DE69514839D1 - Verfahren zum herstellen von gereinigten acrylestern - Google Patents

Verfahren zum herstellen von gereinigten acrylestern

Info

Publication number
DE69514839D1
DE69514839D1 DE69514839T DE69514839T DE69514839D1 DE 69514839 D1 DE69514839 D1 DE 69514839D1 DE 69514839 T DE69514839 T DE 69514839T DE 69514839 T DE69514839 T DE 69514839T DE 69514839 D1 DE69514839 D1 DE 69514839D1
Authority
DE
Germany
Prior art keywords
acrylic esters
producing clean
clean acrylic
producing
esters
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69514839T
Other languages
English (en)
Other versions
DE69514839T2 (de
Inventor
Peter Arnoldy
Eric Kragtwijk
Paul Kremers
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Imperial Chemical Industries Ltd
Original Assignee
Imperial Chemical Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Imperial Chemical Industries Ltd filed Critical Imperial Chemical Industries Ltd
Application granted granted Critical
Publication of DE69514839D1 publication Critical patent/DE69514839D1/de
Publication of DE69514839T2 publication Critical patent/DE69514839T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
    • C07C69/52—Esters of acyclic unsaturated carboxylic acids having the esterified carboxyl group bound to an acyclic carbon atom
    • C07C69/533—Monocarboxylic acid esters having only one carbon-to-carbon double bond
    • C07C69/54—Acrylic acid esters; Methacrylic acid esters
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/48—Separation; Purification; Stabilisation; Use of additives
    • C07C67/52—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation
    • C07C67/54—Separation; Purification; Stabilisation; Use of additives by change in the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C67/00—Preparation of carboxylic acid esters
    • C07C67/36—Preparation of carboxylic acid esters by reaction with carbon monoxide or formates
    • C07C67/38—Preparation of carboxylic acid esters by reaction with carbon monoxide or formates by addition to an unsaturated carbon-to-carbon bond
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/22—Accessories

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69514839T 1994-08-18 1995-08-15 Verfahren zum herstellen von gereinigten acrylestern Expired - Fee Related DE69514839T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP94202354 1994-08-18
PCT/EP1995/003246 WO1996006066A1 (en) 1994-08-18 1995-08-15 Process for preparing refined acrylic esters

Publications (2)

Publication Number Publication Date
DE69514839D1 true DE69514839D1 (de) 2000-03-02
DE69514839T2 DE69514839T2 (de) 2000-06-15

Family

ID=8217104

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69514839T Expired - Fee Related DE69514839T2 (de) 1994-08-18 1995-08-15 Verfahren zum herstellen von gereinigten acrylestern

Country Status (13)

Country Link
US (1) US5968322A (de)
EP (1) EP0804407B1 (de)
JP (1) JPH10504553A (de)
KR (1) KR970704662A (de)
AU (1) AU3384395A (de)
BR (1) BR9508592A (de)
CA (1) CA2197666A1 (de)
DE (1) DE69514839T2 (de)
ES (1) ES2143067T3 (de)
MX (1) MX9701236A (de)
SK (1) SK21497A3 (de)
TW (1) TW360637B (de)
WO (1) WO1996006066A1 (de)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19746689A1 (de) * 1997-10-22 1999-04-29 Basf Ag Verfahren zur Herstellung von (Meth)acrylsäure
JP4143218B2 (ja) * 1999-04-23 2008-09-03 株式会社日本触媒 薄膜式蒸発装置における重合防止方法および薄膜式蒸発装置
FR2801306B1 (fr) 1999-11-24 2001-12-28 Atofina Procede de purification des monomeres (meth) acryliques par distillation
EP1201641B1 (de) * 2000-10-23 2013-08-14 Nippon Shokubai Co., Ltd. Zusammensetzungen von Vinylethergruppe-enthaltenden (Meth)acrylsäureestern und Verfahren zu ihrer Herstellung
TWI288756B (en) * 2001-12-24 2007-10-21 Ind Tech Res Inst Catalyst composition for living free radical polymerization and process for polymerizing (meth)acrylic, vinyl, vinylidene, and diene monomers using the catalyst composition
RU2350598C2 (ru) * 2003-11-28 2009-03-27 Мицубиси Кемикал Корпорейшн Способ очистки (мет)акриловой кислоты
WO2005102984A1 (ja) * 2004-04-26 2005-11-03 Daikin Industries, Ltd. 含フッ素アクリル酸エステルの製造方法
KR100601392B1 (ko) 2004-11-09 2006-07-13 한국화학연구원 에틸렌글리콜디(메타)아크릴레이트의 제조방법
US20080021241A1 (en) * 2004-11-12 2008-01-24 Carlson Curtis I Jr Process for production of methacrylic acid
CN104557539A (zh) * 2014-12-23 2015-04-29 安徽助成信息科技有限公司 一种丙烯酸甲酯（ma）与丙酸甲酯（mp）的分离方法
WO2016163553A1 (ja) * 2015-04-09 2016-10-13 ダイキン工業株式会社 アクリル酸誘導体含有組成物、及びアクリル酸誘導体の安定化方法
BR112023022355A2 (pt) 2021-04-28 2023-12-26 Mitsubishi Chem Corp Composição contendo metacrilato de metila e método de produção de polímero de metacrilato de metila
JPWO2022230915A1 (de) 2021-04-28 2022-11-03
WO2022230596A1 (ja) 2021-04-28 2022-11-03 三菱ケミカル株式会社 メタクリル酸メチル含有組成物
CN117203245A (zh) 2021-04-28 2023-12-08 三菱化学株式会社 含有甲基丙烯酸甲酯的组合物和甲基丙烯酸甲酯聚合物的制造方法
WO2022230914A1 (ja) 2021-04-28 2022-11-03 三菱ケミカル株式会社 メタクリル酸メチル含有組成物及びメタクリル酸メチル重合体の製造方法
CN117355501A (zh) 2021-11-30 2024-01-05 三菱化学株式会社 含有甲基丙烯酸甲酯的组合物、含有甲基丙烯酸甲酯的组合物的保存方法和甲基丙烯酸甲酯聚合物的制造方法
WO2023143974A1 (de) * 2022-01-28 2023-08-03 Basf Se Lagerung und/oder transport ethylenisch ungesättigter verbindungen

