DE60119816D1 - Moduliertes Differentialabtastkalorimeter - Google Patents
Moduliertes DifferentialabtastkalorimeterInfo
- Publication number
- DE60119816D1 DE60119816D1 DE60119816T DE60119816T DE60119816D1 DE 60119816 D1 DE60119816 D1 DE 60119816D1 DE 60119816 T DE60119816 T DE 60119816T DE 60119816 T DE60119816 T DE 60119816T DE 60119816 D1 DE60119816 D1 DE 60119816D1
- Authority
- DE
- Germany
- Prior art keywords
- differential scanning
- scanning calorimeter
- modulated differential
- modulated
- calorimeter
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K17/00—Measuring quantity of heat
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01K—MEASURING TEMPERATURE; MEASURING QUANTITY OF HEAT; THERMALLY-SENSITIVE ELEMENTS NOT OTHERWISE PROVIDED FOR
- G01K17/00—Measuring quantity of heat
- G01K17/04—Calorimeters using compensation methods, i.e. where the absorbed or released quantity of heat to be measured is compensated by a measured quantity of heating or cooling
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4806—Details not adapted to a particular type of sample
- G01N25/4826—Details not adapted to a particular type of sample concerning the heating or cooling arrangements
- G01N25/4833—Details not adapted to a particular type of sample concerning the heating or cooling arrangements specially adapted for temperature scanning
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N25/00—Investigating or analyzing materials by the use of thermal means
- G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
- G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation
- G01N25/4846—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample
- G01N25/4866—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation for a motionless, e.g. solid sample by using a differential method
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Combustion & Propulsion (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Or Analyzing Materials Using Thermal Means (AREA)
Applications Claiming Priority (8)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US53394900A | 2000-03-23 | 2000-03-23 | |
US533949 | 2000-03-23 | ||
US09/643,870 US6431747B1 (en) | 2000-03-23 | 2000-08-23 | Heat flux differential scanning calorimeter sensor |
US643870 | 2000-08-23 | ||
US643869 | 2000-08-23 | ||
US09/643,869 US6428203B1 (en) | 2000-03-23 | 2000-08-23 | Power compensation differential scanning calorimeter |
US769313 | 2001-01-26 | ||
US09/769,313 US6561692B2 (en) | 2000-03-23 | 2001-01-26 | Differential scanning calorimeter |
Publications (2)
Publication Number | Publication Date |
---|---|
DE60119816D1 true DE60119816D1 (de) | 2006-06-29 |
DE60119816T2 DE60119816T2 (de) | 2006-11-02 |
Family
ID=27504646
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE60119816T Expired - Lifetime DE60119816T2 (de) | 2000-03-23 | 2001-03-20 | Moduliertes Differentialabtastkalorimeter |
Country Status (4)
Country | Link |
---|---|
US (1) | US6561692B2 (de) |
EP (3) | EP1136803A1 (de) |
JP (3) | JP3936847B2 (de) |
DE (1) | DE60119816T2 (de) |
Families Citing this family (48)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6843595B2 (en) | 2001-01-26 | 2005-01-18 | Waters Investment Limited | Differential scanning calorimeter accounting for heat leakage |
US6648504B2 (en) * | 2002-03-01 | 2003-11-18 | Waters Investment Limited | System and method for calibrating contact thermal resistances in differential scanning calorimeters |
ATE521886T1 (de) * | 2002-06-10 | 2011-09-15 | Mettler Toledo Ag | Verfahren und vorrichtung für die thermische analyse eines materials |
FR2856794B1 (fr) * | 2003-06-25 | 2006-05-05 | Setaram Soc Et D Automatisatio | Cellule de mesure pour un calorimetre a compensation de puissance et dispositif comportant deux telles cellules |
US6860632B2 (en) * | 2003-07-28 | 2005-03-01 | Perkinelmer Instruments Llc | Instrument material holder and method of fabrication thereof |
KR100814414B1 (ko) * | 2003-09-01 | 2008-03-18 | 학교법인 포항공과대학교 | 발열량 측정장치 및 방법 |
US7371006B2 (en) * | 2004-02-10 | 2008-05-13 | Perkinelmer Las, Inc. | Differential scanning calorimeter (DSC) with temperature controlled furnace |
US7447607B2 (en) * | 2004-08-31 | 2008-11-04 | Watow Electric Manufacturing | System and method of compensation for device mounting and thermal transfer error |
US20080273572A1 (en) * | 2006-06-02 | 2008-11-06 | James Madison University | Thermal detector for chemical or biological agents |
US7470057B2 (en) * | 2006-08-24 | 2008-12-30 | Waters Investments Limited | Differential scanning calorimeter sensor and method |
US7578613B2 (en) * | 2006-09-14 | 2009-08-25 | Waters Investments Limited | Modulated differential scanning calorimeter solvent loss calibration apparatus and method |
US8087821B2 (en) * | 2007-06-06 | 2012-01-03 | Waters Technologies Corporation | Infrared heated differential scanning calorimeter |
GB2462954B (en) | 2007-06-06 | 2011-08-17 | Waters Investments Ltd | System and method for thermal analysis using variable thermal resistance |
DE102007057260A1 (de) | 2007-11-26 | 2009-06-04 | Stephan Reiß, Michael Conrad GbR (vertretungsberechtigter Gesellschafter: Stephan Reiß, 13125 Berlin | Verfahren und Anordnung zur Bestimmung der optischen Abbildungsqualität von Gleitsichtgläsern |
FR2925163B1 (fr) * | 2007-12-12 | 2010-02-26 | Centre Nat Rech Scient | Procede et appareil d'analyse thermique |
US8147133B2 (en) * | 2009-05-26 | 2012-04-03 | The United States Of America As Represented By The Secretary Of The Navy | Top loaded twin cell calorimeter system with removable reference |
US8012770B2 (en) | 2009-07-31 | 2011-09-06 | Invisible Sentinel, Inc. | Device for detection of antigens and uses thereof |
JP2013511702A (ja) * | 2009-11-20 | 2013-04-04 | ネッシー ガーテゥボー ゲーエムベーハー | 熱分析システムおよび熱分析方法 |
JP5642525B2 (ja) * | 2010-02-02 | 2014-12-17 | 株式会社日立ハイテクサイエンス | 示差走査熱量計 |
CN101769705B (zh) * | 2010-02-10 | 2012-06-06 | 云南省计量测试技术研究院 | 一种检定或校准数显测高仪示值误差的量块直立等温测量方法 |
RU2475714C2 (ru) * | 2010-09-22 | 2013-02-20 | Общество с ограниченной ответственностью "Техноаналит" | Дифференциальный микрокалориметр и способ измерения тепловыделения |
WO2014018688A2 (en) * | 2012-07-24 | 2014-01-30 | The Trustees Of Columbia University In The City Of New York | Mems-based isothermal titration calorimetry |
US9513240B2 (en) * | 2011-02-22 | 2016-12-06 | The Trustees Of Columbia University In The City Of New York | MEMS-based calorimeter, fabrication, and use thereof |
EP2678651B1 (de) * | 2011-02-22 | 2017-08-23 | The Trustees of Columbia University in the City of New York | Mems-basiertes kalorienmessgerät |
JP6190395B2 (ja) | 2012-03-09 | 2017-08-30 | インビジブル・センチネル,インコーポレーテッド | 単一信号で複数被検体を検出する方法及び組成物 |
WO2014039376A2 (en) * | 2012-09-04 | 2014-03-13 | Waters Technologies Corporation | Quasiadiabatic differential scanning calorimeter |
JP2016524713A (ja) | 2013-06-05 | 2016-08-18 | ザ トラスティーズ オブ コロンビア ユニバーシティ イン ザ シティ オブ ニューヨーク | Mems式熱量計、その製造および使用 |
CN103575427B (zh) * | 2013-09-24 | 2016-01-13 | 中国科学院力学研究所 | 一种采用导热标定热流计的方法 |
US8851744B1 (en) * | 2013-10-02 | 2014-10-07 | Onicon, Inc. | Calibration apparatus and method for heat transfer measurement |
CN104180929B (zh) * | 2014-08-06 | 2016-08-17 | 山东省计算中心(国家超级计算济南中心) | 一种热阻式热流传感器的校准方法 |
CN104155005B (zh) * | 2014-08-21 | 2017-02-15 | 中国航空工业集团公司北京长城计量测试技术研究所 | 一种比较法辐射热流计校准装置 |
WO2016065361A2 (en) | 2014-10-24 | 2016-04-28 | The Trustees Of Columbia University In The City Of New York | Mems-based calorimeter, fabrication, and use thereof |
CN104391005B (zh) * | 2014-11-28 | 2017-01-18 | 西安近代化学研究所 | 一种高机械感度含能材料溶解热的测量装置及方法 |
CN105372289B (zh) * | 2015-11-21 | 2018-06-08 | 中国人民解放军第二炮兵工程大学 | 一种含能材料表观比热容的测量修正方法 |
CN106706700A (zh) * | 2016-11-11 | 2017-05-24 | 四川天策聚材科技有限公司 | 导电高分子复合材料相变‑电阻关系在线监测系统及方法 |
CN107300430B (zh) * | 2017-07-18 | 2023-06-16 | 甘肃蓝科石化高新装备股份有限公司 | 一种真空绝热低温管漏热量测量装置及其测量方法 |
RU2655459C1 (ru) * | 2017-08-22 | 2018-05-28 | Антон Владимирович Шмаков | Способ измерения теплоемкости материалов |
RU2654823C1 (ru) * | 2017-08-22 | 2018-05-22 | Антон Владимирович Шмаков | Способ измерения теплопроводности твердых материалов |
RU2654824C1 (ru) * | 2017-08-22 | 2018-05-22 | Антон Владимирович Шмаков | Устройство для измерения теплоемкости материалов |
RU2654826C1 (ru) * | 2017-08-22 | 2018-05-22 | Антон Владимирович Шмаков | Устройство для измерения теплопроводности твердых материалов |
US11204289B2 (en) | 2018-08-23 | 2021-12-21 | Waters Technologies Corporation | Multiple sample differential scanning calorimeter |
JP6976991B2 (ja) * | 2019-06-06 | 2021-12-08 | Nissha株式会社 | 2成分ガスの濃度比算出方法および検知対象ガスの濃度算出方法 |
JP6792040B1 (ja) * | 2019-09-25 | 2020-11-25 | ネッチ ゲレーテバウ ゲーエムベーハー | 熱分析装置、試料ホルダ組立体及び熱分析方法 |
CN111024270B (zh) * | 2019-12-11 | 2020-11-17 | 浙江大学 | 一种嵌入式热流传感器测量误差的修正方法 |
EP4078161A1 (de) * | 2019-12-20 | 2022-10-26 | TA Instruments-Waters LLC | Wärmeflussratenbestimmung für ein einzelproben-differenz-kalorimeter |
WO2021220395A1 (ja) * | 2020-04-28 | 2021-11-04 | 日本電信電話株式会社 | 温度測定装置および温度測定方法 |
CN113109391B (zh) * | 2021-05-21 | 2022-03-04 | 中国计量大学 | 一种基于补偿功率调制的绝热反应动态比热容测定方法 |
EP4350312A1 (de) * | 2022-10-04 | 2024-04-10 | Mettler-Toledo GmbH | Kalibrierungsverfahren für ein differentialscanning-kalorimeter |
Family Cites Families (25)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3263484A (en) | 1962-04-04 | 1966-08-02 | Perkin Elmer Corp | Differential microcalorimeter |
US3732722A (en) | 1971-08-20 | 1973-05-15 | Perkin Elmer Corp | Material holder |
US4095453A (en) | 1977-02-25 | 1978-06-20 | E. I. Du Pont De Nemours And Company | Differential thermal analysis cell |
US4350466A (en) | 1980-05-08 | 1982-09-21 | Mgs Machine Corporation | Apparatus for handling articles |
US4330933A (en) | 1980-07-28 | 1982-05-25 | The Perkin-Elmer Corporation | Fabrication method for instrument material holder |
DE3049105A1 (de) | 1980-12-24 | 1982-07-15 | Bayer Ag, 5090 Leverkusen | Reaktorkalorimeter zur bestimmung thermokinetischer daten |
US4530608A (en) | 1984-05-14 | 1985-07-23 | The Perkin-Elmer Corp. | Baseline control for a differential scanning calorimeter |
US4614721A (en) | 1984-12-10 | 1986-09-30 | Rocwell | Heat recovery calorimeter |
HU194405B (en) | 1985-05-10 | 1988-01-28 | Magyar Optikai Muevek | Temperature control system for testing thermic phase transformations |
DE3529489A1 (de) | 1985-08-16 | 1987-02-26 | Max Planck Gesellschaft | Verfahren und einrichtung zum bestimmen der waermekapazitaet einer probe |
CH678579A5 (de) | 1989-04-24 | 1991-09-30 | Mettler Toledo Ag | |
US5224775C2 (en) | 1992-03-02 | 2002-04-23 | Ta Instr Inc | Method and apparatus for modulated differential analysis |
US5474385A (en) | 1992-03-02 | 1995-12-12 | Ta Instruments, Inc. | Method and apparatus for parsed dynamic differential analysis |
US5211477A (en) | 1992-05-29 | 1993-05-18 | Ford Motor Company | Method and apparatus for simultaneous differential scanning calorimetry and microdielectrometry |
US5288147A (en) | 1992-11-09 | 1994-02-22 | Ta Instruments, Inc. | Thermopile differential thermal analysis sensor |
JP2909950B2 (ja) | 1993-09-24 | 1999-06-23 | セイコーインスツルメンツ株式会社 | 熱分析装置 |
US5549387A (en) | 1994-06-01 | 1996-08-27 | The Perkin-Elmer Corporation | Apparatus and method for differential analysis using real and imaginary signal components |
WO1995033199A1 (en) | 1994-06-01 | 1995-12-07 | Perkin-Elmer Corporation | Apparatus and method for differential analysis using real and imaginary signal components |
US5672289A (en) | 1996-01-11 | 1997-09-30 | The Perkin-Elmer Corporation | Heater control circuit |
US5813763A (en) | 1996-10-11 | 1998-09-29 | Microcal Incorporated | Ultrasensitive differential microcalorimeter |
EP0883801B1 (de) | 1996-11-01 | 2004-09-15 | TA Instruments, Inc. | Differentialabtastkalorimeter |
US6200022B1 (en) | 1997-04-21 | 2001-03-13 | Ta Instruments, Inc. | Method and apparatus for localized dynamic mechano-thermal analysis with scanning probe microscopy |
US6079873A (en) | 1997-10-20 | 2000-06-27 | The United States Of America As Represented By The Secretary Of Commerce | Micron-scale differential scanning calorimeter on a chip |
JP3370592B2 (ja) | 1998-01-19 | 2003-01-27 | セイコーインスツルメンツ株式会社 | 示差熱分析装置 |
JP3137605B2 (ja) | 1998-07-14 | 2001-02-26 | セイコーインスツルメンツ株式会社 | 熱流束型示差走査熱量計 |
-
2001
- 2001-01-26 US US09/769,313 patent/US6561692B2/en not_active Expired - Lifetime
- 2001-03-14 EP EP01106270A patent/EP1136803A1/de not_active Withdrawn
- 2001-03-16 JP JP2001076965A patent/JP3936847B2/ja not_active Expired - Lifetime
- 2001-03-16 JP JP2001076887A patent/JP3936846B2/ja not_active Expired - Lifetime
- 2001-03-16 JP JP2001076792A patent/JP4074441B2/ja not_active Expired - Lifetime
- 2001-03-20 DE DE60119816T patent/DE60119816T2/de not_active Expired - Lifetime
- 2001-03-20 EP EP01106939A patent/EP1136802B1/de not_active Expired - Lifetime
- 2001-03-23 EP EP01107288.1A patent/EP1139083B1/de not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
EP1136802A1 (de) | 2001-09-26 |
JP3936846B2 (ja) | 2007-06-27 |
US20030072348A1 (en) | 2003-04-17 |
EP1139083B1 (de) | 2016-05-11 |
JP4074441B2 (ja) | 2008-04-09 |
EP1136802B1 (de) | 2006-05-24 |
US6561692B2 (en) | 2003-05-13 |
EP1139083A1 (de) | 2001-10-04 |
DE60119816T2 (de) | 2006-11-02 |
JP2001330575A (ja) | 2001-11-30 |
JP2001349855A (ja) | 2001-12-21 |
JP2001349856A (ja) | 2001-12-21 |
JP3936847B2 (ja) | 2007-06-27 |
EP1136803A1 (de) | 2001-09-26 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition |