DE69103472T2 - Monodisperses Kalziumkarbonat vom Vaterittyp, Verfahren zur Herstellung desselben und Verfahren zur Kontrolle des Teilchenwachstums und der Teilchenform. - Google Patents
Monodisperses Kalziumkarbonat vom Vaterittyp, Verfahren zur Herstellung desselben und Verfahren zur Kontrolle des Teilchenwachstums und der Teilchenform.Info
- Publication number
- DE69103472T2 DE69103472T2 DE69103472T DE69103472T DE69103472T2 DE 69103472 T2 DE69103472 T2 DE 69103472T2 DE 69103472 T DE69103472 T DE 69103472T DE 69103472 T DE69103472 T DE 69103472T DE 69103472 T2 DE69103472 T2 DE 69103472T2
- Authority
- DE
- Germany
- Prior art keywords
- calcium carbonate
- quicklime
- vaterite
- particle size
- methanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 title claims description 697
- 229910000019 calcium carbonate Inorganic materials 0.000 title claims description 298
- 239000002245 particle Substances 0.000 title claims description 164
- 238000000034 method Methods 0.000 title claims description 75
- 230000008569 process Effects 0.000 title claims description 32
- ODINCKMPIJJUCX-UHFFFAOYSA-N Calcium oxide Chemical compound [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 342
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 271
- 238000006243 chemical reaction Methods 0.000 claims description 208
- 239000000292 calcium oxide Substances 0.000 claims description 174
- 235000012255 calcium oxide Nutrition 0.000 claims description 171
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 123
- 239000011159 matrix material Substances 0.000 claims description 74
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 65
- 239000000920 calcium hydroxide Substances 0.000 claims description 63
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 63
- 238000003763 carbonization Methods 0.000 claims description 63
- 239000001569 carbon dioxide Substances 0.000 claims description 61
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 61
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 58
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 55
- 239000000203 mixture Substances 0.000 claims description 47
- 239000000725 suspension Substances 0.000 claims description 37
- 238000009826 distribution Methods 0.000 claims description 31
- 239000011164 primary particle Substances 0.000 claims description 21
- 239000007787 solid Substances 0.000 claims description 14
- 239000004572 hydraulic lime Substances 0.000 claims description 5
- 235000010216 calcium carbonate Nutrition 0.000 description 300
- 239000007789 gas Substances 0.000 description 54
- 230000000704 physical effect Effects 0.000 description 26
- 230000000052 comparative effect Effects 0.000 description 25
- 229920006267 polyester film Polymers 0.000 description 22
- 239000007900 aqueous suspension Substances 0.000 description 21
- 238000002441 X-ray diffraction Methods 0.000 description 19
- GBMDVOWEEQVZKZ-UHFFFAOYSA-N methanol;hydrate Chemical compound O.OC GBMDVOWEEQVZKZ-UHFFFAOYSA-N 0.000 description 19
- 238000001878 scanning electron micrograph Methods 0.000 description 17
- 238000000635 electron micrograph Methods 0.000 description 15
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 14
- 229920000728 polyester Polymers 0.000 description 14
- 238000004519 manufacturing process Methods 0.000 description 13
- 238000004220 aggregation Methods 0.000 description 12
- 230000002776 aggregation Effects 0.000 description 12
- 239000010954 inorganic particle Substances 0.000 description 12
- 238000003756 stirring Methods 0.000 description 12
- 238000002360 preparation method Methods 0.000 description 11
- 239000011541 reaction mixture Substances 0.000 description 11
- 239000010419 fine particle Substances 0.000 description 10
- 238000005259 measurement Methods 0.000 description 10
- 230000015572 biosynthetic process Effects 0.000 description 9
- 239000013078 crystal Substances 0.000 description 8
- 239000006185 dispersion Substances 0.000 description 8
- 238000001879 gelation Methods 0.000 description 7
- 229910021532 Calcite Inorganic materials 0.000 description 6
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 6
- 239000000377 silicon dioxide Substances 0.000 description 6
- 239000002002 slurry Substances 0.000 description 6
- 239000012798 spherical particle Substances 0.000 description 6
- 238000005299 abrasion Methods 0.000 description 5
- 239000003795 chemical substances by application Substances 0.000 description 5
- 239000011362 coarse particle Substances 0.000 description 5
- 238000000576 coating method Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 230000000877 morphologic effect Effects 0.000 description 5
- 239000011163 secondary particle Substances 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 239000011248 coating agent Substances 0.000 description 4
- 239000000945 filler Substances 0.000 description 4
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 4
- 239000000049 pigment Substances 0.000 description 4
- 239000000843 powder Substances 0.000 description 4
- 239000005995 Aluminium silicate Substances 0.000 description 3
- 235000019738 Limestone Nutrition 0.000 description 3
- 235000012211 aluminium silicate Nutrition 0.000 description 3
- 238000001354 calcination Methods 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 239000006028 limestone Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000003973 paint Substances 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 239000005060 rubber Substances 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 238000001238 wet grinding Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- -1 alkali metal salt Chemical class 0.000 description 2
- 150000001447 alkali salts Chemical class 0.000 description 2
- 239000012298 atmosphere Substances 0.000 description 2
- 239000011324 bead Substances 0.000 description 2
- 238000007664 blowing Methods 0.000 description 2
- NKWPZUCBCARRDP-UHFFFAOYSA-L calcium bicarbonate Chemical compound [Ca+2].OC([O-])=O.OC([O-])=O NKWPZUCBCARRDP-UHFFFAOYSA-L 0.000 description 2
- 229910000020 calcium bicarbonate Inorganic materials 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000008021 deposition Effects 0.000 description 2
- 239000002612 dispersion medium Substances 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 230000004660 morphological change Effects 0.000 description 2
- 239000003960 organic solvent Substances 0.000 description 2
- 239000000123 paper Substances 0.000 description 2
- KJFMBFZCATUALV-UHFFFAOYSA-N phenolphthalein Chemical compound C1=CC(O)=CC=C1C1(C=2C=CC(O)=CC=2)C2=CC=CC=C2C(=O)O1 KJFMBFZCATUALV-UHFFFAOYSA-N 0.000 description 2
- 102000054765 polymorphisms of proteins Human genes 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- QNRATNLHPGXHMA-XZHTYLCXSA-N (r)-(6-ethoxyquinolin-4-yl)-[(2s,4s,5r)-5-ethyl-1-azabicyclo[2.2.2]octan-2-yl]methanol;hydrochloride Chemical compound Cl.C([C@H]([C@H](C1)CC)C2)CN1[C@@H]2[C@H](O)C1=CC=NC2=CC=C(OCC)C=C21 QNRATNLHPGXHMA-XZHTYLCXSA-N 0.000 description 1
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- PQUXFUBNSYCQAL-UHFFFAOYSA-N 1-(2,3-difluorophenyl)ethanone Chemical compound CC(=O)C1=CC=CC(F)=C1F PQUXFUBNSYCQAL-UHFFFAOYSA-N 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 235000006508 Nelumbo nucifera Nutrition 0.000 description 1
- 240000002853 Nelumbo nucifera Species 0.000 description 1
- 235000006510 Nelumbo pentapetala Nutrition 0.000 description 1
- 229920000388 Polyphosphate Polymers 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000008186 active pharmaceutical agent Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000002981 blocking agent Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 239000001110 calcium chloride Substances 0.000 description 1
- 229910001628 calcium chloride Inorganic materials 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000003990 capacitor Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 230000008094 contradictory effect Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 229910021641 deionized water Inorganic materials 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 238000009837 dry grinding Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000004299 exfoliation Methods 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000003546 flue gas Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 150000002681 magnesium compounds Chemical class 0.000 description 1
- 239000000696 magnetic material Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002609 medium Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000001139 pH measurement Methods 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 239000001205 polyphosphate Substances 0.000 description 1
- 235000011176 polyphosphates Nutrition 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 229940047670 sodium acrylate Drugs 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 239000012756 surface treatment agent Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 230000002123 temporal effect Effects 0.000 description 1
- 238000001132 ultrasonic dispersion Methods 0.000 description 1
- 230000037303 wrinkles Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
- C01F11/184—Preparation of calcium carbonate by carbonation of solutions based on non-aqueous solvents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F11/00—Compounds of calcium, strontium, or barium
- C01F11/18—Carbonates
- C01F11/182—Preparation of calcium carbonate by carbonation of aqueous solutions and characterised by an additive other than CaCO3-seeds
- C01F11/183—Preparation of calcium carbonate by carbonation of aqueous solutions and characterised by an additive other than CaCO3-seeds the additive being an organic compound
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F5/00—Compounds of magnesium
- C01F5/24—Magnesium carbonates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/20—Particle morphology extending in two dimensions, e.g. plate-like
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Nanotechnology (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP13748390A JP2882852B2 (ja) | 1990-05-28 | 1990-05-28 | 単分散した板状炭酸カルシウム及びその製造方法 |
| JP13748290A JP2956041B2 (ja) | 1990-05-28 | 1990-05-28 | フィルムのブロッキング防止用球状又は楕円球状バテライト炭酸カルシウム |
| JP3081532A JP3043454B2 (ja) | 1991-03-20 | 1991-03-20 | バテライト型炭酸カルシウムの粒子成長方法、形態制御方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69103472D1 DE69103472D1 (de) | 1994-09-22 |
| DE69103472T2 true DE69103472T2 (de) | 1994-12-08 |
Family
ID=27303613
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69103472T Expired - Fee Related DE69103472T2 (de) | 1990-05-28 | 1991-05-28 | Monodisperses Kalziumkarbonat vom Vaterittyp, Verfahren zur Herstellung desselben und Verfahren zur Kontrolle des Teilchenwachstums und der Teilchenform. |
Country Status (5)
| Country | Link |
|---|---|
| US (2) | US5275651A (enExample) |
| EP (1) | EP0459399B1 (enExample) |
| KR (1) | KR0176250B1 (enExample) |
| DE (1) | DE69103472T2 (enExample) |
| TW (1) | TW198000B (enExample) |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5275651A (en) * | 1990-05-28 | 1994-01-04 | Maruo Calcium Company Limited | Monodisperse vaterite type calcium carbonate, its manufacturing method and method of controlling growth of particles and shape thereof |
| EP0488603B1 (en) * | 1990-11-26 | 2000-01-19 | Teijin Limited | Biaxially oriented polyester film |
| EP0847420B1 (en) * | 1995-08-29 | 2000-02-16 | Exxon Chemical Patents Inc. | Radiation tolerant polypropylene and its useful articles |
| KR100204117B1 (ko) * | 1996-09-11 | 1999-06-15 | 유규재 | 탄산칼슘의 제조법 |
| FI105471B (fi) * | 1997-09-08 | 2000-08-31 | Fp Pigments Oy | Menetelmä kalsiumkarbonaattipartikkelien valmistamiseksi |
| FI105470B (fi) * | 1997-09-08 | 2000-08-31 | Fp Pigments Oy | Menetelmä ja laitteisto saostetun kalsiumkarbonaatin tuottamiseksi |
| DE69801140T2 (de) * | 1997-09-12 | 2001-11-29 | Nippon Paper Industries Co. Ltd., Tokio/Tokyo | Verfahren zur Herstellung von beschichtetem Druckpapier |
| US6251356B1 (en) | 1999-07-21 | 2001-06-26 | G. R. International, Inc. | High speed manufacturing process for precipitated calcium carbonate employing sequential perssure carbonation |
| US7048900B2 (en) * | 2001-01-31 | 2006-05-23 | G.R. International, Inc. | Method and apparatus for production of precipitated calcium carbonate and silicate compounds in common process equipment |
| FR2821095B1 (fr) * | 2001-02-16 | 2003-04-11 | Arjo Wiggins Sa | Procede d'obtention d'une feuille papetiere comportant de la calcite |
| JP3484425B2 (ja) * | 2001-03-14 | 2004-01-06 | 花王株式会社 | 歯磨剤 |
| FI118734B (fi) * | 2002-05-31 | 2008-02-29 | Preseco Oy | Menetelmä eloperäisen materiaalin jäännöksen käsittelemiseksi |
| RU2246445C2 (ru) * | 2002-06-05 | 2005-02-20 | Пойлов Владимир Зотович | Способ получения крупнодисперсного химически осажденного карбоната кальция с пластинчатой формой частиц |
| US7166271B2 (en) * | 2003-10-28 | 2007-01-23 | J.M. Huber Corporation | Silica-coated boehmite composites suitable for dentifrices |
| US20050106110A1 (en) * | 2003-11-19 | 2005-05-19 | Sung-Tsuen Liu | Stabilized vaterite |
| US7361324B2 (en) * | 2004-06-21 | 2008-04-22 | J. M. Huber Corporation | Precipitated calcium carbonate |
| WO2006011872A1 (en) * | 2004-06-25 | 2006-02-02 | J.M. Huber Corporation | Stabilized vaterite |
| US7422999B2 (en) * | 2005-02-14 | 2008-09-09 | The Lubrizol Corporation | Overbased vaterite containing salt composition |
| CN100378003C (zh) * | 2005-03-31 | 2008-04-02 | 中国石油化工股份有限公司 | 一种制备六方碳钙石的方法 |
| JP4897687B2 (ja) * | 2005-09-06 | 2012-03-14 | 丸尾カルシウム株式会社 | 粉体塗料用充填剤及びそれを配合してなる粉体塗料組成物 |
| WO2009019536A1 (en) * | 2007-08-03 | 2009-02-12 | Tas Ahmet Cueneyt | Calcium carbonate microtablets and method for the preparation thereof |
| US20100239467A1 (en) * | 2008-06-17 | 2010-09-23 | Brent Constantz | Methods and systems for utilizing waste sources of metal oxides |
| US20100144521A1 (en) * | 2008-05-29 | 2010-06-10 | Brent Constantz | Rocks and Aggregate, and Methods of Making and Using the Same |
| CN101910469A (zh) | 2008-07-16 | 2010-12-08 | 卡勒拉公司 | 电化学系统中的co2利用 |
| EP2200948A4 (en) | 2008-09-30 | 2014-09-03 | Calera Corp | CO2 SEQUESTRATING BUILDING MATERIALS |
| US8869477B2 (en) | 2008-09-30 | 2014-10-28 | Calera Corporation | Formed building materials |
| US7815880B2 (en) * | 2008-09-30 | 2010-10-19 | Calera Corporation | Reduced-carbon footprint concrete compositions |
| US20100258035A1 (en) * | 2008-12-24 | 2010-10-14 | Brent Constantz | Compositions and methods using substances containing carbon |
| EP2240629A4 (en) * | 2009-01-28 | 2013-04-24 | Calera Corp | SOLUTION OF LOW ENERGY ELECTROCHEMICAL ION BICARBONATES |
| CN101918614A (zh) | 2009-02-10 | 2010-12-15 | 卡勒拉公司 | 用氢和电催化电极低电压生产碱 |
| US8883104B2 (en) * | 2009-03-02 | 2014-11-11 | Calera Corporation | Gas stream multi-pollutants control systems and methods |
| US20110147227A1 (en) * | 2009-07-15 | 2011-06-23 | Gilliam Ryan J | Acid separation by acid retardation on an ion exchange resin in an electrochemical system |
| KR101831979B1 (ko) | 2011-04-13 | 2018-02-23 | 마루오 칼슘 가부시키가이샤 | 수지용 탄산칼슘 충전재, 그 제조 방법, 및 이 충전재를 포함하는 수지 조성물 |
| DK2766434T4 (da) * | 2011-10-13 | 2023-03-13 | Biosenta Inc | Fremgangsmåde og apparat til fremstilling af calciumcarbonat-belagte calciumhydroxid-partikler |
| BE1021564B1 (fr) * | 2013-01-30 | 2015-12-14 | S.A. Lhoist Recherche Et Developpement | Procede de preparation de gel de carbonate de calcium et produit ainsi obtenu. |
| CN103395812B (zh) * | 2013-07-11 | 2015-01-07 | 大连理工大学 | 一种控制固体碳化法中碳酸钙形貌的方法 |
| CN103623768B (zh) * | 2013-12-09 | 2016-01-06 | 王岩 | 钙基二氧化碳吸附剂及其制备方法 |
| WO2015164589A1 (en) | 2014-04-23 | 2015-10-29 | Calera Corporation | Methods and systems for utilizing carbide lime or slag |
| CN107337225B (zh) * | 2017-04-20 | 2019-07-12 | 广西民族大学 | 一种纳米椭球形碳酸钙颗粒的制备方法 |
| JP7705661B2 (ja) | 2019-07-21 | 2025-07-10 | アレラク， インコーポレイテッド | 焼成石灰石由来のカルシウム化合物を利用するための方法およびシステム |
| US11697598B2 (en) | 2020-02-25 | 2023-07-11 | Arelac, Inc. | Methods and systems for treatment of limestone to form vaterite |
| CN111393879A (zh) * | 2020-04-20 | 2020-07-10 | 池州市贵兴非矿新材料有限公司 | 一种轻质碳酸钙改性工艺 |
| EP4171785A4 (en) | 2020-06-30 | 2024-07-03 | Arelac, Inc. | METHODS AND SYSTEMS FOR PRODUCING VATERIT FROM CALCINATED LIMESTONE USING AN ELECTRIC FURNACE |
| CN116282113B (zh) * | 2023-01-16 | 2025-10-17 | 中南大学 | 一种利用垃圾焚烧飞灰水洗液固化二氧化碳制备高附加值碳酸钙的方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2538802A (en) * | 1947-05-03 | 1951-01-23 | Ecusta Paper Corp | Method of manufacturing calcium carbonate |
| US3321269A (en) * | 1964-07-07 | 1967-05-23 | Toa Gosei Kagaku Kogyo Kabushi | Process for the production of crystalline calcium carbonate of vaterite type |
| US4793985A (en) * | 1982-08-23 | 1988-12-27 | J. M. Huber Corporation | Method of producing ultrafine ground calcium carbonate |
| EP0179597B1 (en) * | 1984-10-18 | 1993-02-03 | Pfizer Inc. | Spherically shaped precipitated calcium carbonate, its preparation and use |
| DE3617169C2 (de) * | 1986-05-22 | 1996-05-23 | Pluss Stauffer Ag | Carbonathaltige mineralische Füllstoffe und Pigmente |
| US4732748A (en) * | 1986-12-10 | 1988-03-22 | Cyprus Mines Corporation | Finely divided calcium carbonate compositions |
| JPH01119512A (ja) * | 1987-10-31 | 1989-05-11 | Agency Of Ind Science & Technol | 板状塩基性炭酸カルシウムの製造方法 |
| US4835195A (en) * | 1988-08-12 | 1989-05-30 | Rayfield Jerry W | Dry ground/wet ground calcium carbonate filler compositions |
| JPH02243514A (ja) * | 1989-03-15 | 1990-09-27 | Kyodo Kumiai Tsukumi Fine Ceramics Kenkyu Center | 微細球状バテライト系炭酸カルシウムの製造方法 |
| US5275651A (en) * | 1990-05-28 | 1994-01-04 | Maruo Calcium Company Limited | Monodisperse vaterite type calcium carbonate, its manufacturing method and method of controlling growth of particles and shape thereof |
-
1991
- 1991-05-28 US US07/706,423 patent/US5275651A/en not_active Expired - Fee Related
- 1991-05-28 EP EP91108695A patent/EP0459399B1/en not_active Expired - Lifetime
- 1991-05-28 DE DE69103472T patent/DE69103472T2/de not_active Expired - Fee Related
- 1991-05-28 KR KR1019910008739A patent/KR0176250B1/ko not_active Expired - Fee Related
- 1991-06-01 TW TW080104299A patent/TW198000B/zh active
-
1993
- 1993-10-19 US US08/138,048 patent/US5494651A/en not_active Expired - Fee Related
Also Published As
| Publication number | Publication date |
|---|---|
| EP0459399A1 (en) | 1991-12-04 |
| EP0459399B1 (en) | 1994-08-17 |
| KR910019907A (ko) | 1991-12-19 |
| US5275651A (en) | 1994-01-04 |
| US5494651A (en) | 1996-02-27 |
| TW198000B (enExample) | 1993-01-11 |
| KR0176250B1 (ko) | 1999-03-20 |
| DE69103472D1 (de) | 1994-09-22 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE69103472T2 (de) | Monodisperses Kalziumkarbonat vom Vaterittyp, Verfahren zur Herstellung desselben und Verfahren zur Kontrolle des Teilchenwachstums und der Teilchenform. | |
| DE69128730T2 (de) | Verfahren zur Verbesserung der optischen Eigenschaften von Papier | |
| DE69104436T2 (de) | Ausgefälltes Calciumcarbonat. | |
| DE69202933T2 (de) | Kalzium-Magnesiumkarbonatzusammensetzung und Herstellungsverfahren. | |
| EP1151966B1 (de) | Stabiles, plättchenförmiges, calcitisches Calciumcarbonat, Verfahren zu dessen Herstellung und seine Verwendung | |
| DE69431664T2 (de) | Verfahren zur herstellung von kugelartigen aggregaten aus plättchenförmigem synthetischem hydrotalcit | |
| DE1592147C3 (de) | Verfahren zur Herstellung von Kalzit mit neuartigem Kristallhabitus | |
| DE69634164T2 (de) | Aluminiumoxydteilchen mit erhöhter Dispergierbarkeit und Plastizität und Verfahren zu ihrer Herstellung | |
| DE3685782T2 (de) | Magnesiumhydroxyd und verfahren zu seiner herstellung. | |
| EP0014382A2 (de) | Plättchenförmige Eisenoxidpigmente und Verfahren zu deren Herstellung sowie deren Verwendung | |
| DE202012012628U1 (de) | Gefällte Calciumcarbonatteilchen und Verwendung davon | |
| DE102007018975A1 (de) | Kugelförmige Calciumcarbonat-Teilchen | |
| DE69122549T2 (de) | Valerit-Typ-Kalziumkarbonat enthaltende Polyesterzusammensetzung | |
| EP1222146B1 (de) | Verfahren zur kontinuierlichen herstellung von gefälltem calciumcarbonat | |
| EP0327660B1 (de) | Verfahren zur Herstellung von Füllstoffen und Flammschutzmitteln auf der Basis von Aluminiumhydroxid in Form von Hydrargillit | |
| EP0143363B1 (de) | Calcitischer Füllstoff und Verfahren zu seiner Herstellung | |
| DE102008026268A1 (de) | Verfahren zur Herstellung eines lagerstabilen Bariumsulfats mit guter Dispergierbarkeit | |
| DE60116259T3 (de) | Zusammengesetzte pigmente enthaltend in situ gefälltem calciumcarbonat | |
| DE2151471B2 (de) | Stabilisierte, ferromagnetische chromdioxidteilchen und verfahren zu deren herstellung | |
| JP3768540B2 (ja) | バテライト型炭酸カルシウムの形態制御方法・粒子成長方法 | |
| DE1134974B (de) | Verfahren zur Herstellung von feindispersem Calciumcarbonat | |
| JP3043454B2 (ja) | バテライト型炭酸カルシウムの粒子成長方法、形態制御方法 | |
| EP0543843B1 (de) | Verfahren zur herstellung von metallhydroxiden mit geringer spezifischer oberfläche | |
| EP0368093B1 (de) | Herstellung von nadelförmigem, im wesentlichen aus eisenhaltigem Chromdioxid bestehenden, ferromagnetischen Material | |
| DE69115245T2 (de) | Neue Pigmente auf Aluminiumsilikat-Basis, Verfahren zu ihrer Produktion sowie ihre Benutzung als Füllstoffe besonders für Papier. |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |