DE60119816D1 - Moduliertes Differentialabtastkalorimeter - Google Patents

Moduliertes Differentialabtastkalorimeter

Info

Publication number
DE60119816D1
DE60119816D1 DE60119816T DE60119816T DE60119816D1 DE 60119816 D1 DE60119816 D1 DE 60119816D1 DE 60119816 T DE60119816 T DE 60119816T DE 60119816 T DE60119816 T DE 60119816T DE 60119816 D1 DE60119816 D1 DE 60119816D1
Authority
DE
Germany
Prior art keywords
differential scanning
scanning calorimeter
modulated differential
modulated
calorimeter
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60119816T
Other languages
English (en)
Other versions
DE60119816T2 (de
Inventor
Robert L Danley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TA Instruments Inc
Original Assignee
TA Instruments Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US09/643,870 external-priority patent/US6431747B1/en
Priority claimed from US09/643,869 external-priority patent/US6428203B1/en
Application filed by TA Instruments Inc filed Critical TA Instruments Inc
Application granted granted Critical
Publication of DE60119816D1 publication Critical patent/DE60119816D1/de
Publication of DE60119816T2 publication Critical patent/DE60119816T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K17/00Measuring quantity of heat
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01KMEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
    • G01K17/00Measuring quantity of heat
    • G01K17/04Calorimeters using compensation methods, i.e. where the absorbed or released quantity of heat to be measured is compensated by a measured quantity of heating or cooling
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
    • G01N25/48Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
    • G01N25/4806Details not adapted to a particular type of sample
    • G01N25/4826Details not adapted to a particular type of sample concerning the heating or cooling arrangements
    • G01N25/4833Details not adapted to a particular type of sample concerning the heating or cooling arrangements specially adapted for temperature scanning
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means
    • G01N25/20Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
    • G01N25/48Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
    • G01N25/4846Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample
    • G01N25/4866Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample by using a differential method

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)
DE60119816T 2000-03-23 2001-03-20 Moduliertes Differentialabtastkalorimeter Expired - Lifetime DE60119816T2 (de)

Applications Claiming Priority (8)

Application Number Priority Date Filing Date Title
US53394900A 2000-03-23 2000-03-23
US533949 2000-03-23
US09/643,870 US6431747B1 (en) 2000-03-23 2000-08-23 Heat flux differential scanning calorimeter sensor
US643870 2000-08-23
US643869 2000-08-23
US09/643,869 US6428203B1 (en) 2000-03-23 2000-08-23 Power compensation differential scanning calorimeter
US769313 2001-01-26
US09/769,313 US6561692B2 (en) 2000-03-23 2001-01-26 Differential scanning calorimeter

Publications (2)

Publication Number Publication Date
DE60119816D1 true DE60119816D1 (de) 2006-06-29
DE60119816T2 DE60119816T2 (de) 2006-11-02

Family

ID=27504646

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60119816T Expired - Lifetime DE60119816T2 (de) 2000-03-23 2001-03-20 Moduliertes Differentialabtastkalorimeter

Country Status (4)

Country Link
US (1) US6561692B2 (de)
EP (3) EP1136803A1 (de)
JP (3) JP3936847B2 (de)
DE (1) DE60119816T2 (de)

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ATE521886T1 (de) * 2002-06-10 2011-09-15 Mettler Toledo Ag Verfahren und vorrichtung für die thermische analyse eines materials
FR2856794B1 (fr) * 2003-06-25 2006-05-05 Setaram Soc Et D Automatisatio Cellule de mesure pour un calorimetre a compensation de puissance et dispositif comportant deux telles cellules
US6860632B2 (en) * 2003-07-28 2005-03-01 Perkinelmer Instruments Llc Instrument material holder and method of fabrication thereof
KR100814414B1 (ko) * 2003-09-01 2008-03-18 학교법인 포항공과대학교 발열량 측정장치 및 방법
US7371006B2 (en) * 2004-02-10 2008-05-13 Perkinelmer Las, Inc. Differential scanning calorimeter (DSC) with temperature controlled furnace
US7447607B2 (en) * 2004-08-31 2008-11-04 Watow Electric Manufacturing System and method of compensation for device mounting and thermal transfer error
US20080273572A1 (en) * 2006-06-02 2008-11-06 James Madison University Thermal detector for chemical or biological agents
US7470057B2 (en) * 2006-08-24 2008-12-30 Waters Investments Limited Differential scanning calorimeter sensor and method
US7578613B2 (en) * 2006-09-14 2009-08-25 Waters Investments Limited Modulated differential scanning calorimeter solvent loss calibration apparatus and method
US8087821B2 (en) * 2007-06-06 2012-01-03 Waters Technologies Corporation Infrared heated differential scanning calorimeter
GB2462954B (en) 2007-06-06 2011-08-17 Waters Investments Ltd System and method for thermal analysis using variable thermal resistance
DE102007057260A1 (de) 2007-11-26 2009-06-04 Stephan Reiß, Michael Conrad GbR (vertretungsberechtigter Gesellschafter: Stephan Reiß, 13125 Berlin Verfahren und Anordnung zur Bestimmung der optischen Abbildungsqualität von Gleitsichtgläsern
FR2925163B1 (fr) * 2007-12-12 2010-02-26 Centre Nat Rech Scient Procede et appareil d'analyse thermique
US8147133B2 (en) * 2009-05-26 2012-04-03 The United States Of America As Represented By The Secretary Of The Navy Top loaded twin cell calorimeter system with removable reference
US8012770B2 (en) 2009-07-31 2011-09-06 Invisible Sentinel, Inc. Device for detection of antigens and uses thereof
JP2013511702A (ja) * 2009-11-20 2013-04-04 ネッシー ガーテゥボー ゲーエムベーハー 熱分析システムおよび熱分析方法
JP5642525B2 (ja) * 2010-02-02 2014-12-17 株式会社日立ハイテクサイエンス 示差走査熱量計
CN101769705B (zh) * 2010-02-10 2012-06-06 云南省计量测试技术研究院 一种检定或校准数显测高仪示值误差的量块直立等温测量方法
RU2475714C2 (ru) * 2010-09-22 2013-02-20 Общество с ограниченной ответственностью "Техноаналит" Дифференциальный микрокалориметр и способ измерения тепловыделения
WO2014018688A2 (en) * 2012-07-24 2014-01-30 The Trustees Of Columbia University In The City Of New York Mems-based isothermal titration calorimetry
US9513240B2 (en) * 2011-02-22 2016-12-06 The Trustees Of Columbia University In The City Of New York MEMS-based calorimeter, fabrication, and use thereof
EP2678651B1 (de) * 2011-02-22 2017-08-23 The Trustees of Columbia University in the City of New York Mems-basiertes kalorienmessgerät
JP6190395B2 (ja) 2012-03-09 2017-08-30 インビジブル・センチネル,インコーポレーテッド 単一信号で複数被検体を検出する方法及び組成物
WO2014039376A2 (en) * 2012-09-04 2014-03-13 Waters Technologies Corporation Quasiadiabatic differential scanning calorimeter
JP2016524713A (ja) 2013-06-05 2016-08-18 ザ トラスティーズ オブ コロンビア ユニバーシティ イン ザ シティ オブ ニューヨーク Mems式熱量計、その製造および使用
CN103575427B (zh) * 2013-09-24 2016-01-13 中国科学院力学研究所 一种采用导热标定热流计的方法
US8851744B1 (en) * 2013-10-02 2014-10-07 Onicon, Inc. Calibration apparatus and method for heat transfer measurement
CN104180929B (zh) * 2014-08-06 2016-08-17 山东省计算中心(国家超级计算济南中心) 一种热阻式热流传感器的校准方法
CN104155005B (zh) * 2014-08-21 2017-02-15 中国航空工业集团公司北京长城计量测试技术研究所 一种比较法辐射热流计校准装置
WO2016065361A2 (en) 2014-10-24 2016-04-28 The Trustees Of Columbia University In The City Of New York Mems-based calorimeter, fabrication, and use thereof
CN104391005B (zh) * 2014-11-28 2017-01-18 西安近代化学研究所 一种高机械感度含能材料溶解热的测量装置及方法
CN105372289B (zh) * 2015-11-21 2018-06-08 中国人民解放军第二炮兵工程大学 一种含能材料表观比热容的测量修正方法
CN106706700A (zh) * 2016-11-11 2017-05-24 四川天策聚材科技有限公司 导电高分子复合材料相变‑电阻关系在线监测系统及方法
CN107300430B (zh) * 2017-07-18 2023-06-16 甘肃蓝科石化高新装备股份有限公司 一种真空绝热低温管漏热量测量装置及其测量方法
RU2655459C1 (ru) * 2017-08-22 2018-05-28 Антон Владимирович Шмаков Способ измерения теплоемкости материалов
RU2654823C1 (ru) * 2017-08-22 2018-05-22 Антон Владимирович Шмаков Способ измерения теплопроводности твердых материалов
RU2654824C1 (ru) * 2017-08-22 2018-05-22 Антон Владимирович Шмаков Устройство для измерения теплоемкости материалов
RU2654826C1 (ru) * 2017-08-22 2018-05-22 Антон Владимирович Шмаков Устройство для измерения теплопроводности твердых материалов
US11204289B2 (en) 2018-08-23 2021-12-21 Waters Technologies Corporation Multiple sample differential scanning calorimeter
JP6976991B2 (ja) * 2019-06-06 2021-12-08 Nissha株式会社 2成分ガスの濃度比算出方法および検知対象ガスの濃度算出方法
JP6792040B1 (ja) * 2019-09-25 2020-11-25 ネッチ ゲレーテバウ ゲーエムベーハー 熱分析装置、試料ホルダ組立体及び熱分析方法
CN111024270B (zh) * 2019-12-11 2020-11-17 浙江大学 一种嵌入式热流传感器测量误差的修正方法
EP4078161A1 (de) * 2019-12-20 2022-10-26 TA Instruments-Waters LLC Wärmeflussratenbestimmung für ein einzelproben-differenz-kalorimeter
WO2021220395A1 (ja) * 2020-04-28 2021-11-04 日本電信電話株式会社 温度測定装置および温度測定方法
CN113109391B (zh) * 2021-05-21 2022-03-04 中国计量大学 一种基于补偿功率调制的绝热反应动态比热容测定方法
EP4350312A1 (de) * 2022-10-04 2024-04-10 Mettler-Toledo GmbH Kalibrierungsverfahren für ein differentialscanning-kalorimeter

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Also Published As

Publication number Publication date
EP1136802A1 (de) 2001-09-26
JP3936846B2 (ja) 2007-06-27
US20030072348A1 (en) 2003-04-17
EP1139083B1 (de) 2016-05-11
JP4074441B2 (ja) 2008-04-09
EP1136802B1 (de) 2006-05-24
US6561692B2 (en) 2003-05-13
EP1139083A1 (de) 2001-10-04
DE60119816T2 (de) 2006-11-02
JP2001330575A (ja) 2001-11-30
JP2001349855A (ja) 2001-12-21
JP2001349856A (ja) 2001-12-21
JP3936847B2 (ja) 2007-06-27
EP1136803A1 (de) 2001-09-26

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