DE60019649D1 - Verfahren zur herstellung von 1,1,1,3,3-pentachlorpropan - Google Patents

Verfahren zur herstellung von 1,1,1,3,3-pentachlorpropan

Info

Publication number
DE60019649D1
DE60019649D1 DE60019649T DE60019649T DE60019649D1 DE 60019649 D1 DE60019649 D1 DE 60019649D1 DE 60019649 T DE60019649 T DE 60019649T DE 60019649 T DE60019649 T DE 60019649T DE 60019649 D1 DE60019649 D1 DE 60019649D1
Authority
DE
Germany
Prior art keywords
pentachloropropane
product mixture
reactor
iron metal
ferric chloride
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE60019649T
Other languages
English (en)
Other versions
DE60019649T2 (de
Inventor
Richard Wilson
Rodney Klausmeyer
Lloyd Branam
Derrek Burrows
Jim Strathe
John Dawkins
Lichtenstein, Iii
Joseph Weller
John Tummons
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Occidental Chemical Corp
Original Assignee
Vulcan Materials Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Vulcan Materials Co filed Critical Vulcan Materials Co
Publication of DE60019649D1 publication Critical patent/DE60019649D1/de
Application granted granted Critical
Publication of DE60019649T2 publication Critical patent/DE60019649T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/26—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton
    • C07C17/272—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions
    • C07C17/278—Preparation of halogenated hydrocarbons by reactions involving an increase in the number of carbon atoms in the skeleton by addition reactions of only halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/383—Separation; Purification; Stabilisation; Use of additives by distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
DE60019649T 2000-09-29 2000-12-13 Verfahren zur herstellung von 1,1,1,3,3-pentachlorpropan Expired - Lifetime DE60019649T2 (de)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US671993 1996-06-28
US09/671,993 US6313360B1 (en) 2000-09-29 2000-09-29 Process for the manufacture of 1, 1, 1, 3, 3-pentachloropropane
PCT/US2000/032454 WO2002028806A1 (en) 2000-09-29 2000-12-13 Process for the manufacture of 1,1,1,3,3-pentachloropropane

Publications (2)

Publication Number Publication Date
DE60019649D1 true DE60019649D1 (de) 2005-05-25
DE60019649T2 DE60019649T2 (de) 2006-01-19

Family

ID=24696710

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60019649T Expired - Lifetime DE60019649T2 (de) 2000-09-29 2000-12-13 Verfahren zur herstellung von 1,1,1,3,3-pentachlorpropan

Country Status (8)

Country Link
US (1) US6313360B1 (de)
EP (1) EP1328496B1 (de)
JP (1) JP2004524272A (de)
AT (1) ATE293586T1 (de)
DE (1) DE60019649T2 (de)
ES (1) ES2237488T3 (de)
MX (1) MXPA03002713A (de)
WO (1) WO2002028806A1 (de)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6500995B1 (en) * 2001-06-14 2002-12-31 Vulcan Chemicals Water-enhanced production of 1,1,1,3,3,-pentachloropropane
US20050177012A1 (en) * 2001-07-20 2005-08-11 Pcbu Services, Inc. Halocarbon production processes, halocarbon separation processes, and halocarbon separation systems
US7094936B1 (en) 2001-07-20 2006-08-22 Great Lakes Chemical Corporation Process for preparing halogenated alkanes
US20030028057A1 (en) * 2001-07-20 2003-02-06 Stephen Owens Methods and materials for the preparation and purification of halogenated hydrocarbons
US6552238B1 (en) * 2001-08-31 2003-04-22 Vulcan Chemicals Separation of heavy ends from streams of halogenated alkanes
US6720466B2 (en) * 2002-04-17 2004-04-13 Vulcan Chemicals, a division of Vulcan Materials Company 1,1,1,3,3-pentachloropropane process purge stream concentration using a secondary refluxed evaporator and secondary product recovery
US20040225166A1 (en) * 2003-05-05 2004-11-11 Vulcan Chemicals A Business Group Of Vulcan Materials Company Method for producing 1,1,1,3-tetrachloropropane and other haloalkanes with iron catalyst
US7112709B2 (en) * 2003-09-09 2006-09-26 Vulcan Chemicals Method for reusing heavy end by-products in the manufacture of polychlorinated alkanes
US7265082B2 (en) * 2004-08-04 2007-09-04 Honeywell International Inc. Azeotrope-like compositions of 1,1,1,3,3-pentachloropropane and carbon tetrachloride
US20070106099A1 (en) * 2005-11-10 2007-05-10 Pcbu Services, Inc. Production processes and systems
CN100427442C (zh) * 2005-12-19 2008-10-22 浙江蓝天环保高科技股份有限公司 1,1,1,3,3-五氯丙烷的改进制备方法
EP1908744A1 (de) * 2006-10-06 2008-04-09 SOLVAY (Société Anonyme) Verfahren zur Herstellung von halogenierten Kohlenwasserstoffen mit mitdestens 3 Kohlenatomen im Beisein von Eisen und einem Phosphit
US9738577B2 (en) * 2006-10-11 2017-08-22 Honeywell International Inc. Process for the manufacture of 1,1,1,3,3-pentachloropropane
SI2687504T1 (sl) 2007-12-19 2016-02-29 Occidental Chemical Corporation Metode za izdelavo kloriranih ogljikovodikov
JP2011057650A (ja) * 2009-09-14 2011-03-24 Tokuyama Corp クロロプロペンの製造方法
CN101913980A (zh) * 2010-09-07 2010-12-15 西安近代化学研究所 1，1，1，3，3-五氯丙烷的生产方法
JP5642495B2 (ja) * 2010-10-22 2014-12-17 株式会社トクヤマ ポリクロロプロパンを製造するための連続バッチ反応方法
CN103119006A (zh) * 2010-10-22 2013-05-22 株式会社德山 用于制造聚氯丙烷的连续分批反应方法
JP5783707B2 (ja) * 2010-11-15 2015-09-24 株式会社トクヤマ ポリクロロプロパンを製造するための連続バッチ反応方法
US9156752B2 (en) 2011-01-04 2015-10-13 Honeywell International Inc. High purity E-1-chloro-3,3,3-trifluoropropene and methods of making the same
US8722946B2 (en) * 2011-06-03 2014-05-13 Honeywell International Inc. Method for avoiding the generation of by-products during the production of haloalkane compounds
US10112166B2 (en) * 2011-06-03 2018-10-30 Honeywell International Inc. Method for capturing and recycling iron catalyst used in the production of haloalkane compounds
US8835702B2 (en) * 2011-06-03 2014-09-16 Honeywell International Inc. Method for mitigating the formation of by-products during the production of haloalkane compounds
JP6375498B2 (ja) 2011-10-14 2018-08-22 ハニーウェル インターナショナル，インコーポレイティド ２，３，３，３−テトラフルオロプロペンの製造方法
CN103373894B (zh) * 2012-04-13 2015-03-18 中化蓝天集团有限公司 一种制备c3饱和卤代烷烃的连续方法
JP6158032B2 (ja) * 2012-10-17 2017-07-05 株式会社トクヤマ 反応ガスをリサイクルした塩素化プロパンの製造方法
US9289758B2 (en) 2013-01-22 2016-03-22 Axiall Ohio, Inc. Processes for producing chlorinated hydrocarbons and methods for recovering polyvalent antimony catalysts therefrom
US8889930B2 (en) 2013-01-22 2014-11-18 Axiall Ohio, Inc. Process for producing chlorinated hydrocarbons
US9067858B2 (en) * 2013-02-12 2015-06-30 Occidental Chemical Corporation Methods for recovering 1,1,1,2,3-pentachloropropane
US9139497B2 (en) 2013-10-23 2015-09-22 Axiall Ohio, Inc. Process for producing chlorinated hydrocarbons in the presence of a polyvalent bismuth compound
PT3412648T (pt) 2014-05-16 2020-07-15 Occidental Chem Co Método de fabrico de 1,1,3,3-tetracloropropeno
US9896400B2 (en) 2014-10-16 2018-02-20 Spolek Pro Chemickou A Hutni Vyrobu A.S. Process for producing a chlorinated C3-6 alkane
FR3027304B1 (fr) * 2014-10-16 2018-02-23 Arkema France Compositions a base de 1,1,1,3,3-pentachloropropane
CN104496745B (zh) * 2014-11-28 2018-05-04 巨化集团技术中心 一种合成氯代烃的制备方法
CN104513127B (zh) * 2014-11-28 2018-08-03 巨化集团技术中心 一种1,1,1,3,3-五氯丙烷的制备方法
CN105418360B (zh) * 2015-11-11 2017-09-08 西安近代化学研究所 一种制备1,1,1,3,3‑五氯丁烷的方法
JP6843866B2 (ja) 2016-01-04 2021-03-17 ブルー キューブ アイピー エルエルシー ハロゲン化アルカンを調製するための改善されたプロセス
CN105859512B (zh) * 2016-04-19 2019-01-22 浙江衢州巨新氟化工有限公司 一种1,1,1,3,3-五氯丙烷的制备方法
PT3481797T (pt) 2016-07-05 2021-05-13 Occidental Chem Co Fotocloração de clorofórmio em tetracloreto de carbono
WO2018022488A1 (en) * 2016-07-26 2018-02-01 Occidental Chemical Corporation Methods for producing halogenated propanes
CN108033872B (zh) * 2017-12-05 2021-07-09 安庆市华璞环保材料科技有限责任公司 一种清洁环保生产1,1’,2,3-四氯丙烯的方法及其设备
US11192841B2 (en) 2018-04-03 2021-12-07 Blue Cube Ip Llc Processes for preparing halogenated alkanes
CN111902384B (zh) * 2018-04-03 2024-05-14 蓝立方知识产权有限责任公司 在氯化烷烃生产中回收催化剂的方法
WO2020146722A1 (en) 2019-01-10 2020-07-16 Occidental Chemical Corporation Photochlorination of partially-chlorinated chloromethanes to carbon tetrachloride

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE22877T1 (de) * 1983-07-06 1986-11-15 Monsanto Co Verfahren zur herstellung von monoaddukten von olefinen und damit reagierfaehigen telogenen.
EP0729932A1 (de) * 1995-03-03 1996-09-04 Central Glass Company, Limited Verfahren zur Herstellung von Halopropan
JP2000086545A (ja) * 1998-09-18 2000-03-28 Asahi Glass Co Ltd １，１，１，３，３−ペンタクロロプロパンの製造方法
BE1012268A3 (fr) * 1998-11-05 2000-08-01 Solvay Procede de preparation d'hydrocarbures halogenes.
US6187978B1 (en) 1999-05-12 2001-02-13 Alliedsignal Inc. Continuous process for manufacturing halogenated compounds

Also Published As

Publication number Publication date
EP1328496A1 (de) 2003-07-23
ES2237488T3 (es) 2005-08-01
WO2002028806A1 (en) 2002-04-11
EP1328496B1 (de) 2005-04-20
JP2004524272A (ja) 2004-08-12
US6313360B1 (en) 2001-11-06
DE60019649T2 (de) 2006-01-19
MXPA03002713A (es) 2005-07-25
ATE293586T1 (de) 2005-05-15

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Legal Events

Date Code Title Description
8327 Change in the person/name/address of the patent owner

Owner name: BASIC CHEMICALS COMPANY, LLC, DALLAS, TEX., US

8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: OCCIDENTAL CHEMICAL CORP. (N.D.GES.D. STAATES , US