DE60214937D1 - Verfahren zur Herstellung eines polymerdispergierten Polyols - Google Patents

Verfahren zur Herstellung eines polymerdispergierten Polyols

Info

Publication number
DE60214937D1
DE60214937D1 DE60214937T DE60214937T DE60214937D1 DE 60214937 D1 DE60214937 D1 DE 60214937D1 DE 60214937 T DE60214937 T DE 60214937T DE 60214937 T DE60214937 T DE 60214937T DE 60214937 D1 DE60214937 D1 DE 60214937D1
Authority
DE
Germany
Prior art keywords
catalyst
ring
polyol
addition polymerization
polyoxyalkylene polyol
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60214937T
Other languages
English (en)
Other versions
DE60214937T2 (de
Inventor
Yoshinori Toyota
Akio Horie
Hiroshi Wada
Kayoko Sugiyama
Etsuko Akagi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AGC Inc
Original Assignee
Asahi Glass Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=26618943&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE60214937(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Asahi Glass Co Ltd filed Critical Asahi Glass Co Ltd
Publication of DE60214937D1 publication Critical patent/DE60214937D1/de
Application granted granted Critical
Publication of DE60214937T2 publication Critical patent/DE60214937T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0838—Manufacture of polymers in the presence of non-reactive compounds
    • C08G18/0842—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents
    • C08G18/0847—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of solvents for the polymers
    • C08G18/0852—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of solvents for the polymers the solvents being organic
    • C08G18/0857—Manufacture of polymers in the presence of non-reactive compounds in the presence of liquid diluents in the presence of solvents for the polymers the solvents being organic the solvent being a polyol
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
    • C08G18/4063—Mixtures of compounds of group C08G18/62 with other macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
    • C08G18/4072—Mixtures of compounds of group C08G18/63 with other macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4866—Polyethers having a low unsaturation value
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
    • C08G18/6552—Compounds of group C08G18/63
    • C08G18/6558—Compounds of group C08G18/63 with compounds of group C08G18/32 or polyamines of C08G18/38
    • C08G18/657—Compounds of group C08G18/63 with compounds of group C08G18/32 or polyamines of C08G18/38 with compounds of C08G18/3225 or C08G18/3271 or polyamines of C08G18/38
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7607—Compounds of C08G18/7614 and of C08G18/7657
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0008—Foam properties flexible
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0041—Foam properties having specified density
    • C08G2110/005—< 50kg/m3
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0083—Foam properties prepared using water as the sole blowing agent
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/06—Flexible foams

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Polyethers (AREA)
DE60214937T 2001-07-18 2002-07-17 Verfahren zur Herstellung eines polymerdispergierten Polyols Expired - Lifetime DE60214937T2 (de)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2001218348 2001-07-18
JP2001218348 2001-07-18
JP2002032839 2002-02-08
JP2002032839 2002-02-08

Publications (2)

Publication Number Publication Date
DE60214937D1 true DE60214937D1 (de) 2006-11-09
DE60214937T2 DE60214937T2 (de) 2007-05-24

Family

ID=26618943

Family Applications (2)

Application Number Title Priority Date Filing Date
DE60231259T Expired - Lifetime DE60231259D1 (de) 2001-07-18 2002-07-17 Verfahren zur Herstellung eines Polyols und eines polymerdispergierten Polyols
DE60214937T Expired - Lifetime DE60214937T2 (de) 2001-07-18 2002-07-17 Verfahren zur Herstellung eines polymerdispergierten Polyols

Family Applications Before (1)

Application Number Title Priority Date Filing Date
DE60231259T Expired - Lifetime DE60231259D1 (de) 2001-07-18 2002-07-17 Verfahren zur Herstellung eines Polyols und eines polymerdispergierten Polyols

Country Status (9)

Country Link
US (1) US6815467B2 (de)
EP (2) EP1277775B1 (de)
KR (1) KR100873594B1 (de)
CN (1) CN1257928C (de)
AT (1) ATE340812T1 (de)
AU (1) AU2002300142B2 (de)
CA (1) CA2393891A1 (de)
DE (2) DE60231259D1 (de)
TW (1) TWI242570B (de)

