222A (en) * | 1985-10-16 | 1986-05-20 | Dow Corning Corporation | Lower density silicone elastomeric foam |
US4599367A (en) * | 1985-10-16 | 1986-07-08 | Dow Corning Corporation | Water-blown silicone foam |
US4659851A (en) * | 1986-03-26 | 1987-04-21 | Dow Corning Corporation | Novel organosilicon compounds |
JPS62240361A (ja) * | 1986-04-11 | 1987-10-21 | Toray Silicone Co Ltd | 硬化性オルガノポリシロキサン組成物 |
JP3270489B2 (ja) * | 1991-01-30 | 2002-04-02 | 東レ・ダウコーニング・シリコーン株式会社 | 硬化性オルガノポリシロキサン組成物 |
CA2064989A1 (en) * | 1991-04-23 | 1992-10-24 | Dawn M. Houghtaling | One part solventless conformal coatings |
GB9217151D0 (en) * | 1992-08-13 | 1992-09-23 | Dow Corning | Organosiloxane elastomeric foams |
US5252627A (en) * | 1993-01-04 | 1993-10-12 | Dow Corning Corporation | Apparatus and method for blending and dispensing foamable, curable organosiloxane compositions |
-
1996
- 1996-12-30 US US08/775,123 patent/US5683527A/en not_active Expired - Lifetime
-
1997
- 1997-05-01 US US08/846,446 patent/US5744507A/en not_active Expired - Lifetime
- 1997-12-15 TW TW086118915A patent/TW455624B/zh not_active IP Right Cessation
- 1997-12-18 DE DE69703021T patent/DE69703021T2/de not_active Expired - Lifetime
- 1997-12-18 EP EP97122354A patent/EP0851002B1/de not_active Expired - Lifetime
- 1997-12-24 AU AU49259/97A patent/AU726202B2/en not_active Ceased
- 1997-12-29 KR KR1019970076170A patent/KR100580799B1/ko not_active IP Right Cessation
-
1998
- 1998-01-05 JP JP00040298A patent/JP4018219B2/ja not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
KR100580799B1 (ko) | 2006-09-28 |
US5744507A (en) | 1998-04-28 |
EP0851002A2 (de) | 1998-07-01 |
AU726202B2 (en) | 2000-11-02 |
US5683527A (en) | 1997-11-04 |
JPH10195217A (ja) | 1998-07-28 |
DE69703021T2 (de) | 2001-05-03 |
TW455624B (en) | 2001-09-21 |
EP0851002B1 (de) | 2000-09-06 |
AU4925997A (en) | 1998-07-02 |
JP4018219B2 (ja) | 2007-12-05 |
EP0851002A3 (de) | 1998-11-11 |
KR19980064777A (ko) | 1998-10-07 |
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