DE60115934D1 - Verfahren zur herstellung von polyamiden - Google Patents

Verfahren zur herstellung von polyamiden

Info

Publication number
DE60115934D1
DE60115934D1 DE60115934T DE60115934T DE60115934D1 DE 60115934 D1 DE60115934 D1 DE 60115934D1 DE 60115934 T DE60115934 T DE 60115934T DE 60115934 T DE60115934 T DE 60115934T DE 60115934 D1 DE60115934 D1 DE 60115934D1
Authority
DE
Germany
Prior art keywords
polyamides
rich
compound
mixture
end groups
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60115934T
Other languages
English (en)
Other versions
DE60115934T2 (de
Inventor
Jean-Francois Thierry
Matthieu Helft
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rhodia Polyamide Intermediates SAS
Original Assignee
Rhodia Polyamide Intermediates SAS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Polyamide Intermediates SAS filed Critical Rhodia Polyamide Intermediates SAS
Publication of DE60115934D1 publication Critical patent/DE60115934D1/de
Application granted granted Critical
Publication of DE60115934T2 publication Critical patent/DE60115934T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
    • C08G69/28—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1856—Stationary reactors having moving elements inside placed in parallel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
    • C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
    • C08G69/04—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/00033—Continuous processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00027—Process aspects
    • B01J2219/0004—Processes in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B01J2219/00063—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00081—Tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094—Jackets
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00177—Controlling or regulating processes controlling the pH
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00182—Controlling or regulating processes controlling the level of reactants in the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00186—Controlling or regulating processes controlling the composition of the reactive mixture

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyamides (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Artificial Filaments (AREA)
DE60115934T 2000-10-04 2001-10-03 Verfahren zur herstellung von polyamiden Expired - Lifetime DE60115934T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR0012678A FR2814747B1 (fr) 2000-10-04 2000-10-04 Procede de fabrication de polyamides
FR0012678 2000-10-04
PCT/FR2001/003045 WO2002028942A1 (fr) 2000-10-04 2001-10-03 Procede de fabrication de polyamides

Publications (2)

Publication Number Publication Date
DE60115934D1 true DE60115934D1 (de) 2006-01-19
DE60115934T2 DE60115934T2 (de) 2006-07-27

Family

ID=8854994

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60115934T Expired - Lifetime DE60115934T2 (de) 2000-10-04 2001-10-03 Verfahren zur herstellung von polyamiden

Country Status (21)

Country Link
US (1) US6995233B2 (de)
EP (1) EP1325057B1 (de)
JP (1) JP3887310B2 (de)
KR (1) KR100580350B1 (de)
CN (1) CN1197897C (de)
AT (1) ATE312865T1 (de)
AU (1) AU2001293947A1 (de)
BR (1) BR0114522B1 (de)
CA (1) CA2424985C (de)
DE (1) DE60115934T2 (de)
ES (1) ES2250482T3 (de)
FR (1) FR2814747B1 (de)
HU (1) HUP0303365A3 (de)
IL (1) IL155232A (de)
MX (1) MX237616B (de)
PL (1) PL210249B1 (de)
RU (1) RU2247130C2 (de)
SK (1) SK4192003A3 (de)
TW (1) TWI265941B (de)
UA (1) UA74846C2 (de)
WO (1) WO2002028942A1 (de)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2914308B1 (fr) * 2007-03-27 2009-05-01 Rhodia Recherches & Tech Procede de fabrication de polyamide
US20140296472A1 (en) 2011-12-05 2014-10-02 Invista North America S.A R.L. Process for the preparation of polyamides
WO2013107425A1 (zh) * 2012-01-20 2013-07-25 北京伊克希德化工技术有限公司 尼龙66等以双组分单体为原料的尼龙连续聚合方法及设备
CN104130396B (zh) 2013-05-01 2018-05-29 英威达纺织（英国）有限公司 使用补充二胺的尼龙盐溶液制备方法
CN104130135B (zh) 2013-05-01 2018-07-03 英威达纺织（英国）有限公司 用于生产部分平衡酸溶液的方法
CN104130133B (zh) 2013-05-01 2018-01-19 英威达纺织（英国）有限公司 尼龙盐溶液制备方法中的前馈工序控制
TW201502163A (zh) * 2013-05-01 2015-01-16 Invista Tech Sarl 包含多重後段製程之聚醯胺合成
TW201512225A (zh) * 2013-05-01 2015-04-01 Invista Tech Sarl 將添加劑直接注入高壓釜中
TW201500405A (zh) 2013-05-01 2015-01-01 Invista Tech Sarl 用於尼龍鹽溶液製備方法的前饋及反饋程序控制
TW201444792A (zh) 2013-05-01 2014-12-01 Invista Tech Sarl 用於計量供製造尼龍鹽溶液之二羧酸粉末之方法
TW201443103A (zh) 2013-05-01 2014-11-16 Invista Tech Sarl 自部分平衡之酸性溶液製備尼龍鹽溶液的方法
TW201446728A (zh) 2013-05-01 2014-12-16 Invista Tech Sarl 用於尼龍鹽溶液製備方法之前饋程序控制及線上ｐｈ反饋
TW201446811A (zh) 2013-05-01 2014-12-16 Invista Tech Sarl 尼龍鹽溶液製備方法之前饋程序控制及ｐｈ反饋
WO2015055251A1 (en) * 2013-10-18 2015-04-23 Henkel Ag & Co. Kgaa Method for ageing the reaction mixture in a sulfonation process
CN104569025B (zh) * 2013-10-29 2017-01-04 中国石油化工股份有限公司 一种检测尼龙盐预聚温度的方法
CN104710317B (zh) 2013-12-17 2019-01-25 英威达纺织（英国）有限公司 用有分散头的容器生产pba溶液的尼龙盐溶液生产方法
US20170022300A1 (en) * 2013-12-20 2017-01-26 Horiba Stec, Co., Ltd. Continuous reaction apparatus and method of continuous polymerization using the same
RU2707291C2 (ru) * 2014-12-22 2019-11-26 Родиа Операсьон Катализаторы окисления циклоалканов и способ получения спиртов и кетонов
WO2017167692A1 (en) * 2016-04-01 2017-10-05 Solvay Specialty Polymers Usa, Llc (co)polyamides obtainable from 1,4-cyclohexanedicarboxylic acid and a diamine of formula h2n-(ch2)2-o-(ch2)2-o-(ch2)2-nh2
TWI787251B (zh) * 2017-04-13 2022-12-21 英商英威達紡織（英國）有限公司 製備用於聚醯胺化製程之前體之單體平衡控制
CN110914339B (zh) * 2017-08-01 2022-05-10 艾德凡斯化学公司 聚合聚酰胺的环状低聚物的方法
EP3556794A1 (de) * 2018-04-17 2019-10-23 SABIC Global Technologies B.V. Polykondensations-stöchiometrie-kontrolle
US20220144884A1 (en) * 2019-02-28 2022-05-12 Tokyo Institute Of Technology Method for producing amide
JPWO2021049266A1 (de) * 2019-09-12 2021-03-18
RU2767395C1 (ru) * 2020-09-11 2022-03-17 Акционерное общество "Государственный Ордена Трудового Красного Знамени научно-исследовательский институт химии и технологии элементоорганических соединений" (АО "ГНИИХТЭОС") Способ получения сополиамидов

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Publication number Priority date Publication date Assignee Title
JPH05222178A (ja) * 1992-02-14 1993-08-31 Fuji Photo Film Co Ltd 反応制御方法
US5403910A (en) * 1993-03-25 1995-04-04 E. I. Du Pont De Nemours & Company Low temperature nylon polymerization process
US5674974A (en) * 1994-11-23 1997-10-07 E. I. Du Pont De Nemours And Company Continuous polymerization process for polyamides
US5532487A (en) * 1994-11-23 1996-07-02 E. I. Du Pont De Nemours And Company Near-infrared measurement and control of polyamide processes
EP0984830B1 (de) * 1997-05-29 2002-12-04 E.I. Du Pont De Nemours And Company Prozessleituerfahren fürventilierte polymerisationsvorichtung
EP1080130B1 (de) * 1998-05-29 2004-10-13 Solutia Inc. Kontinuierliches verfahren zur polyamidherstellung
US6169162B1 (en) * 1999-05-24 2001-01-02 Solutia Inc. Continuous polyamidation process
FR2794760B1 (fr) * 1999-06-11 2001-08-17 Rhodianyl Procede de fabrication de polyamides
DE60119595T2 (de) * 2000-01-21 2006-09-14 Mitsubishi Gas Chemical Co., Inc. Verfahren zur Herstellung von Polyamid
JP2002194079A (ja) * 2000-12-22 2002-07-10 Mitsubishi Gas Chem Co Inc ポリアミドの製造方法

Also Published As

Publication number Publication date
JP3887310B2 (ja) 2007-02-28
ATE312865T1 (de) 2005-12-15
PL210249B1 (pl) 2011-12-30
HUP0303365A3 (en) 2004-03-01
RU2247130C2 (ru) 2005-02-27
FR2814747A1 (fr) 2002-04-05
TWI265941B (en) 2006-11-11
CN1197897C (zh) 2005-04-20
CA2424985C (fr) 2010-07-13
MX237616B (es) 2006-06-08
AU2001293947A1 (en) 2002-04-15
MXPA03003001A (es) 2004-12-06
US6995233B2 (en) 2006-02-07
EP1325057B1 (de) 2005-12-14
FR2814747B1 (fr) 2002-12-06
SK4192003A3 (en) 2003-09-11
HUP0303365A2 (hu) 2004-01-28
ES2250482T3 (es) 2006-04-16
EP1325057A1 (de) 2003-07-09
CA2424985A1 (fr) 2002-04-11
WO2002028942A1 (fr) 2002-04-11
JP2004519531A (ja) 2004-07-02
CN1474843A (zh) 2004-02-11
BR0114522A (pt) 2003-09-16
KR100580350B1 (ko) 2006-05-16
PL362557A1 (en) 2004-11-02
BR0114522B1 (pt) 2011-05-03
IL155232A (en) 2008-01-06
IL155232A0 (en) 2003-11-23
KR20030063355A (ko) 2003-07-28
DE60115934T2 (de) 2006-07-27
UA74846C2 (en) 2006-02-15
US20040019179A1 (en) 2004-01-29

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Legal Events

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8328 Change in the person/name/address of the agent

Representative=s name: PFENNING MEINIG & PARTNER GBR, 80339 MUENCHEN

8364 No opposition during term of opposition
8328 Change in the person/name/address of the agent

Representative=s name: MAIWALD PATENTANWALTSGESELLSCHAFT MBH, 80335 MUENC