DE69517542D1 - Verfahren zur Herstellung von Wasserstoffsuperoxyd und ein Reaktor für dieses Verfahren - Google Patents

Verfahren zur Herstellung von Wasserstoffsuperoxyd und ein Reaktor für dieses Verfahren

Info

Publication number
DE69517542D1
DE69517542D1 DE69517542T DE69517542T DE69517542D1 DE 69517542 D1 DE69517542 D1 DE 69517542D1 DE 69517542 T DE69517542 T DE 69517542T DE 69517542 T DE69517542 T DE 69517542T DE 69517542 D1 DE69517542 D1 DE 69517542D1
Authority
DE
Germany
Prior art keywords
reactor
working solution
top part
fixed bed
catalyst bed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69517542T
Other languages
English (en)
Other versions
DE69517542T2 (de
Inventor
Ilkka Turunen
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kemira Oyj
Original Assignee
Kemira Chemicals Oy
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kemira Chemicals Oy filed Critical Kemira Chemicals Oy
Application granted granted Critical
Publication of DE69517542D1 publication Critical patent/DE69517542D1/de
Publication of DE69517542T2 publication Critical patent/DE69517542T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/022—Preparation from organic compounds
    • C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/30—Loose or shaped packing elements, e.g. Raschig rings or Berl saddles, for pouring into the apparatus for mass or heat transfer
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/0007—Pressure measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00539—Pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00548—Flow
DE69517542T 1994-03-15 1995-03-15 Verfahren zur Herstellung von Wasserstoffsuperoxyd und ein Reaktor für dieses Verfahren Expired - Fee Related DE69517542T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FI941217A FI95457C (fi) 1994-03-15 1994-03-15 Menetelmä vetyperoksidin valmistamiseksi ja siinä käytettävä reaktori

Publications (2)

Publication Number Publication Date
DE69517542D1 true DE69517542D1 (de) 2000-07-27
DE69517542T2 DE69517542T2 (de) 2000-11-16

Family

ID=8540316

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69517542T Expired - Fee Related DE69517542T2 (de) 1994-03-15 1995-03-15 Verfahren zur Herstellung von Wasserstoffsuperoxyd und ein Reaktor für dieses Verfahren

Country Status (6)

Country Link
US (1) US5637286A (de)
EP (1) EP0672617B1 (de)
JP (1) JPH07300303A (de)
AT (1) ATE193998T1 (de)
DE (1) DE69517542T2 (de)
FI (1) FI95457C (de)

Families Citing this family (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19747407A1 (de) * 1997-10-27 1999-04-29 Basf Ag Verfahren zur Hydrierung einer Anthrachinon-Verbindung in Gegenwart eines mindestens ein Metall der VIII. Nebengruppe des Periodensystems als Aktivmetall enthaltenden Katalysators
GB2334028A (en) * 1998-02-04 1999-08-11 Solvay Making hydrogen peroxide by the anthraquinone process
DE19808385A1 (de) * 1998-02-27 1999-09-02 Basf Ag Verfahren zur Suspensionshydrierung einer Anthrachinon-Verbindung in einem speziellen Reaktor zur Herstellung von Wasserstoffperoxid
PL194706B1 (pl) * 1998-09-12 2007-06-29 Degussa Sposób przeprowadzania reakcji gazu z cieczą orazreaktor przepływowy do przeprowadzania tego sposobu
DE19841843A1 (de) * 1998-09-12 2000-03-30 Degussa Verfahren zur Durchführung von Gas-Flüssig-Reaktionen und Durchflußreaktor hierfür
DE19953185A1 (de) 1999-11-05 2001-05-23 Degussa Verfahren zur Herstellung von Wasserstoffperoxid
US6455023B1 (en) * 2000-10-11 2002-09-24 Corning Incorporated Metallic catalysts for non-neutral liquid media
DE10052323A1 (de) * 2000-10-21 2002-05-02 Degussa Kontinierliches Verfahren zur Hydrierung
WO2002051778A1 (en) * 2000-12-27 2002-07-04 Corning Incorporated Flow control in a three-phase monolithic catalyst reactor
FI110427B (fi) 2001-03-28 2003-01-31 Kemira Chemicals Oy Työliuoksen hydraus vetyperoksidin valmistusprosessissa
US7147833B2 (en) 2002-03-25 2006-12-12 Huckins Harold A Method for producing hydrogen peroxide from hydrogen and oxygen
EP1919824A4 (de) * 2005-08-31 2010-10-13 Fmc Corp Autoxidative herstellung von wasserstoffperoxid mittels hydrierung in einem mikroreaktor
CA2620353C (en) * 2005-08-31 2013-05-28 Fmc Corporation Auto-oxidation production of hydrogen peroxide via oxidation in a microreactor
CN102009960A (zh) * 2010-11-18 2011-04-13 清华大学 一种蒽醌法生产过氧化氢的加氢方法
US8474240B1 (en) * 2012-08-10 2013-07-02 NW Licensing Company LLC Regenerative gas generator
CN104418307B (zh) * 2013-08-22 2016-06-22 中国石油化工股份有限公司 一种蒽醌法生产双氧水多段氢化工艺
CN104418309B (zh) * 2013-09-05 2016-08-17 中国石油化工股份有限公司 一种过氧化氢的制备方法
CN107055481A (zh) * 2016-10-18 2017-08-18 上海睿思化工科技有限公司 一种过氧化氢的制备方法
CN106395755B (zh) * 2016-11-02 2019-12-10 上海睿思化工科技有限公司 一种蒽醌法制备过氧化氢的方法
CN109678120B (zh) * 2017-10-19 2020-06-09 中国石油化工股份有限公司 一种蒽醌法生产双氧水的氢化反应器及氢化方法
CN114644321A (zh) * 2020-12-21 2022-06-21 大连理工江苏研究院有限公司 一种基于蒽醌法制备过氧化氢的改进系统及工艺

