DE3902042A1 - Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungen - Google Patents
Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungenInfo
- Publication number
- DE3902042A1 DE3902042A1 DE3902042A DE3902042A DE3902042A1 DE 3902042 A1 DE3902042 A1 DE 3902042A1 DE 3902042 A DE3902042 A DE 3902042A DE 3902042 A DE3902042 A DE 3902042A DE 3902042 A1 DE3902042 A1 DE 3902042A1
- Authority
- DE
- Germany
- Prior art keywords
- tin
- aqueous
- optionally
- lead
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002253 acid Substances 0.000 title claims description 15
- 230000008021 deposition Effects 0.000 title claims description 10
- 229910000978 Pb alloy Inorganic materials 0.000 title claims description 6
- 229910001128 Sn alloy Inorganic materials 0.000 title claims description 6
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 14
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 12
- 238000005882 aldol condensation reaction Methods 0.000 claims description 12
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical group [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 claims description 11
- 239000003929 acidic solution Substances 0.000 claims description 11
- 239000007859 condensation product Substances 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 claims description 10
- 150000003839 salts Chemical class 0.000 claims description 10
- -1 aliphatic amines Chemical class 0.000 claims description 7
- 239000002184 metal Substances 0.000 claims description 7
- 229920000151 polyglycol Polymers 0.000 claims description 7
- 239000010695 polyglycol Substances 0.000 claims description 7
- 150000008365 aromatic ketones Chemical class 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 6
- 239000000080 wetting agent Substances 0.000 claims description 6
- 150000001735 carboxylic acids Chemical class 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- BWHOZHOGCMHOBV-UHFFFAOYSA-N Benzalacetone Natural products CC(=O)C=CC1=CC=CC=C1 BWHOZHOGCMHOBV-UHFFFAOYSA-N 0.000 claims description 4
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 4
- 150000003998 acyclic ketones Chemical class 0.000 claims description 4
- 150000001299 aldehydes Chemical class 0.000 claims description 4
- 125000000217 alkyl group Chemical group 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- BWHOZHOGCMHOBV-BQYQJAHWSA-N trans-benzylideneacetone Chemical compound CC(=O)\C=C\C1=CC=CC=C1 BWHOZHOGCMHOBV-BQYQJAHWSA-N 0.000 claims description 4
- 150000003934 aromatic aldehydes Chemical class 0.000 claims description 3
- 125000003118 aryl group Chemical group 0.000 claims description 3
- UIERETOOQGIECD-UHFFFAOYSA-N Angelic acid Natural products CC=C(C)C(O)=O UIERETOOQGIECD-UHFFFAOYSA-N 0.000 claims description 2
- 125000002877 alkyl aryl group Chemical group 0.000 claims description 2
- 150000001408 amides Chemical class 0.000 claims description 2
- 150000001413 amino acids Chemical class 0.000 claims description 2
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- 239000007795 chemical reaction product Substances 0.000 claims description 2
- RXKJFZQQPQGTFL-UHFFFAOYSA-N dihydroxyacetone Chemical compound OCC(=O)CO RXKJFZQQPQGTFL-UHFFFAOYSA-N 0.000 claims description 2
- 150000002429 hydrazines Chemical class 0.000 claims description 2
- IMACFCSSMIZSPP-UHFFFAOYSA-N phenacyl chloride Chemical compound ClCC(=O)C1=CC=CC=C1 IMACFCSSMIZSPP-UHFFFAOYSA-N 0.000 claims description 2
- UIERETOOQGIECD-ONEGZZNKSA-N tiglic acid Chemical compound C\C=C(/C)C(O)=O UIERETOOQGIECD-ONEGZZNKSA-N 0.000 claims description 2
- 241000282376 Panthera tigris Species 0.000 claims 1
- 239000002736 nonionic surfactant Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 1
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 10
- 238000000151 deposition Methods 0.000 description 7
- AICMYQIGFPHNCY-UHFFFAOYSA-J methanesulfonate;tin(4+) Chemical compound [Sn+4].CS([O-])(=O)=O.CS([O-])(=O)=O.CS([O-])(=O)=O.CS([O-])(=O)=O AICMYQIGFPHNCY-UHFFFAOYSA-J 0.000 description 5
- 229940098779 methanesulfonic acid Drugs 0.000 description 5
- IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical compound [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 description 5
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 4
- 235000019256 formaldehyde Nutrition 0.000 description 4
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 4
- LLABTCPIBSAMGS-UHFFFAOYSA-L lead(2+);methanesulfonate Chemical compound [Pb+2].CS([O-])(=O)=O.CS([O-])(=O)=O LLABTCPIBSAMGS-UHFFFAOYSA-L 0.000 description 3
- 150000004002 naphthaldehydes Chemical class 0.000 description 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 2
- 229920000847 nonoxynol Polymers 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- GSJBKPNSLRKRNR-UHFFFAOYSA-N $l^{2}-stannanylidenetin Chemical compound [Sn].[Sn] GSJBKPNSLRKRNR-UHFFFAOYSA-N 0.000 description 1
- SQAINHDHICKHLX-UHFFFAOYSA-N 1-naphthaldehyde Chemical compound C1=CC=C2C(C=O)=CC=CC2=C1 SQAINHDHICKHLX-UHFFFAOYSA-N 0.000 description 1
- QQGRFMIMXPWKPM-UHFFFAOYSA-N 2,3,4-tributylphenol Chemical compound CCCCC1=CC=C(O)C(CCCC)=C1CCCC QQGRFMIMXPWKPM-UHFFFAOYSA-N 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-M Bisulfite Chemical compound OS([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-M 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001721 carbon Chemical class 0.000 description 1
- 239000010406 cathode material Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 229960004279 formaldehyde Drugs 0.000 description 1
- LQBJWKCYZGMFEV-UHFFFAOYSA-N lead tin Chemical compound [Sn].[Pb] LQBJWKCYZGMFEV-UHFFFAOYSA-N 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 238000001465 metallisation Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/30—Electroplating: Baths therefor from solutions of tin
- C25D3/32—Electroplating: Baths therefor from solutions of tin characterised by the organic bath constituents used
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/56—Electroplating: Baths therefor from solutions of alloys
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/56—Electroplating: Baths therefor from solutions of alloys
- C25D3/60—Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of tin
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electrolytic Production Of Metals (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3902042A DE3902042A1 (de) | 1989-01-25 | 1989-01-25 | Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungen |
| DE90100870T DE59004841D1 (de) | 1989-01-25 | 1990-01-17 | Wässrige, saure Lösungen für die elektrolytische Abscheidung von Zinn und/oder Blei/Zinnlegierungen. |
| EP90100870A EP0379948B1 (de) | 1989-01-25 | 1990-01-17 | Wässrige, saure Lösungen für die elektrolytische Abscheidung von Zinn und/oder Blei/Zinnlegierungen |
| US07/469,066 US5021130A (en) | 1989-01-25 | 1990-01-23 | Aqueous acidic solutions for the electrodeposition of tin and lead/tin alloys |
| JP02014730A JP3096465B2 (ja) | 1989-01-25 | 1990-01-24 | 錫及び／又は鉛／錫合金の電着用酸性水溶液 |
| DD90337314A DD291785A5 (de) | 1989-01-25 | 1990-01-24 | Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungen |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3902042A DE3902042A1 (de) | 1989-01-25 | 1989-01-25 | Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE3902042A1 true DE3902042A1 (de) | 1990-07-26 |
| DE3902042C2 DE3902042C2 (enExample) | 1991-05-02 |
Family
ID=6372697
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE3902042A Granted DE3902042A1 (de) | 1989-01-25 | 1989-01-25 | Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungen |
| DE90100870T Expired - Lifetime DE59004841D1 (de) | 1989-01-25 | 1990-01-17 | Wässrige, saure Lösungen für die elektrolytische Abscheidung von Zinn und/oder Blei/Zinnlegierungen. |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE90100870T Expired - Lifetime DE59004841D1 (de) | 1989-01-25 | 1990-01-17 | Wässrige, saure Lösungen für die elektrolytische Abscheidung von Zinn und/oder Blei/Zinnlegierungen. |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5021130A (enExample) |
| EP (1) | EP0379948B1 (enExample) |
| JP (1) | JP3096465B2 (enExample) |
| DD (1) | DD291785A5 (enExample) |
| DE (2) | DE3902042A1 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19545427A1 (de) * | 1994-12-09 | 1996-07-11 | Glyco Metall Werke | Schichtwerkstoff für Gleitelemente sowie Verfahren und Mittel zu seiner Herstellung |
| DE19728777A1 (de) * | 1997-07-05 | 1999-04-08 | Glyco Metall Werke | Schichtverbundwerkstoff für Gleitelemente sowie Verfahren zur Herstellung von Lagerschalen |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5651873A (en) * | 1994-06-30 | 1997-07-29 | Mitsubishi Materials Corporation | Electroplating solution for forming Pb-Sn alloy bump electrodes on semiconductor wafer surface |
| US6267863B1 (en) | 1999-02-05 | 2001-07-31 | Lucent Technologies Inc. | Electroplating solution for electroplating lead and lead/tin alloys |
| EP1260614B1 (en) * | 2001-05-24 | 2008-04-23 | Shipley Co. L.L.C. | Tin plating |
| US6730209B2 (en) * | 2002-02-22 | 2004-05-04 | Lucent Technologies Inc. | Solder electroplating bath including brighteners having reduced volatility |
| GB0216331D0 (en) | 2002-07-13 | 2002-08-21 | Dana Corp | Bearings |
| AU2003272790A1 (en) * | 2002-10-08 | 2004-05-04 | Honeywell International Inc. | Semiconductor packages, lead-containing solders and anodes and methods of removing alpha-emitters from materials |
| JP4749746B2 (ja) * | 2005-03-24 | 2011-08-17 | Ｄｏｗａメタルテック株式会社 | 錫めっき材およびその製造方法 |
| CN110428939B (zh) * | 2019-08-09 | 2020-06-30 | 常州大学 | 一种高导电石墨烯铜/铝复合导线的制备方法 |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2525942A (en) * | 1945-06-29 | 1950-10-17 | Standard Oil Co | Electrodepositing bath and process |
| DE1260262B (de) * | 1963-05-06 | 1968-02-01 | Friedr Blasberg G M B H | Galvanisches Bad und Verfahren zur elektrolytischen Abscheidung hochglaenzender Zinnueberzuege |
| US4582576A (en) * | 1985-03-26 | 1986-04-15 | Mcgean-Rohco, Inc. | Plating bath and method for electroplating tin and/or lead |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4132610A (en) * | 1976-05-18 | 1979-01-02 | Hyogo Prefectural Government | Method of bright electroplating of tin-lead alloy |
-
1989
- 1989-01-25 DE DE3902042A patent/DE3902042A1/de active Granted
-
1990
- 1990-01-17 DE DE90100870T patent/DE59004841D1/de not_active Expired - Lifetime
- 1990-01-17 EP EP90100870A patent/EP0379948B1/de not_active Expired - Lifetime
- 1990-01-23 US US07/469,066 patent/US5021130A/en not_active Expired - Lifetime
- 1990-01-24 JP JP02014730A patent/JP3096465B2/ja not_active Expired - Lifetime
- 1990-01-24 DD DD90337314A patent/DD291785A5/de not_active IP Right Cessation
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2525942A (en) * | 1945-06-29 | 1950-10-17 | Standard Oil Co | Electrodepositing bath and process |
| DE1260262B (de) * | 1963-05-06 | 1968-02-01 | Friedr Blasberg G M B H | Galvanisches Bad und Verfahren zur elektrolytischen Abscheidung hochglaenzender Zinnueberzuege |
| US4582576A (en) * | 1985-03-26 | 1986-04-15 | Mcgean-Rohco, Inc. | Plating bath and method for electroplating tin and/or lead |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19545427A1 (de) * | 1994-12-09 | 1996-07-11 | Glyco Metall Werke | Schichtwerkstoff für Gleitelemente sowie Verfahren und Mittel zu seiner Herstellung |
| DE19728777A1 (de) * | 1997-07-05 | 1999-04-08 | Glyco Metall Werke | Schichtverbundwerkstoff für Gleitelemente sowie Verfahren zur Herstellung von Lagerschalen |
| DE19728777C2 (de) * | 1997-07-05 | 2001-03-15 | Federal Mogul Wiesbaden Gmbh | Schichtverbundwerkstoff für Gleitlager sowie Verfahren zur Herstellung von Lagerschalen |
Also Published As
| Publication number | Publication date |
|---|---|
| JP3096465B2 (ja) | 2000-10-10 |
| EP0379948A2 (de) | 1990-08-01 |
| US5021130A (en) | 1991-06-04 |
| JPH02232389A (ja) | 1990-09-14 |
| EP0379948B1 (de) | 1994-03-09 |
| DE3902042C2 (enExample) | 1991-05-02 |
| EP0379948A3 (de) | 1991-07-31 |
| DD291785A5 (de) | 1991-07-11 |
| DE59004841D1 (de) | 1994-04-14 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE69127394T2 (de) | Zinn-Elektroplattierung bei hoher Geschwindigkeit | |
| DE2122263C2 (de) | Verfahren zur Herstellung eines primären Glänzers für saure galvanische Verzinnungsbäder und dessen Verwendung | |
| DE60029549T2 (de) | Lösung für das Elektroplattieren einer glänzenden Zinn-Kupfer-Legierung | |
| DE69613075T2 (de) | Plattierungsbad für Sn-Bi Legierungen und Verfahren zur Abscheidung von Sn-Bi Legierungsfilmen | |
| DE2152785A1 (de) | Bad und Verfahren für die galvanische Abscheidung von Zinn, Blei oder Legierungen davon | |
| DE3902042C2 (enExample) | ||
| DE3710368C2 (enExample) | ||
| DE2428499A1 (de) | Glanzverzinkung | |
| DE3856429T2 (de) | Zinn, Blei- oder Zinn-Blei-Legierungselektrolyten für Elektroplattieren bei hoher Geschwindigkeit | |
| DE69724324T2 (de) | Verfahren zur Herstellung von halbglänzenden und von glänzenden elektrogalvanischen Beschichtungen unter Verwendung hoher Stromdichten in einem Bad, das ein Zinksalz einer Schwefel-enthaltenden Säure enthält und Zusammensetzung dafür | |
| DE2830441A1 (de) | Waessriges bad zur galvanischen abscheidung von zink und dessen verwendung | |
| DE2608644C3 (de) | Glanzzinkbad | |
| DE2319197B2 (de) | Waessriges bad und verfahren zur galvanischen abscheidung eines duktilen, festhaftenden zinkueberzugs | |
| CH629541A5 (de) | Verfahren zur elektrolytischen abscheidung einer eisenlegierung. | |
| DE3302502A1 (de) | Waessriges saures bad zur erzeugung galvanisch abgeschiedener zink-kobaltlegierungen und ein verfahren zur erzeugung halbglaenzender bis glaenzender zink-kobalt-legierungsueberzuege auf einem substrat unter verwendung dieses bades | |
| DE3122390A1 (de) | "waessriges galvanisches bad und verfahren zur abscheidung einer eine chromauflage vortaeuschenden kobalt-zink-legierung" | |
| DE2658934B2 (de) | Wäßriges cyanidfreies alkalisches Zinkbad zur galvanischen Erzeugung hochglänzender Zinküberzüge | |
| DE1952218A1 (de) | Verfahren und Mittel zum galvanischen Verzinnen | |
| WO1991016474A1 (de) | Saure nickelbäder, enthaltend 1-(2-sulfoethyl)-pyridiniumbetain | |
| DE2815786C2 (de) | Wäßriges Bad und Verfahren elektrochemischen Abscheidung von glänzenden Eisen-Nickel-Überzügen | |
| DE1956144C2 (de) | Wässriges saures Bad zur galvanischen Abscheidung eines Zinnüberzugs und Verfahren hierzu | |
| DE2431332A1 (de) | Galvanische abscheidung von glaenzendem nickel-eisen | |
| DE3228911C2 (enExample) | ||
| DE3139641C2 (de) | Galvanisches Bad zur Verwendung mit unlöslichen Anoden zur Abscheidung halbglänzender, duktiler und spannungsfreier Nickelüberzüge und Verfahren zu deren Abscheidung | |
| DE2948999C2 (de) | Wässriges, saures Bad zur galvanischen Abscheidung von Gold und Verfahren zur galvanischen Abscheidung von Hartgold unter seiner Verwendung |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| OP8 | Request for examination as to paragraph 44 patent law | ||
| D2 | Grant after examination | ||
| 8364 | No opposition during term of opposition | ||
| 8339 | Ceased/non-payment of the annual fee |