JP3096465B2 - 錫及び／又は鉛／錫合金の電着用酸性水溶液 - Google Patents
錫及び／又は鉛／錫合金の電着用酸性水溶液Info
- Publication number
- JP3096465B2 JP3096465B2 JP02014730A JP1473090A JP3096465B2 JP 3096465 B2 JP3096465 B2 JP 3096465B2 JP 02014730 A JP02014730 A JP 02014730A JP 1473090 A JP1473090 A JP 1473090A JP 3096465 B2 JP3096465 B2 JP 3096465B2
- Authority
- JP
- Japan
- Prior art keywords
- tin
- lead
- aqueous solution
- acidic aqueous
- electrodeposition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 title claims description 21
- 230000002378 acidificating effect Effects 0.000 title claims description 15
- 239000007864 aqueous solution Substances 0.000 title claims description 15
- 238000004070 electrodeposition Methods 0.000 title claims description 11
- 229910001128 Sn alloy Inorganic materials 0.000 title claims description 7
- 229910000978 Pb alloy Inorganic materials 0.000 title description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 14
- 229910001174 tin-lead alloy Inorganic materials 0.000 claims description 10
- -1 aliphatic amino acid Chemical class 0.000 claims description 8
- 229920000151 polyglycol Polymers 0.000 claims description 8
- 239000010695 polyglycol Substances 0.000 claims description 8
- 239000000080 wetting agent Substances 0.000 claims description 8
- IKHGUXGNUITLKF-UHFFFAOYSA-N Acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 claims description 6
- 150000003998 acyclic ketones Chemical class 0.000 claims description 6
- 150000003839 salts Chemical class 0.000 claims description 6
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims description 5
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 150000004002 naphthaldehydes Chemical class 0.000 claims description 5
- HSJKGGMUJITCBW-UHFFFAOYSA-N 3-hydroxybutanal Chemical compound CC(O)CC=O HSJKGGMUJITCBW-UHFFFAOYSA-N 0.000 claims description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 4
- BWHOZHOGCMHOBV-UHFFFAOYSA-N Benzalacetone Natural products CC(=O)C=CC1=CC=CC=C1 BWHOZHOGCMHOBV-UHFFFAOYSA-N 0.000 claims description 4
- 150000008365 aromatic ketones Chemical class 0.000 claims description 4
- 150000001875 compounds Chemical class 0.000 claims description 4
- BWHOZHOGCMHOBV-BQYQJAHWSA-N trans-benzylideneacetone Chemical compound CC(=O)\C=C\C1=CC=CC=C1 BWHOZHOGCMHOBV-BQYQJAHWSA-N 0.000 claims description 4
- UIERETOOQGIECD-UHFFFAOYSA-N Angelic acid Natural products CC=C(C)C(O)=O UIERETOOQGIECD-UHFFFAOYSA-N 0.000 claims description 3
- IKHGUXGNUITLKF-XPULMUKRSA-N acetaldehyde Chemical compound [14CH]([14CH3])=O IKHGUXGNUITLKF-XPULMUKRSA-N 0.000 claims description 3
- 125000002877 alkyl aryl group Chemical group 0.000 claims description 3
- 239000007795 chemical reaction product Substances 0.000 claims description 3
- LQBJWKCYZGMFEV-UHFFFAOYSA-N lead tin Chemical compound [Sn].[Pb] LQBJWKCYZGMFEV-UHFFFAOYSA-N 0.000 claims description 3
- IMACFCSSMIZSPP-UHFFFAOYSA-N phenacyl chloride Chemical group ClCC(=O)C1=CC=CC=C1 IMACFCSSMIZSPP-UHFFFAOYSA-N 0.000 claims description 3
- UIERETOOQGIECD-ONEGZZNKSA-N tiglic acid Chemical compound C\C=C(/C)C(O)=O UIERETOOQGIECD-ONEGZZNKSA-N 0.000 claims description 3
- 229910021626 Tin(II) chloride Inorganic materials 0.000 claims description 2
- 150000008431 aliphatic amides Chemical class 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 229910021529 ammonia Inorganic materials 0.000 claims description 2
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 2