Family Cites Families (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1227047A (en) * 1916-06-13 1917-05-22 William P Gray Brush.
BE519509A (de) * 1952-04-28
US2837411A (en) * 1952-11-25 1958-06-03 Olin Mathieson Process for production of hydrogen peroxide
US2966398A (en) * 1958-03-12 1960-12-27 Fmc Corp Production of hydrogen peroxide by slurrying the anthraquinone working soulution
US3009782A (en) * 1958-05-22 1961-11-21 Fmc Corp Production of hydrogen peroxide by anthraquinone process in the presence of a fixed bed catalyst
NL139013B (nl) * 1965-12-04 1973-06-15 Degussa Werkwijze voor het bereiden van waterstofperoxyde volgens het antrachinonkringloopprocede.
US3565581A (en) * 1968-05-16 1971-02-23 Fmc Corp Production of hydrogen peroxide in the anthraquinone process using a novel catalytic fixed bed
DE2042522C3 (de) * 1970-08-27 1979-01-25 Deutsche Gold- U. Silber-Scheideanstalt, Vormals Roessler, 6000 Frankfurt Verfahren zur Herstellung sehr reiner, wässriger, höher konzentrierter Wasserstoffperoxidlösungen
US3755552A (en) * 1970-10-21 1973-08-28 Fmc Corp Process for producing hydrogen peroxide
JPS59500228A (ja) * 1982-02-19 1984-02-16 ツルキンデン，ピエ−ル スポ−ツグラウンド舗装
US4428922A (en) * 1982-05-14 1984-01-31 Fmc Corporation Process for manufacturing hydrogen peroxide
SE431532B (sv) * 1982-09-08 1984-02-13 Eka Ab Forfarande vid framstellning av veteperoxid
US4428923A (en) * 1982-11-09 1984-01-31 Degussa Aktiengesellschaft Continuous process for the production of hydrogen peroxide according to the anthraquinone process
FI77633B (fi) * 1986-12-05 1988-12-30 Kemira Oy Foerfarande foer framstaellning av vaeteperoxid.
FI82669C (fi) * 1989-01-27 1991-04-10 Kemira Oy Foerfarande foer framstaellning av vaeteperoxid.
SE464867B (sv) * 1989-02-23 1991-06-24 Eka Nobel Ab Foerfarande vid framstaellning av vaeteperoxid enligt antrakinonprocessen

Also Published As

Publication number Publication date
US5637286A (en) 1997-06-10
FI95457C (fi) 1996-02-12
FI941217A0 (fi) 1994-03-15
DE69517542T2 (de) 2000-11-16
ATE193998T1 (de) 2000-07-15
FI95457B (fi) 1995-10-31
JPH07300303A (ja) 1995-11-14
EP0672617B1 (de) 2000-06-21
EP0672617A1 (de) 1995-09-20

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: KEMIRA OYJ, HELSINKI, FI

8339 Ceased/non-payment of the annual fee