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EP1916271B1 (de) * 2001-12-21 2012-08-08 Asahi Glass Company, Limited Flexibler Polyurethanschaumstoff von geringer Beständigkeit und Herstellungsverfahren dafür
DE60318000T2 (de) * 2002-10-15 2008-04-03 Mitsubishi Gas Chemical Co., Inc. Kraftstoffsystem mit ausgezeichneten Dichtigkeitseigenschaften
US6884826B2 (en) * 2003-06-09 2005-04-26 Bayer Antwerp, N.V. Process for preparing double metal cyanide catalyzed polyols
CN100415794C (zh) * 2003-07-24 2008-09-03 旭硝子株式会社 聚氨酯树脂及其制造方法
KR101115276B1 (ko) * 2003-09-19 2012-03-05 아사히 가라스 가부시키가이샤 연질 폴리우레탄 폼 및 그 제조 방법
US7005552B2 (en) * 2003-11-03 2006-02-28 Bayer Materialscience Llc Single reactor synthesis of KOH-capped polyols based on DMC-synthesized intermediates
US20050101681A1 (en) * 2003-11-07 2005-05-12 Kaushiva Bryan D. Molded polyurethane foam with property enhancements for improved comfort and greater durability
DE102004047406A1 (de) 2004-09-28 2006-03-30 Basf Ag Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen
DE102004047524A1 (de) * 2004-09-28 2006-03-30 Basf Ag Verfahren zur Herstellung von Polyurethan-Weichschaumstoffen
WO2006054657A1 (ja) * 2004-11-18 2006-05-26 Asahi Glass Company, Limited 軟質ポリウレタンフォームの製造方法
EP1882711A1 (de) * 2005-05-16 2008-01-30 Asahi Glass Company, Limited Härtbare zusammensetzung
CN101180336B (zh) * 2005-05-25 2011-07-20 旭硝子株式会社 软质聚氨酯泡沫塑料及其制造方法、利用该软质聚氨酯泡沫塑料的汽车用座垫
WO2007018129A1 (ja) * 2005-08-05 2007-02-15 Asahi Glass Company, Limited 軟質ポリウレタンフォーム、その製造方法および自動車用シート
KR20090068216A (ko) * 2006-09-27 2009-06-25 아사히 가라스 가부시키가이샤 연질 폴리우레탄폼의 제조 방법
DK2077287T3 (da) * 2006-10-25 2013-07-22 Asahi Glass Co Ltd Fremgangsmåde til fremstilling af blødt polyurethanskum
US20080234458A1 (en) * 2007-03-20 2008-09-25 West Richard A Polyol and method of making polyol using soy-based powder
EP2161289A4 (de) * 2007-06-22 2010-07-07 Asahi Glass Co Ltd Verfahren zur herstellung von polymer-dispergiertem polyol und verfahren zur herstellung von flexiblem polyurethanschaumstoff
JP5303885B2 (ja) 2007-09-18 2013-10-02 旭硝子株式会社 軟質ポリウレタンフォームの製造方法および軟質ポリウレタンフォーム
KR100941637B1 (ko) * 2008-05-21 2010-02-11 에스케이씨 주식회사 반응성이 제어된, 폴리올 제조용 복금속 시안계 촉매 및이의 제조방법
EP2290002B1 (de) * 2008-06-16 2018-08-08 Sanyo Chemical Industries, Ltd. Polymerpolyol und verfahren zur herstellung von polyurethan
CN102369232B (zh) * 2009-03-30 2013-08-14 三洋化成工业株式会社 聚氧化烯多元醇或聚氧化烯一元醇以及聚氨酯树脂
US9068088B2 (en) * 2009-09-30 2015-06-30 Sealanttech Protective air barrier sealant for conditioned and unconditioned building walls
US20110077316A1 (en) * 2009-09-30 2011-03-31 Collins William Davis Biosealant Protective Barrier for Surfaces
KR20130060213A (ko) 2010-04-30 2013-06-07 바스프 에스이 폴리에테르 폴리올, 폴리에테르 폴리올의 제조 방법, 및 폴리우레탄 제조를 위한 그의 용도
KR20130094688A (ko) * 2010-04-30 2013-08-26 아사히 가라스 가부시키가이샤 폴리옥시알킬렌폴리올, 폴리머 분산 폴리올, 및 연질 폴리우레탄폼, 그리고 이들의 제조 방법
US9115246B2 (en) 2010-04-30 2015-08-25 Basf Se Polyether polyols, process for preparing polyether polyols and their use for producing polyurethanes
CN101967226B (zh) * 2010-09-28 2013-09-11 山东蓝星东大化工有限责任公司 高活性高分子量聚醚多元醇的合成方法
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Also Published As

Publication number Publication date
EP1632513B2 (de) 2012-09-05
CN1400231A (zh) 2003-03-05
AU2002300142B2 (en) 2007-03-22
CA2393891A1 (en) 2003-01-18
EP1277775A1 (de) 2003-01-22
KR100873594B1 (ko) 2008-12-11
DE60214937T2 (de) 2007-05-24
ATE340812T1 (de) 2006-10-15
EP1277775B1 (de) 2006-09-27
EP1632513A1 (de) 2006-03-08
CN1257928C (zh) 2006-05-31
KR20030009171A (ko) 2003-01-29
EP1632513B1 (de) 2009-02-18
TWI242570B (en) 2005-11-01
DE60231259D1 (de) 2009-04-02
US6815467B2 (en) 2004-11-09
US20030100801A1 (en) 2003-05-29

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