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA768651A (en) * 1967-10-03 J. Humphrey William Process for the preparation of acrylic acid esters
US908001A (en) * 1908-05-12 1908-12-29 Wilhelm Herbst Fireproof floor construction.
GB920353A (en) * 1959-12-10 1963-03-06 Knapsack Ag Process for stabilizing acrylic acid alkyl esters
US3666794A (en) * 1969-01-22 1972-05-30 Toyo Soda Mfg Co Ltd Stabilization of acrylic acid or esters thereof
JPS4915153B1 (de) * 1969-06-06 1974-04-12
GB1307582A (en) * 1969-06-10 1973-02-21 Rohm & Haas Inhibition of polymerization of acrylic acids
US3812175A (en) * 1970-01-26 1974-05-21 Nat Lead Co Multiple stage carbonylation process
BE787750A (fr) * 1971-08-20 1973-02-19 Union Carbide Corp Procede pour inhiber la polymerisation d'acrylates et methacrylates pendant leur distillation
US3988213A (en) * 1972-09-25 1976-10-26 Nippon Shokubai Kagaku Kogyo Co., Ltd. Method of distilling vinyl compounds
FR2201275A1 (en) * 1972-09-29 1974-04-26 Nippon Catalytic Chem Ind Distillation of (meth)acrylic monomers - in presence of polymerisation inhibitor in column with perforated plates, and without overflow tube
US4021310A (en) * 1972-12-22 1977-05-03 Nippon Shokubai Kagaku Kogyo Co., Ltd. Method for inhibiting the polymerization of acrylic acid or its esters
JPS52125116A (en) * 1976-04-12 1977-10-20 Mitsubishi Rayon Co Ltd Stabilization of methyl methacrylate
JPS59219252A (ja) * 1983-05-30 1984-12-10 Nippon Oil & Fats Co Ltd アクリル酸エステルまたはメタクリル酸エステルの精製法
GB8432376D0 (en) * 1984-12-21 1985-02-06 Shell Int Research Carbonylation of acetylenically unsaturated compounds
DE3543115A1 (de) * 1985-12-06 1987-06-11 Degussa Verfahren zur herstellung von tetrahydrofurfuryl-(2)-methacrylat und dazu geeigneter katalysator
EP0539628B1 (de) * 1991-10-30 1996-01-03 Shell Internationale Researchmaatschappij B.V. Verfahren zur Herstellung von Acrylestern
EP0571044B1 (de) * 1992-05-20 1997-04-09 Shell Internationale Researchmaatschappij B.V. Wiedergewinnung von Carbonsäureesterreaktionsprodukten
JP3684582B2 (ja) * 1993-08-09 2005-08-17 三菱化学株式会社 （メタ）アクリル酸又は（メタ）アクリル酸エステルの重合防止方法

Also Published As

Publication number Publication date
ES2143067T3 (es) 2000-05-01
SK21497A3 (en) 1997-11-05
MX9701236A (es) 1997-05-31
TW360637B (en) 1999-06-11
CA2197666A1 (en) 1996-02-29
BR9508592A (pt) 1997-12-23
DE69514839T2 (de) 2000-06-15
US5968322A (en) 1999-10-19
EP0804407B1 (de) 2000-01-26
JPH10504553A (ja) 1998-05-06
KR970704662A (ko) 1997-09-06
AU3384395A (en) 1996-03-14
WO1996006066A1 (en) 1996-02-29
EP0804407A1 (de) 1997-11-05

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee