DE4213154C1 - - Google Patents

Info

Publication number
DE4213154C1
DE4213154C1 DE4213154A DE4213154A DE4213154C1 DE 4213154 C1 DE4213154 C1 DE 4213154C1 DE 4213154 A DE4213154 A DE 4213154A DE 4213154 A DE4213154 A DE 4213154A DE 4213154 C1 DE4213154 C1 DE 4213154C1
Authority
DE
Germany
Prior art keywords
pfos
water
distillation
oxidizing agent
polymerization
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE4213154A
Other languages
German (de)
English (en)
Inventor
Ludwig Dr. 8263 Burghausen De Mayer
Gernot Dr. 8269 Burgkirchen De Loehr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dyneon GmbH
Original Assignee
Hoechst AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hoechst AG filed Critical Hoechst AG
Priority to DE4213154A priority Critical patent/DE4213154C1/de
Priority to EP93106036A priority patent/EP0566974B1/de
Priority to DE59300654T priority patent/DE59300654D1/de
Priority to JP09455293A priority patent/JP3517429B2/ja
Priority to CA002094557A priority patent/CA2094557A1/en
Priority to US08/050,874 priority patent/US5312935A/en
Priority to PL93298658A priority patent/PL171431B1/pl
Priority to KR1019930006768A priority patent/KR930021598A/ko
Application granted granted Critical
Publication of DE4213154C1 publication Critical patent/DE4213154C1/de
Priority to HK98106874A priority patent/HK1007742A1/xx
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42Separation; Purification; Stabilisation; Use of additives
    • C07C51/487Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE4213154A 1992-04-22 1992-04-22 Expired - Fee Related DE4213154C1 (US20020193084A1-20021219-M00002.png)

Priority Applications (9)

Application Number Priority Date Filing Date Title
DE4213154A DE4213154C1 (US20020193084A1-20021219-M00002.png) 1992-04-22 1992-04-22
DE59300654T DE59300654D1 (de) 1992-04-22 1993-04-14 Reinigung von fluorierten Carbonsäuren.
EP93106036A EP0566974B1 (de) 1992-04-22 1993-04-14 Reinigung von fluorierten Carbonsäuren
CA002094557A CA2094557A1 (en) 1992-04-22 1993-04-21 Purification of fluorinated carboxylic acids
JP09455293A JP3517429B2 (ja) 1992-04-22 1993-04-21 弗素化カルボン酸の精製方法
US08/050,874 US5312935A (en) 1992-04-22 1993-04-21 Purification of fluorinated carboxylic acids
PL93298658A PL171431B1 (pl) 1992-04-22 1993-04-21 Sposób oczyszczania zanieczyszczonych fluorowanych kwasów karboksylowych PL PL
KR1019930006768A KR930021598A (ko) 1992-04-22 1993-04-22 플루오르화된 카복실산의 정제방법
HK98106874A HK1007742A1 (en) 1992-04-22 1998-06-26 Purification of fluorinated carboxylic acids

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE4213154A DE4213154C1 (US20020193084A1-20021219-M00002.png) 1992-04-22 1992-04-22

Publications (1)

Publication Number Publication Date
DE4213154C1 true DE4213154C1 (US20020193084A1-20021219-M00002.png) 1993-06-17

Family

ID=6457194

Family Applications (2)

Application Number Title Priority Date Filing Date
DE4213154A Expired - Fee Related DE4213154C1 (US20020193084A1-20021219-M00002.png) 1992-04-22 1992-04-22
DE59300654T Expired - Fee Related DE59300654D1 (de) 1992-04-22 1993-04-14 Reinigung von fluorierten Carbonsäuren.

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE59300654T Expired - Fee Related DE59300654D1 (de) 1992-04-22 1993-04-14 Reinigung von fluorierten Carbonsäuren.

Country Status (8)

Country Link
US (1) US5312935A (US20020193084A1-20021219-M00002.png)
EP (1) EP0566974B1 (US20020193084A1-20021219-M00002.png)
JP (1) JP3517429B2 (US20020193084A1-20021219-M00002.png)
KR (1) KR930021598A (US20020193084A1-20021219-M00002.png)
CA (1) CA2094557A1 (US20020193084A1-20021219-M00002.png)
DE (2) DE4213154C1 (US20020193084A1-20021219-M00002.png)
HK (1) HK1007742A1 (US20020193084A1-20021219-M00002.png)
PL (1) PL171431B1 (US20020193084A1-20021219-M00002.png)

Families Citing this family (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5663824A (en) * 1993-11-02 1997-09-02 Lucent Technologies Inc. Optical modulators as monolithically integrated optical isolators
DE19824614A1 (de) 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
DE19824615A1 (de) 1998-06-02 1999-12-09 Dyneon Gmbh Verfahren zur Rückgewinnung von fluorierten Alkansäuren aus Abwässern
US6252105B1 (en) 1998-07-06 2001-06-26 Solvay Fluor Und Derivate Gmbh Synthesis of low-fluoride organic compounds
CN1207256C (zh) * 1998-07-06 2005-06-22 索尔微氟及衍生物有限公司 贫氟化物有机化合物的制备
DE19933696A1 (de) * 1999-07-17 2001-01-18 Dyneon Gmbh Verfahren zur Rückgewinnung fluorierter Emulgatoren aus wässrigen Phasen
US6794550B2 (en) 2000-04-14 2004-09-21 3M Innovative Properties Company Method of making an aqueous dispersion of fluoropolymers
JP5055652B2 (ja) 2000-08-11 2012-10-24 ダイキン工業株式会社 含フッ素界面活性剤の回収方法
US6281374B1 (en) 2000-08-23 2001-08-28 E. I. Du Pont De Nemours And Company Fluorinated alkanoic acid purification process
US6720437B2 (en) 2001-02-07 2004-04-13 E. I. Du Pont De Nemours And Company Fluorinated carboxylic acid recovery and reuse
US7125941B2 (en) * 2001-03-26 2006-10-24 3M Innovative Properties Company Aqueous emulsion polymerization process for producing fluoropolymers
US6737489B2 (en) 2001-05-21 2004-05-18 3M Innovative Properties Company Polymers containing perfluorovinyl ethers and applications for such polymers
US7045571B2 (en) 2001-05-21 2006-05-16 3M Innovative Properties Company Emulsion polymerization of fluorinated monomers
US7279522B2 (en) 2001-09-05 2007-10-09 3M Innovative Properties Company Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant
US6833418B2 (en) 2002-04-05 2004-12-21 3M Innovative Properties Company Dispersions containing perfluorovinyl ether homopolymers and use thereof
US6822059B2 (en) 2002-04-05 2004-11-23 3M Innovative Properties Company Dispersions containing bicomponent fluoropolymer particles and use thereof
US7341647B2 (en) * 2002-06-13 2008-03-11 Yamasaki Industries Co., Ltd. Coke carbonization furnace cover for promoting increase in temperature of coal particles near the cover
CN100381366C (zh) * 2002-06-19 2008-04-16 笹仓机械工程有限公司 含氟乳化剂的回收方法
EP1562640B1 (en) * 2002-10-18 2012-12-05 McMaster University Methods for purifying radiolabelled compounds
EP1533325B1 (en) * 2003-11-17 2011-10-19 3M Innovative Properties Company Aqueous dispersions of polytetrafluoroethylene having a low amount of fluorinated surfactant
ATE433350T1 (de) * 2004-03-01 2009-06-15 3M Innovative Properties Co Verfahren zum beschichten eines gegenstands mit einer fluorhaltigen kunststoffsdispersion
GB2427170A (en) * 2005-06-17 2006-12-20 3M Innovative Properties Co Fluoropolymer film having glass microspheres
US20080015304A1 (en) * 2006-07-13 2008-01-17 Klaus Hintzer Aqueous emulsion polymerization process for producing fluoropolymers
GB0514387D0 (en) * 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant
GB0525978D0 (en) * 2005-12-21 2006-02-01 3M Innovative Properties Co Fluorinated Surfactants For Making Fluoropolymers
GB0523853D0 (en) 2005-11-24 2006-01-04 3M Innovative Properties Co Fluorinated surfactants for use in making a fluoropolymer
US20070025902A1 (en) * 2005-07-15 2007-02-01 3M Innovative Properties Company Recovery of fluorinated carboxylic acid from adsorbent particles
GB0514398D0 (en) * 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
GB2430437A (en) * 2005-09-27 2007-03-28 3M Innovative Properties Co Method of making a fluoropolymer
US7728087B2 (en) 2005-12-23 2010-06-01 3M Innovative Properties Company Fluoropolymer dispersion and method for making the same
US20070276103A1 (en) * 2006-05-25 2007-11-29 3M Innovative Properties Company Fluorinated Surfactants
US7754795B2 (en) * 2006-05-25 2010-07-13 3M Innovative Properties Company Coating composition
US8119750B2 (en) * 2006-07-13 2012-02-21 3M Innovative Properties Company Explosion taming surfactants for the production of perfluoropolymers
US7820851B2 (en) * 2006-09-28 2010-10-26 Perkinelmer Health Sciences, Inc. Isotopically labeled polyfluorinated compound useful as an imaging tracer
US20100084343A1 (en) * 2007-02-16 2010-04-08 Mader Brian T System and process for the removal of fluorochemicals from water
US20080264864A1 (en) * 2007-04-27 2008-10-30 3M Innovative Properties Company PROCESS FOR REMOVING FLUORINATED EMULSIFIER FROM FLUOROPOLMER DISPERSIONS USING AN ANION-EXCHANGE RESIN AND A pH-DEPENDENT SURFACTANT AND FLUOROPOLYMER DISPERSIONS CONTAINING A pH-DEPENDENT SURFACTANT
FR2921565B1 (fr) * 2007-09-28 2011-05-20 Rhodia Operations Procede de recuperation d'acides fluorocarboxyliques
WO2009157416A1 (ja) 2008-06-24 2009-12-30 旭硝子株式会社 含フッ素化合物の精製方法
JP5347851B2 (ja) 2008-09-08 2013-11-20 ダイキン工業株式会社 フルオロカルボン酸の製造方法
JP6532524B2 (ja) 2014-04-18 2019-06-19 スリーエム イノベイティブ プロパティズ カンパニー 分枝状フッ素化乳化剤の回収
JP6795033B2 (ja) 2016-06-16 2020-12-02 ダイキン工業株式会社 炭素数2〜20の含フッ素有機酸の製造方法および炭素数2〜20の含フッ素有機酸を含む組成物

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01117840A (ja) * 1987-10-30 1989-05-10 Shinakita Kasei Kk n―ペルフルオロオクタン酸の分離方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3833626A (en) * 1968-09-23 1974-09-03 Chem Nunchritz Veb Process for preparing perfluorinated mono-and dicarboxylic acids
US3709795A (en) * 1970-02-02 1973-01-09 Monsanto Co Purification of carboxylic acids by chemical treatment and distillation
US4609497A (en) * 1985-03-14 1986-09-02 E. I. Du Pont De Nemours And Company Process for separating surfactants used in the manufacture of concentrated fluoropolymer dispersions
DE3606174A1 (de) * 1986-02-26 1987-08-27 Hoechst Ag Verfahren zur herstellung von perfluorcarbonsaeuren

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01117840A (ja) * 1987-10-30 1989-05-10 Shinakita Kasei Kk n―ペルフルオロオクタン酸の分離方法

Also Published As

Publication number Publication date
JPH0625072A (ja) 1994-02-01
HK1007742A1 (en) 1999-04-23
US5312935A (en) 1994-05-17
KR930021598A (ko) 1993-11-22
JP3517429B2 (ja) 2004-04-12
EP0566974A1 (de) 1993-10-27
EP0566974B1 (de) 1995-09-27
PL298658A1 (en) 1993-12-13
CA2094557A1 (en) 1993-10-23
PL171431B1 (pl) 1997-04-30
DE59300654D1 (de) 1995-11-02

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Legal Events

Date Code Title Description
8100 Publication of the examined application without publication of unexamined application
D1 Grant (no unexamined application published) patent law 81
8364 No opposition during term of opposition
8327 Change in the person/name/address of the patent owner

Owner name: DYNEON GMBH, 84508 BURGKIRCHEN, DE

R119 Application deemed withdrawn, or ip right lapsed, due to non-payment of renewal fee

Effective date: 20111101