DE60026794D1 - Verfahren zur katalytischen Gasphasenoxidation - Google Patents

Verfahren zur katalytischen Gasphasenoxidation

Info

Publication number
DE60026794D1
DE60026794D1 DE60026794T DE60026794T DE60026794D1 DE 60026794 D1 DE60026794 D1 DE 60026794D1 DE 60026794 T DE60026794 T DE 60026794T DE 60026794 T DE60026794 T DE 60026794T DE 60026794 D1 DE60026794 D1 DE 60026794D1
Authority
DE
Germany
Prior art keywords
gas phase
phase oxidation
catalytic gas
catalytic
oxidation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60026794T
Other languages
English (en)
Other versions
DE60026794T2 (de
Inventor
Takeshi Nishimura
Masakatsu Mori
Masatsugu Kitaura
Osamu Dodo
Daisuke Nakamura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nippon Shokubai Co Ltd
Original Assignee
Nippon Shokubai Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nippon Shokubai Co Ltd filed Critical Nippon Shokubai Co Ltd
Publication of DE60026794D1 publication Critical patent/DE60026794D1/de
Application granted granted Critical
Publication of DE60026794T2 publication Critical patent/DE60026794T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/008—Details of the reactor or of the particulate material; Processes to increase or to retard the rate of reaction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/27—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation
    • C07C45/32—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen
    • C07C45/33—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties
    • C07C45/34—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds
    • C07C45/35—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by oxidation with molecular oxygen of CHx-moieties in unsaturated compounds in propene or isobutene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
    • C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B01J2208/00221—Plates; Jackets; Cylinders comprising baffles for guiding the flow of the heat exchange medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE60026794T 1999-08-31 2000-08-24 Verfahren zur katalytischen Gasphasenoxidation Expired - Lifetime DE60026794T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP24605699 1999-08-31
JP24605699 1999-08-31

Publications (2)

Publication Number Publication Date
DE60026794D1 true DE60026794D1 (de) 2006-05-11
DE60026794T2 DE60026794T2 (de) 2007-01-18

Family

ID=17142819

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60026794T Expired - Lifetime DE60026794T2 (de) 1999-08-31 2000-08-24 Verfahren zur katalytischen Gasphasenoxidation

Country Status (8)

Country Link
US (1) US6613940B1 (de)
EP (1) EP1080781B1 (de)
KR (1) KR100457894B1 (de)
CN (1) CN1096878C (de)
BR (1) BR0003855A (de)
DE (1) DE60026794T2 (de)
MY (1) MY122598A (de)
ZA (1) ZA200004211B (de)

Families Citing this family (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4092090B2 (ja) * 2001-06-26 2008-05-28 株式会社日本触媒 固体粒子充填反応器およびその反応器を用いた接触気相酸化方法
BRPI0306797B1 (pt) 2002-01-11 2016-07-12 Mitsubishi Chem Corp reator multitubular, e, métodos de oxidação catalítica em fase vapor e para iniciar um reator tipo casco-tubo
RU2295383C2 (ru) * 2002-03-11 2007-03-20 Мицубиси Кемикал Корпорейшн Способ каталитического окисления в паровой фазе
JP4145607B2 (ja) * 2002-08-23 2008-09-03 三菱化学株式会社 多管式反応器を用いた気相接触酸化方法
KR100553825B1 (ko) 2003-09-01 2006-02-21 주식회사 엘지화학 고정층 촉매 부분 산화 반응기에서 개선된 제열 시스템을통한 불포화알데히드 및 불포화산의 제조 방법
JP2005330205A (ja) * 2004-05-19 2005-12-02 Mitsubishi Chemicals Corp （メタ）アクロレイン又は（メタ）アクリル酸の製造方法
JP4341591B2 (ja) * 2005-06-22 2009-10-07 住友化学株式会社 塩素製造用反応器および塩素の製造方法
KR100868454B1 (ko) * 2005-07-08 2008-11-11 주식회사 엘지화학 고정층 촉매 부분산화 반응기에서 고효율의 불포화산의제조방법
CN101233075B (zh) * 2005-09-30 2012-10-24 松下电器产业株式会社 氢生成装置及燃料电池系统
KR100866757B1 (ko) * 2006-02-24 2008-11-03 주식회사 엘지화학 반응기 및 열교환기 환상도관을 위한 열매체 분산기구
TWI322882B (en) 2006-02-24 2010-04-01 Lg Chemical Ltd Annular distributor having guide vane to improve flow rate distribution, reactor/heat exchanger including the annular distributor and method of producing unsaturated aldehyde or unsaturated acid from olefin by catalytic gas phase oxidation in the reactor
US20080008747A1 (en) * 2006-07-07 2008-01-10 Royds Robert B Transdermal patch
DE102007003076A1 (de) * 2007-01-16 2008-07-17 Basf Se Verfahren zur Herstellung einer das Element Eisen in oxidischer Form enthaltenden Multielementoxidmasse
EP2389241B1 (de) 2009-01-21 2018-06-06 Basf Se Rohrbündelreaktor und verfahren für unkatalysierte oder homogenkatalysierte reaktionen
EP2468394A1 (de) * 2010-12-23 2012-06-27 Shell Internationale Research Maatschappij B.V. Rohrbündelreaktor mit Katalysator und Verwendung
DE102011084476A1 (de) * 2011-10-13 2013-04-18 Man Diesel & Turbo Se Rohrbündelreaktor
JP6156860B2 (ja) 2012-04-04 2017-07-05 住友化学株式会社 多管式反応器および多管式反応器の設計方法
CN103706303A (zh) * 2013-12-12 2014-04-09 桂林华德机械设备有限公司 一种新型甲醛氧化器
DE102014103691A1 (de) 2014-03-18 2015-09-24 Basf Se Wärmetauscher, Reaktoranordnung umfassend diesen Wärmetauscher und Verfahren zum Temperieren eines Reaktors
CN107597056A (zh) * 2017-11-09 2018-01-19 曹恩康 一种放热反应用反应热可再利用的反应釜

Family Cites Families (10)

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Publication number Priority date Publication date Assignee Title
DE838598C (de) * 1948-10-02 1952-06-03 Metallgesellschaft Ag Verfahren und Vorrichtung zur Durchfuehrung exothermer katalytischer Reaktionen in Kontaktoefen
BE793928A (fr) * 1972-01-13 1973-05-02 Deggendorfer Werft Eisenbau Appareil pour la mise en oeuvre de processus chimiques exothermiques et endothermiques
US4203906A (en) * 1977-07-13 1980-05-20 Nippon Shokubai Kagaku Kogyo Co., Ltd. Process for catalytic vapor phase oxidation
DE2750824C2 (de) 1977-11-14 1979-08-09 Deggendorfer Werft Und Eisenbau Gmbh, 8360 Deggendorf Röhren-Reaktor zur Durchführung katalytischer Reaktionen
DE3409159A1 (de) 1984-03-13 1985-09-26 Deggendorfer Werft Und Eisenbau Gmbh, 8360 Deggendorf Rohrbuendel-reaktionsapparat
US5379391A (en) * 1991-03-01 1995-01-03 Storage Technology Corporation Method and apparatus to access data records in a cache memory by multiple virtual addresses
JP2778878B2 (ja) * 1991-09-12 1998-07-23 株式会社日本触媒 エチレンオキシドの製造方法
DE4431957A1 (de) 1994-09-08 1995-03-16 Basf Ag Verfahren zur katalytischen Gasphasenoxidation von Propen zu Acrolein
DE4431949A1 (de) * 1994-09-08 1995-03-16 Basf Ag Verfahren zur katalytischen Gasphasenoxidation von Acrolein zu Acrylsäure
JP3559456B2 (ja) * 1998-09-18 2004-09-02 株式会社日本触媒 接触気相酸化方法及び多管式反応器

Also Published As

Publication number Publication date
ZA200004211B (en) 2001-02-14
CN1096878C (zh) 2002-12-25
MY122598A (en) 2006-04-29
KR20010050268A (ko) 2001-06-15
CN1289635A (zh) 2001-04-04
KR100457894B1 (ko) 2004-11-18
EP1080781B1 (de) 2006-03-22
EP1080781A1 (de) 2001-03-07
US6613940B1 (en) 2003-09-02
DE60026794T2 (de) 2007-01-18
BR0003855A (pt) 2001-04-03

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