DE68909166T2 - Verfahren zur Herstellung von in 5-Stellung substituierten 3-Furaldehyden. - Google Patents
Verfahren zur Herstellung von in 5-Stellung substituierten 3-Furaldehyden.Info
- Publication number
- DE68909166T2 DE68909166T2 DE89310601T DE68909166T DE68909166T2 DE 68909166 T2 DE68909166 T2 DE 68909166T2 DE 89310601 T DE89310601 T DE 89310601T DE 68909166 T DE68909166 T DE 68909166T DE 68909166 T2 DE68909166 T2 DE 68909166T2
- Authority
- DE
- Germany
- Prior art keywords
- furaldehydes
- substituted
- preparation
- followed
- lithium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- AZVSIHIBYRHSLB-UHFFFAOYSA-N 3-furaldehyde Chemical group O=CC=1C=COC=1 AZVSIHIBYRHSLB-UHFFFAOYSA-N 0.000 title abstract 2
- -1 5-substituted-3-furaldehydes Chemical class 0.000 abstract 1
- 239000012039 electrophile Substances 0.000 abstract 1
- WGOPGODQLGJZGL-UHFFFAOYSA-N lithium;butane Chemical compound [Li+].CC[CH-]C WGOPGODQLGJZGL-UHFFFAOYSA-N 0.000 abstract 1
- AXSMTZCJJBPZAA-UHFFFAOYSA-N lithium;morpholin-4-ide Chemical compound [Li]N1CCOCC1 AXSMTZCJJBPZAA-UHFFFAOYSA-N 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/0803—Compounds with Si-C or Si-Si linkages
- C07F7/0825—Preparations of compounds not comprising Si-Si or Si-cyano linkages
- C07F7/0827—Syntheses with formation of a Si-C bond
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/22—Tin compounds
- C07F7/2208—Compounds having tin linked only to carbon, hydrogen and/or halogen
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Furan Compounds (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Nitrogen And Oxygen As The Only Ring Hetero Atoms (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Photoreceptors In Electrophotography (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Pyridine Compounds (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/259,225 US4935530A (en) | 1988-10-18 | 1988-10-18 | Process for preparing 5-substituted-3-furaldehydes |
Publications (2)
Publication Number | Publication Date |
---|---|
DE68909166D1 DE68909166D1 (de) | 1993-10-21 |
DE68909166T2 true DE68909166T2 (de) | 1994-02-10 |
Family
ID=22984077
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE89310601T Expired - Fee Related DE68909166T2 (de) | 1988-10-18 | 1989-10-16 | Verfahren zur Herstellung von in 5-Stellung substituierten 3-Furaldehyden. |
Country Status (19)
Country | Link |
---|---|
US (1) | US4935530A (de) |
EP (1) | EP0365256B1 (de) |
JP (1) | JPH02164876A (de) |
KR (1) | KR900006311A (de) |
CN (1) | CN1023802C (de) |
AT (1) | ATE94552T1 (de) |
AU (1) | AU614474B2 (de) |
CA (1) | CA2000677A1 (de) |
DE (1) | DE68909166T2 (de) |
DK (1) | DK517889A (de) |
ES (1) | ES2044137T3 (de) |
FI (1) | FI894924A0 (de) |
HU (1) | HU204806B (de) |
IE (1) | IE63693B1 (de) |
IL (1) | IL91981A0 (de) |
NO (1) | NO172799C (de) |
NZ (1) | NZ231026A (de) |
PT (1) | PT92016B (de) |
ZA (1) | ZA897768B (de) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5082954A (en) * | 1987-06-08 | 1992-01-21 | Allergan, Inc. | Intermediates and processes for preparing 4-substituted 2-5(H)-furanones as anti-inflammatory agents |
US5322953A (en) * | 1987-06-08 | 1994-06-21 | Allergan, Inc. | 2-trialkylsilyl-3-furaldehydes |
US5171863A (en) * | 1987-06-08 | 1992-12-15 | Allergan, Inc. | Intermediates for preparing 4-substituted 2-5(H)-furanones as anti-inflammatory agents |
US5043457A (en) * | 1990-04-17 | 1991-08-27 | Allergan, Inc. | 2(5H)-furanones substituted in the 3 position, as Ca2+ channel antagonists and anti-inflammatory agents |
US5037811A (en) * | 1990-04-17 | 1991-08-06 | Allergan, Inc. | 4-(oxygen, sulfur or nitrogen substituted)-methyl 5-hydroxy-2(5H)-furanones as anti-inflammatory agents |
US5134128A (en) * | 1987-06-08 | 1992-07-28 | Allergan, Inc. | Anti-inflammatory furanones |
US5045564A (en) * | 1988-12-07 | 1991-09-03 | Allergan, Inc. | Anti-inflammatory 2-furanones |
US5258400A (en) * | 1989-11-20 | 1993-11-02 | Allergan, Inc. | Anti-inflammatory furanone compounds |
US5112853A (en) * | 1989-11-20 | 1992-05-12 | Allergan, Inc. | Anti-inflammatory furanone compounds |
US5225571A (en) * | 1991-04-30 | 1993-07-06 | Allergan, Inc. | Substituted dihydroxy-bis-[5-hydroxy-2(5H)-furanone-4-yl]-alkanes as anti-inflammatory agents |
US5183906A (en) * | 1991-04-30 | 1993-02-02 | Allergan, Inc. | 2- and 5-alkyl and phenyl substituted 4-(1-hydroxy, 1-acyloxy or 1-carbamoyloxy)-5-hydroxy-2 (5h)-furanones as anti-inflammatory agents |
US5171864A (en) * | 1991-08-30 | 1992-12-15 | Allergan, Inc. | Di-(5-hydroxy-2(5H)-2-oxo-4-furyl)methyl-alpha,omega alkane-dioates and N,N-bis-(5-hydroxy-2(5H)-2-oxo-4-furyl)methyl-alpha,omega-dialkanoic acid amides as anti-inflammatory agents |
US5169963A (en) * | 1991-08-30 | 1992-12-08 | Allergan, Inc. | Di-(5-hydroxy-2(5H)2-oxo-4-furyl)alkylmethyl-alpha,omega alkanedioates and N,N-bis-(5-hydroxy-2(5H)2-oxo-4-furyl)alkylmethyl-alpha,omega-dialkanoic acid amides as anti-inflammatory agents |
US5268387A (en) * | 1992-04-24 | 1993-12-07 | Allergan, Inc. | Pharmaceutical compositions and method for administering 3 and 4-substituted 2(5H)-furanones to a mammal for inhibiting bone loss |
US5451686A (en) * | 1994-04-15 | 1995-09-19 | Allergan, Inc. | 3 and 5 alkyl and phenyl 4-(hydroxy or acyloxy)-alkyl substituted 2(5H)-furanones as anti-inflammatory agents |
US5639468A (en) * | 1995-06-07 | 1997-06-17 | University Of Southern California | Method for reducing or preventing post-surgical adhesion formation using manoalide and analogs thereof |
US7393963B2 (en) * | 2004-12-10 | 2008-07-01 | Archer-Daniels-Midland Company | Conversion of 2,5-(hydroxymethyl)furaldehyde to industrial derivatives, purification of the derivatives, and industrial uses therefor |
US7317116B2 (en) | 2004-12-10 | 2008-01-08 | Archer-Daniels-Midland-Company | Processes for the preparation and purification of hydroxymethylfuraldehyde and derivatives |
KR101463933B1 (ko) * | 2012-08-14 | 2014-11-26 | 한국과학기술원 | 5-치환된 또는 2,5-치환된 3-푸르알데히드 유도체의 제조방법 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4221585A (en) * | 1978-08-04 | 1980-09-09 | E. I. Du Pont De Nemours And Company | N-[(2,6-Dimethoxypyrimidin-4-yl)]aminocarbonyl benzene sulfonamides and their herbicidal compositions and methods of use |
US4195026A (en) * | 1978-12-04 | 1980-03-25 | Iowa State University Research Foundation, Inc. | Substituted furans from butenolides |
US4500520A (en) * | 1983-03-01 | 1985-02-19 | E. I. Du Pont De Nemours And Company | Antiinflammatory and/or analgesic silylfurans |
JPH01501935A (ja) * | 1986-04-07 | 1989-07-06 | ジ・アップジョン・カンパニー | 駆虫薬アシルヒドラゾン、使用方法および組成物 |
GB8609452D0 (en) * | 1986-04-17 | 1986-05-21 | Ici Plc | Fungicides |
CA1329390C (en) * | 1987-06-08 | 1994-05-10 | John N. Bonfiglio | Anti-inflammatory furanones |
-
1988
- 1988-10-18 US US07/259,225 patent/US4935530A/en not_active Expired - Lifetime
-
1989
- 1989-10-13 CA CA002000677A patent/CA2000677A1/en not_active Abandoned
- 1989-10-13 ZA ZA897768A patent/ZA897768B/xx unknown
- 1989-10-13 IL IL91981A patent/IL91981A0/xx not_active IP Right Cessation
- 1989-10-16 EP EP89310601A patent/EP0365256B1/de not_active Expired - Lifetime
- 1989-10-16 NZ NZ231026A patent/NZ231026A/en unknown
- 1989-10-16 AT AT89310601T patent/ATE94552T1/de not_active IP Right Cessation
- 1989-10-16 ES ES89310601T patent/ES2044137T3/es not_active Expired - Lifetime
- 1989-10-16 DE DE89310601T patent/DE68909166T2/de not_active Expired - Fee Related
- 1989-10-16 KR KR1019890014842A patent/KR900006311A/ko not_active Application Discontinuation
- 1989-10-17 FI FI894924A patent/FI894924A0/fi not_active Application Discontinuation
- 1989-10-17 IE IE333589A patent/IE63693B1/en not_active IP Right Cessation
- 1989-10-17 HU HU895337A patent/HU204806B/hu not_active IP Right Cessation
- 1989-10-17 NO NO894133A patent/NO172799C/no unknown
- 1989-10-17 PT PT92016A patent/PT92016B/pt not_active IP Right Cessation
- 1989-10-17 AU AU42968/89A patent/AU614474B2/en not_active Ceased
- 1989-10-18 DK DK517889A patent/DK517889A/da not_active Application Discontinuation
- 1989-10-18 JP JP1274778A patent/JPH02164876A/ja active Pending
- 1989-10-18 CN CN89108793A patent/CN1023802C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
AU614474B2 (en) | 1991-08-29 |
DK517889A (da) | 1990-04-19 |
KR900006311A (ko) | 1990-05-07 |
ATE94552T1 (de) | 1993-10-15 |
JPH02164876A (ja) | 1990-06-25 |
HUT51266A (en) | 1990-04-28 |
FI894924A0 (fi) | 1989-10-17 |
HU204806B (en) | 1992-02-28 |
EP0365256B1 (de) | 1993-09-15 |
NO172799B (no) | 1993-06-01 |
NO894133L (no) | 1990-04-19 |
DK517889D0 (da) | 1989-10-18 |
ES2044137T3 (es) | 1994-01-01 |
PT92016B (pt) | 1995-06-30 |
CN1023802C (zh) | 1994-02-16 |
HU895337D0 (en) | 1990-01-28 |
AU4296889A (en) | 1990-05-10 |
PT92016A (pt) | 1990-04-30 |
DE68909166D1 (de) | 1993-10-21 |
IE63693B1 (en) | 1995-05-31 |
US4935530A (en) | 1990-06-19 |
EP0365256A1 (de) | 1990-04-25 |
NZ231026A (en) | 1991-05-28 |
IL91981A0 (en) | 1990-07-12 |
IE893335L (en) | 1990-04-18 |
CN1042154A (zh) | 1990-05-16 |
NO894133D0 (no) | 1989-10-17 |
ZA897768B (en) | 1990-07-25 |
NO172799C (no) | 1993-09-08 |
CA2000677A1 (en) | 1990-04-18 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8339 | Ceased/non-payment of the annual fee |