- RXKJFZQQPQGTFL-UHFFFAOYSA-N dihydroxyacetone Chemical compound OCC(=O)CO RXKJFZQQPQGTFL-UHFFFAOYSA-N 0.000 claims description 2
- 229910045601 alloy Inorganic materials 0.000 claims 1
- 239000000956 alloy Substances 0.000 claims 1
- AFVFQIVMOAPDHO-UHFFFAOYSA-N Methanesulfonic acid Chemical compound CS(O)(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-N 0.000 description 9
- 239000007859 condensation product Substances 0.000 description 9
- 238000005882 aldol condensation reaction Methods 0.000 description 8
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- AICMYQIGFPHNCY-UHFFFAOYSA-J methanesulfonate;tin(4+) Chemical compound [Sn+4].CS([O-])(=O)=O.CS([O-])(=O)=O.CS([O-])(=O)=O.CS([O-])(=O)=O AICMYQIGFPHNCY-UHFFFAOYSA-J 0.000 description 5
- IUTCEZPPWBHGIX-UHFFFAOYSA-N tin(2+) Chemical compound [Sn+2] IUTCEZPPWBHGIX-UHFFFAOYSA-N 0.000 description 5
- IGFHQQFPSIBGKE-UHFFFAOYSA-N Nonylphenol Natural products CCCCCCCCCC1=CC=C(O)C=C1 IGFHQQFPSIBGKE-UHFFFAOYSA-N 0.000 description 4
- 238000000151 deposition Methods 0.000 description 4
- 229940098779 methanesulfonic acid Drugs 0.000 description 4
- SNQQPOLDUKLAAF-UHFFFAOYSA-N nonylphenol Chemical compound CCCCCCCCCC1=CC=CC=C1O SNQQPOLDUKLAAF-UHFFFAOYSA-N 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000008021 deposition Effects 0.000 description 3
- 239000006185 dispersion Substances 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 150000003934 aromatic aldehydes Chemical class 0.000 description 2
- 150000001735 carboxylic acids Chemical class 0.000 description 2
- LLABTCPIBSAMGS-UHFFFAOYSA-L lead(2+);methanesulfonate Chemical compound [Pb+2].CS([O-])(=O)=O.CS([O-])(=O)=O LLABTCPIBSAMGS-UHFFFAOYSA-L 0.000 description 2
- 229920000847 nonoxynol Polymers 0.000 description 2
- SQAINHDHICKHLX-UHFFFAOYSA-N 1-naphthaldehyde Chemical compound C1=CC=C2C(C=O)=CC=CC2=C1 SQAINHDHICKHLX-UHFFFAOYSA-N 0.000 description 1
- QQGRFMIMXPWKPM-UHFFFAOYSA-N 2,3,4-tributylphenol Chemical compound CCCCC1=CC=C(O)C(CCCC)=C1CCCC QQGRFMIMXPWKPM-UHFFFAOYSA-N 0.000 description 1
- AFVFQIVMOAPDHO-UHFFFAOYSA-M Methanesulfonate Chemical compound CS([O-])(=O)=O AFVFQIVMOAPDHO-UHFFFAOYSA-M 0.000 description 1
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000011260 aqueous acid Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000005282 brightening Methods 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000010406 cathode material Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000002659 electrodeposit Substances 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000009713 electroplating Methods 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 150000004665 fatty acids Chemical class 0.000 description 1
- 238000010907 mechanical stirring Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/30—Electroplating: Baths therefor from solutions of tin
- C25D3/32—Electroplating: Baths therefor from solutions of tin characterised by the organic bath constituents used
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/56—Electroplating: Baths therefor from solutions of alloys
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/56—Electroplating: Baths therefor from solutions of alloys
- C25D3/60—Electroplating: Baths therefor from solutions of alloys containing more than 50% by weight of tin
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electrolytic Production Of Metals (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE3902042.8 | 1989-01-25 | ||
| DE3902042A DE3902042A1 (de) | 1989-01-25 | 1989-01-25 | Waessrige, saure loesungen fuer die elektrolytische abscheidung von zinn und/oder blei/zinnlegierungen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH02232389A JPH02232389A (ja) | 1990-09-14 |
| JP3096465B2 true JP3096465B2 (ja) | 2000-10-10 |
Family
ID=6372697
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP02014730A Expired - Lifetime JP3096465B2 (ja) | 1989-01-25 | 1990-01-24 | 錫及び／又は鉛／錫合金の電着用酸性水溶液 |
Country Status (5)
| Country | Link |
|---|---|
| US (1) | US5021130A (enExample) |
| EP (1) | EP0379948B1 (enExample) |
| JP (1) | JP3096465B2 (enExample) |
| DD (1) | DD291785A5 (enExample) |
| DE (2) | DE3902042A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9666547B2 (en) | 2002-10-08 | 2017-05-30 | Honeywell International Inc. | Method of refining solder materials |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5651873A (en) * | 1994-06-30 | 1997-07-29 | Mitsubishi Materials Corporation | Electroplating solution for forming Pb-Sn alloy bump electrodes on semiconductor wafer surface |
| CN1100893C (zh) * | 1994-12-09 | 2003-02-05 | 格里卡金属工厂格里卡两合公司 | 滑动元件用层状材料及其制备方法和所用试剂 |
| DE19728777C2 (de) * | 1997-07-05 | 2001-03-15 | Federal Mogul Wiesbaden Gmbh | Schichtverbundwerkstoff für Gleitlager sowie Verfahren zur Herstellung von Lagerschalen |
| US6267863B1 (en) | 1999-02-05 | 2001-07-31 | Lucent Technologies Inc. | Electroplating solution for electroplating lead and lead/tin alloys |
| EP1260614B1 (en) * | 2001-05-24 | 2008-04-23 | Shipley Co. L.L.C. | Tin plating |
| US6730209B2 (en) * | 2002-02-22 | 2004-05-04 | Lucent Technologies Inc. | Solder electroplating bath including brighteners having reduced volatility |
| GB0216331D0 (en) | 2002-07-13 | 2002-08-21 | Dana Corp | Bearings |
| JP4749746B2 (ja) * | 2005-03-24 | 2011-08-17 | Ｄｏｗａメタルテック株式会社 | 錫めっき材およびその製造方法 |
| CN110428939B (zh) * | 2019-08-09 | 2020-06-30 | 常州大学 | 一种高导电石墨烯铜/铝复合导线的制备方法 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2525942A (en) * | 1945-06-29 | 1950-10-17 | Standard Oil Co | Electrodepositing bath and process |
| DE1260262B (de) * | 1963-05-06 | 1968-02-01 | Friedr Blasberg G M B H | Galvanisches Bad und Verfahren zur elektrolytischen Abscheidung hochglaenzender Zinnueberzuege |
| US4132610A (en) * | 1976-05-18 | 1979-01-02 | Hyogo Prefectural Government | Method of bright electroplating of tin-lead alloy |
| US4582576A (en) * | 1985-03-26 | 1986-04-15 | Mcgean-Rohco, Inc. | Plating bath and method for electroplating tin and/or lead |
-
1989
- 1989-01-25 DE DE3902042A patent/DE3902042A1/de active Granted
-
1990
- 1990-01-17 DE DE90100870T patent/DE59004841D1/de not_active Expired - Lifetime
- 1990-01-17 EP EP90100870A patent/EP0379948B1/de not_active Expired - Lifetime
- 1990-01-23 US US07/469,066 patent/US5021130A/en not_active Expired - Lifetime
- 1990-01-24 JP JP02014730A patent/JP3096465B2/ja not_active Expired - Lifetime
- 1990-01-24 DD DD90337314A patent/DD291785A5/de not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9666547B2 (en) | 2002-10-08 | 2017-05-30 | Honeywell International Inc. | Method of refining solder materials |
Also Published As
| Publication number | Publication date |
|---|---|
| DE3902042A1 (de) | 1990-07-26 |
| EP0379948A2 (de) | 1990-08-01 |
| US5021130A (en) | 1991-06-04 |
| JPH02232389A (ja) | 1990-09-14 |
| EP0379948B1 (de) | 1994-03-09 |
| DE3902042C2 (enExample) | 1991-05-02 |
| EP0379948A3 (de) | 1991-07-31 |
| DD291785A5 (de) | 1991-07-11 |
| DE59004841D1 (de) | 1994-04-14 |
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